KR850006936A - 티오페닐우레아의 제조방법 - Google Patents

티오페닐우레아의 제조방법 Download PDF

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Publication number
KR850006936A
KR850006936A KR1019850001220A KR850001220A KR850006936A KR 850006936 A KR850006936 A KR 850006936A KR 1019850001220 A KR1019850001220 A KR 1019850001220A KR 850001220 A KR850001220 A KR 850001220A KR 850006936 A KR850006936 A KR 850006936A
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South Korea
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hydrogen
formula
compound
halogen
sup
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KR1019850001220A
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KR900003999B1 (ko
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히로시(외 1) 나가세
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쿠라바야시 이꾸시로오
타께다야꾸힝 코오교오 가부시기가이샤
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C323/39—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton at least one of the nitrogen atoms being part of any of the groups, X being a hetero atom, Y being any atom
    • C07C323/43—Y being a hetero atom
    • C07C323/44—X or Y being nitrogen atoms
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C323/39—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton at least one of the nitrogen atoms being part of any of the groups, X being a hetero atom, Y being any atom

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Cosmetics (AREA)

Abstract

내용 없음

Description

티오페닐우레아의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 하기식(Ⅱ)의 화합물을 하기식(Ⅲ)의 화합물과 반응시켜 하기식(Ⅰ)의 벤조일우레아 유도체를 제조하는 방법.
    상기 식에서,X1은 수소 또는 할로겐이며, X2는 할로겐이며, Y1,Y2및 Y3는 수소, 할로겐 또는 알킬으로서, Y1,Y2및 Y3중 적어도 하나는 수소가 아니며, R은 수소 또는 -CFaZbH(3-a-b)이며, a 및 b는 0,1,2 또는 3의 수로서, a+b3의 조건을 지니며, Z는 할로겐이며, W1및 W2중 하나는 -N=C=O이며, 다른 하나는 아미노임.
  2. 제1항에 있어서, W1이 -N=C=O이며, W2는 아미노인 것을 특징으로 하는 방법.
  3. 제1항에 있어서, W1이 아미노이며, W2가 -N=C=O인 것을 특징으로 하는 방법.
  4. 제1항에 있어서, 하기식(Ⅰa)의 화합물, 하기식(Ⅰb)의 화합물 또는 하기식 (Ⅰc)의 화합물이 제조되는 것을 특징으로 하는 방법.
    상기 식에서, X1a는 F 또는 Cl이며, X2 a는 X1a가 F 인 경우 F 또는 Cl이며, X1a가 C1인 경우 수소 또는 Cl이며, Y1a는 Br,Cl,F 또는 메틸이며, Y2a는 수소, Cl 또는 메틸이며, Z′는 F 또는 Cl이며, Y1b는 수소 또는 F 이며, Y2b는 Br,Cl,F 또는 메틸이며, Y3a는 수소, Cl,F 또는 메틸이며, Y2c는 Br,Cl 또는 F 이며, Y3b는 F 또는Cl임.
  5. 제1항에 있어서, 하기식 (Ⅰd)의 화합물, 하기식(Ⅰc)의 화합물, 하기식 (Ⅰf)의 화합물 또는 하기식(Ⅰg)의 화합물이 제조되는 것을 특징으로 하는 방법.
    상기 식에서, X2b는 F 또는 Cl이며, Y1c는 F 또는 Cl이며, Y2b는 수소 또는 Cl이며, Y3b는 F 또는 Cl임.
  6. 제1항에 있어서, 하기식의 화합물이 제조되는 것을 특징으로 하는 방법.
    상기 식에서, X2b는 F 또는 Cl이며, Y1c는 F 또는 Cl이며, Y2b는 수소 또는 Cl임.
  7. 제6항에 있어서, N-(2,6-디플루오로벤조일)-N′-〔2-플루오로-4-(1,1,2-트리플루오로-2-클로로에틸티오)페닐〕우레아가 제조되는 것을 특징으로 하는 방법.
  8. 제1항에 있어서, N-(2,6-디플루오로벤조일)-N′-〔2-플루오로-4-(1,1,2,2-테트라플루오로에틸티오페닐〕우레아가 제조되는 것을 특징으로 하는 방법.
  9. 제1항에 있어서, N-(2,6-디플루오로벤조일)-N′-〔2-클로로-4-(1,1,2,2,-테트라플루오로에틸티오)페닐〕우레아가 제조되는 것을 특징으로 하는 방법.
  10. 액체담체에 용해 및 분산되거나 또는 고체담체와 혼합 및 흡착된 하기식(Ⅰ)의 벤조일우레아 유도체로 구성되는 것을 특징으로 하는 살충 또는 살난조성물을 제조하는 방법.
    상기 식에서, X1은 수소 또는 할로겐이며, X2는 할로겐이며, Y1,Y2및 Y3는 수소, 할로겐 또는 알킬으로서, Y1,Y2및 Y3중 적어도 하나는 수소가 아니며, R은 수소 또는 -CFaZbH(3-a-b)이며, a 및 b는 0,1,2 또는 3의 수로서 a+b3의 조건을 만족하며, Z는 할로겐임.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019850001220A 1984-02-27 1985-02-27 티오페닐우레아의 제조방법 KR900003999B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP36882/84 1984-02-27
JP36882 1984-02-27
JP59036882A JPS60181067A (ja) 1984-02-27 1984-02-27 ベンゾイル尿素誘導体，その製造法及び殺虫剤

Publications (2)

Publication Number Publication Date
KR850006936A true KR850006936A (ko) 1985-10-25
KR900003999B1 KR900003999B1 (ko) 1990-06-07

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KR1019850001220A KR900003999B1 (ko) 1984-02-27 1985-02-27 티오페닐우레아의 제조방법

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Country Link
US (1) US4632938A (ko)
EP (1) EP0154508B1 (ko)
JP (1) JPS60181067A (ko)
KR (1) KR900003999B1 (ko)
AT (1) ATE50766T1 (ko)
BR (1) BR8500851A (ko)
CA (1) CA1238343A (ko)
DE (1) DE3576333D1 (ko)
IL (1) IL74401A (ko)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5245071A (en) * 1970-05-15 1993-09-14 Duphar International Research B.V. Organic compounds derived from urea or thiourea
US5342958A (en) * 1970-05-15 1994-08-30 Solvay Duphar International Research B.V. Organic compounds derived from urea or thiourea
JPS60181063A (ja) * 1984-02-27 1985-09-14 Takeda Chem Ind Ltd ベンゾイル尿素誘導体、その製造法及び殺虫剤
US5288756A (en) * 1985-10-14 1994-02-22 Ciba-Geigy Corporation Benzoylphenylureas
EP0432135A1 (de) * 1986-02-28 1991-06-12 Ciba-Geigy Ag Zwischenprodukte für Benzoylphenylharnstoffe
US5157155A (en) * 1987-02-04 1992-10-20 Sumitomo Chemical Company, Limited Benzoylurea derivative and its production and use
AU595417B2 (en) * 1987-02-04 1990-03-29 Sumitomo Chemical Company, Limited A benzoylurea derivative and its production and use
FR2645537B1 (fr) * 1989-04-05 1994-03-04 Fabre Medicament Pierre Nouveaux sulfonamides derives d'acides benzocycliques ou benzoheterocycliques, leur preparation et leur application en therapeutique
US5326560A (en) * 1991-04-18 1994-07-05 Henderson Jack A Insecticide carriers and insecticides
JPH11240859A (ja) * 1997-12-26 1999-09-07 Nippon Bayer Agrochem Co Ltd フルオロ置換ベンゾイルウレア類及び有害生物防除剤
CN102976984B (zh) * 2003-08-29 2015-04-08 三井化学株式会社 农园艺用杀虫剂的制备中间体
JP4560026B2 (ja) 2006-10-04 2010-10-13 セイコーエプソン株式会社 フレキシブル基板及びこれを備えた電気光学装置、並びに電子機器

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4013717A (en) * 1970-05-15 1977-03-22 U.S. Philips Corporation Benzoyl phenyl urea derivatives having insecticidal activities
US4089975A (en) * 1977-05-13 1978-05-16 The Dow Chemical Company Method of controlling manure-breeding insects
DE2726684A1 (de) * 1977-06-14 1979-01-04 Hoechst Ag Insektizide mittel
DE2801316A1 (de) * 1978-01-13 1979-07-19 Bayer Ag Substituierte n-phenyl-n'-(2-chlor- 6-fluor-benzoyl)-harnstoffe, verfahren zu ihrer herstellung und ihre verwendung als insektizide
DE2837086A1 (de) * 1978-08-24 1980-03-06 Bayer Ag Substituierte n-phenyl-n'-benzoyl- thioharnstoffe, verfahren zu ihrer herstellung und ihre verwendung als schaedlingsbekaempfungsmittel
EP0023884B1 (de) * 1979-07-11 1983-07-20 Ciba-Geigy Ag N-Phenyl-N'-benzoylharnstoffe, Verfahren zu ihrer Herstellung, diese Verbindungen enthaltende Mittel und ihre Verwendung zur Bekämpfung von Schädlingen
DK172687B1 (da) * 1981-07-30 1999-05-31 Dow Agrosciences Llc Substituerede N-aroyl-N'-phenyl-urinstofforbindelser, mellemprodukt til brug ved fremstilling deraf, en fremgangsmåde til d
GB2106501B (en) * 1981-09-18 1986-01-22 Dow Chemical Co Method for making benzoylphenylureas
GB2106500B (en) * 1981-09-18 1986-01-02 Dow Chemical Co Method for making benzoylphenylureas
GB2106499B (en) * 1981-09-18 1986-01-02 Dow Chemical Co Method for making benzoylphenylureas

Also Published As

Publication number Publication date
JPH0324469B2 (ko) 1991-04-03
BR8500851A (pt) 1985-10-15
EP0154508B1 (en) 1990-03-07
JPS60181067A (ja) 1985-09-14
KR900003999B1 (ko) 1990-06-07
CA1238343A (en) 1988-06-21
DE3576333D1 (de) 1990-04-12
IL74401A0 (en) 1985-05-31
ATE50766T1 (de) 1990-03-15
EP0154508A2 (en) 1985-09-11
US4632938A (en) 1986-12-30
IL74401A (en) 1988-11-30
EP0154508A3 (en) 1986-06-11

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