KR860004118A - 황색아조-및 아족시-스틸벤염료의 저장안정성 농축 수용액의 제조방법 - Google Patents

황색아조-및 아족시-스틸벤염료의 저장안정성 농축 수용액의 제조방법 Download PDF

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Publication number
KR860004118A
KR860004118A KR1019850008398A KR850008398A KR860004118A KR 860004118 A KR860004118 A KR 860004118A KR 1019850008398 A KR1019850008398 A KR 1019850008398A KR 850008398 A KR850008398 A KR 850008398A KR 860004118 A KR860004118 A KR 860004118A
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South Korea
Prior art keywords
exchange reaction
salt
cation exchange
carried out
dye
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KR1019850008398A
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English (en)
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KR930010743B1 (ko
Inventor
티치카스 아타나시오스 (외 2)
Original Assignee
아놀드 자일러, 에른스트 알테르
시바-가이기 에이지
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Application filed by 아놀드 자일러, 에른스트 알테르, 시바-가이기 에이지 filed Critical 아놀드 자일러, 에른스트 알테르
Publication of KR860004118A publication Critical patent/KR860004118A/ko
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Publication of KR930010743B1 publication Critical patent/KR930010743B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0001—Post-treatment of organic pigments or dyes
    • C09B67/002—Influencing the physical properties by treatment with an amine
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B69/00—Dyes not provided for by a single group of this subclass
    • C09B69/02—Dyestuff salts, e.g. salts of acid dyes with basic dyes
    • C09B69/04—Dyestuff salts, e.g. salts of acid dyes with basic dyes of anionic dyes with nitrogen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
    • C09B67/0072—Preparations with anionic dyes or reactive dyes
    • C09B67/0073—Preparations of acid or reactive dyes in liquid form

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Cosmetics (AREA)
  • Paper (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)

Abstract

내용 없음

Description

황색아조- 및 아족시-스틸벤염료의 저장안정성 농축 수용액의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (11)

  1. 알칼리금속 하이드록사이드의 존재하에 4-니트로톨루엔-2-설폰산을 자체-축합시키고, 생성된 거의 불용성인 염료의 알칼리 금속염을 친유성 암모늄염을 경유하는 이중 양이온 교환반응에 의해 수용성 알칸을 암모늄염으로 전환시킴으로써 황색아조- 및 아족시-스틸벤 염료의 저장-안정성 농축 수용액을 제조하는 방법에 있어서, 이중 이온 교환반응을 니트로벤젠/물의 2-상시스템중세서, 1차 이온 교환 반응을 위해서는 총 탄소수가 12 내지 40인 디 또는 트리알킬아민을 사용하고, 2차이온 교환반응을 위해서는 각 알킬부분의 탄소수가 2 내지 4인 모노-, 디- 또는 트리알칸올 아민을 사용하여 수행함을 특징으로 하는 방법.
  2. 제1항에 있어서, 1차 양이온 교환 반응에 총 탄소수 12내지 25인 트리알킬아민을 사용하는 방법.
  3. 제1항에 있어서, 1차 양이온 교환 반응에 트리부틸아민 또는 트리-n-옥틸아민을 사용하는 방법.
  4. 제1항에 있어서, 2차 양이온 교환 반응을 C2-C4디알칸올 아민을 사용하여 수행하는 방법.
  5. 제4항에 있어서, 2차 양이온 교환반응을 디에탄올 아민을 사용하여 수행하는 방법.
  6. 제5항에 있어서, 거의 불용성인 염료염을 친유성 트리부틸암모늄염을 경유하여 수용성이 큰 디에탄올 암모늄염으로 전환시키는 방법.
  7. 제5항에 있어서, 거의 불용성인 염료염을 친유성 트리-n-옥틸암모늄염을 경유하여 수용성이 큰 디에탄올 암모늄 염으로 전환시키는 방법.
  8. 제1항에 있어서, 1차 양이온 교환 반응을 염료의 합성반응으로부터 생성된, 바람직하게는 산성화된 반응혼합물로부터 직접 수행하는 방법.
  9. 셀룰로오즈 물질에 제1항의 방법에 의하여 수득된 염료용액을 도입시키거나 적용하여, 셀룰로오즈 물질을 염색하는 방법.
  10. 제9항에 있어서, 염색할 물질이 종이인 방법.
  11. 제10항에 있어서, 염색을 펄프중에서 행하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019850008398A 1984-11-12 1985-11-11 황색 아조 - 및 아족시스틸벤 염료의 저장안정성 농축 수용액의 제조방법 KR930010743B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH5406/84A CH660017A5 (de) 1984-11-12 1984-11-12 Konzentrierte lagerstabile waessrige loesungen gelber stilbenazo(xy)farbstoffe.
CH5406/84-9 1984-11-12

Publications (2)

Publication Number Publication Date
KR860004118A true KR860004118A (ko) 1986-06-18
KR930010743B1 KR930010743B1 (ko) 1993-11-10

Family

ID=4293049

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019850008398A KR930010743B1 (ko) 1984-11-12 1985-11-11 황색 아조 - 및 아족시스틸벤 염료의 저장안정성 농축 수용액의 제조방법

Country Status (13)

Country Link
US (1) US5041539A (ko)
EP (1) EP0182743B1 (ko)
JP (1) JPH0699644B2 (ko)
KR (1) KR930010743B1 (ko)
AT (1) ATE59059T1 (ko)
AU (1) AU579904B2 (ko)
BR (1) BR8505664A (ko)
CA (1) CA1251786A (ko)
CH (1) CH660017A5 (ko)
DE (1) DE3580901D1 (ko)
ES (1) ES8701211A1 (ko)
FI (1) FI83884C (ko)
ZA (1) ZA858636B (ko)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH692246A5 (de) * 1996-12-13 2002-04-15 Basf Ag Verfahren zur Herstellung von Aminsalzen von 4-Nitrotoluol-2-sulfonsäure.
ATE273351T1 (de) 1999-06-02 2004-08-15 Ciba Sc Holding Ag Gelbe azo- und azoxystilbenfarbstoffe
EP1548069B1 (de) * 2003-12-22 2010-08-04 Basf Se Flüssigformulierungen von Direktfarbstoffen
JP2007262105A (ja) * 2004-07-01 2007-10-11 Nippon Kayaku Co Ltd アゾ及び／又はアゾキシスチルベン染料の濃厚水溶液の製造法
ES2390357T3 (es) * 2005-11-18 2012-11-12 Basf Se Formulaciones líquidas de colorantes directos
GB2433264A (en) * 2005-12-16 2007-06-20 Sun Chemical Ltd Process for preparing ammonium, phosphonium & sulphonium salts of anionic dyes from aqueous solution of a salt of dye & non-aqueous solution of an onium salt
DE112012001131T5 (de) 2011-03-09 2014-01-09 Council Of Scientific & Industrial Research Einstufiges Verfahren zur Synthese von "Yellow-11"-Farbstoff mit gleichmäßigem Farbton

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3679353A (en) * 1969-10-30 1972-07-25 Gaf Corp Direct dye,alkanolamine or morpholine,and neutral salt concentrate and milling preparation thereof
EP0021619A1 (en) * 1979-06-12 1981-01-07 Imperial Chemical Industries Plc A method of making concentrated aqueous solutions of dyes and these solutions
DE3045377A1 (de) * 1980-12-02 1982-08-19 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung elektrolytarmer sulfonsaeuregruppenhaltiger farbstoffe

Also Published As

Publication number Publication date
FI83884B (fi) 1991-05-31
ZA858636B (en) 1986-06-25
KR930010743B1 (ko) 1993-11-10
ES548738A0 (es) 1986-11-16
DE3580901D1 (de) 1991-01-24
CA1251786A (en) 1989-03-28
FI854410A (fi) 1986-05-13
JPS61115959A (ja) 1986-06-03
ATE59059T1 (de) 1990-12-15
CH660017A5 (de) 1987-03-13
EP0182743A3 (en) 1988-03-16
BR8505664A (pt) 1986-08-12
FI854410A0 (fi) 1985-11-08
FI83884C (fi) 1991-09-10
JPH0699644B2 (ja) 1994-12-07
US5041539A (en) 1991-08-20
EP0182743A2 (de) 1986-05-28
EP0182743B1 (de) 1990-12-12
AU4974785A (en) 1986-05-22
ES8701211A1 (es) 1986-11-16
AU579904B2 (en) 1988-12-15

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