KR870008848A - 페닐우레아의 제조방법 - Google Patents

페닐우레아의 제조방법 Download PDF

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KR870008848A
KR870008848A KR870002415A KR870002415A KR870008848A KR 870008848 A KR870008848 A KR 870008848A KR 870002415 A KR870002415 A KR 870002415A KR 870002415 A KR870002415 A KR 870002415A KR 870008848 A KR870008848 A KR 870008848A
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halogen
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dichloro
phenyl
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엘·카르니 로버트
엠·그루버 존
에스·티·루이 알프레드
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월터스몰더스
산도즈 크롭, 프로텍션 코오포레이숀
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    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
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    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
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Abstract

내용 없음

Description

페닐우레아의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. a) 하기의 구조식(Ⅰ)의 화합물을 하기의 구조식(Ⅱ)의 화합물과 반응시키거나, 또는
    b) 하기의 구조식(Ⅲ)의 벤즈아미드를 하기의 구조식(Ⅳ)의 화합물과 반응시키는 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
    식중, X1, X2, X3및 X5는 각각 수소, 할로겐 또는 C1-4알킬이고,
    X4는 수소, 할로겐, 비치환 또는 할로겐화 C1-4알킬 또는 COOR이고,
    X6은 수소, 할로겐, C1-8알킬 또는 COOR´이고,
    Y는 산소 또는 황이고,
    A는 질소 또는 C-R4이고,
    B는 질소 또는 C-R3이고,
    R1및 R4는 각각 수소, 할로겐, 할로겐화 C1-8알킬, 비치환 또는 할로겐화 C1-8알콕시, 비치환 또는 할로겐화 C1-8알킬티오, 또는 비치환 또는 1 내지 4개의 할로겐원자로 치환되거나 하나의 CF3, C1-4알킬 또는 C1-4알콕시기와 0 내지 3개의 할로겐 원자로 치환된 아릴, 아릴옥시 또는 아릴티오이고,
    R2및 R3는 각각 수소, 할로겐, 시아노, 비치환 또는 할로겐화 C1-8알킬, 비치환 또는 할로겐화 C1-8알콕시, 비치환 또는 할로겐화 C1-8알킬티오, COOR˝, 비치환 또는 1 내지 4개의 할로겐 원자로 치환되거나 하나의 C1-4알킬, C1-4알콕시 또는 CF3기와 0 내지 3개의 할로겐원자로 치환된 아릴, 알콕시 또는 아릴티오이고,
    또는 R1및 R2또는 R2및 R3는 공히 4개의 탄소원자로 이루어진 포화 또는 불포화의 가교기를 형성할 수 있고, 경우에 따라서 1 내지 4개의 할로겐 원자로 치환되거나 하나의 트리플루오로메틸기와 0 내지 3개의 할로겐 원자로 치환 가능하고,
    R,R´및 R˝는 각각 수소 또는 C1-8알킬이고,
    A가 C-R4이고 B가 C-R3인 경우에는 R1,R2,R3및 R4모두가 수소는 아니다.
  2. 제 1 항에 있어서, A는 질소이고 B는 C-R3인 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
  3. 제 1 항 또는 제 2 항에 있어서, 아릴, 아릴옥시 또는 아릴티오는 비치환 또는 하나의 메틸, 메톡시 또는 CF3기와 0 또는 1개의 할로겐 또는 1 또는 2개의 할로겐으로 단일치환 또는 이치환되어서 아릴, 아릴옥시 및 아릴티오는 나프틸, 페닐, 피리딜 또는 티에닐을 표시하는 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
  4. 제 3 항에 있어서, Y노 0인 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
  5. 제 3 항 또는 제 4 항에 있어서, X1, X2및 X3는 각각 H 또는 할로겐이고, X4는 H, 할로겐, CH3또는 CF3이고, X5는 H, 할로겐 또는 CH3이고, X6은 H 또는 할로겐이고, R1및 R2는 각각 H, 할로겐 또는 CF3이고, R3는 H, 할로겐, C1-4알킬 또는 CF3이고, R1, R2및 R3중의 하나는 할로페닐, 디할로페닐, 메틸페닐 또는 트리플루오로메틸페닐일 수 있고, 또는 R1과 R2가 공히 비치환, 단일치환 또는 이치환된 구조식 CH=CH-CH=CH의 가교기를 형성하거나, 또는 R2와 R3가 공히 구조식(CH2)4의 가교기를 형성하는 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
  6. 제 5 항에 있어서, X1은 할로겐이고, X3및 X6은 H이고, X4는 할로겐, CH3또는 CF3이고, X5는 할로겐 또는 CH3이고, R3는 H, 할로겐, CF|3또는 할로페닐인 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
  7. 제 6 항에 있어서, 구조식(A)의 화합물은 하기의 화합물 중에서 선택되는 것을 특징으로 하는 구조식(A)의 화합물의 제조방법.
    a) N-3,5-디클로로-4-[4-클로로-3-(4-클로로페닐)-1-피라졸일]페닐-N´-2,6-디플루오로벤조일우레아
    b) N-3,5-디메틸-4-[4-클로로-3-(4-클로로페닐)-1-피라졸일]페닐-N´-2,6-디플루오로벤조일우레아
    c) N-3,5-디클로로-4-(4-브로모-1-피라졸일)-페닐-N´-2-클로로벤조일우레아
    d) N-3,5-디클로로-4-(3,4-디브로모-1-피라졸일)페닐-N´-2-클로로벤조일우레아
    e) N-3,5-디클로로-4-(4,5-디클로로-3-트리플루오로메틸-1-피라졸일) 페닐-N´-2-클로로벤조일우레아
    f) N-3,5-디클로로-4-[3-(4-클로로페닐)-1-피라졸일] 페닐-N´-2-클로로벤조일우레아
    g) N-3,5-디클로로-4-(3,4,5-트리클로로-1-피라졸일)페닐-N´-2-클로로벤조 일우레아
    h) N-3,5-디클로로-4-(4,5-디클로로-3-트리플루오로메틸-1-피라졸일) 페닐-N´-2-플루오로벤조일우레아
    i) N-3,5-디클로로-4-[3-(4-브로모페닐)-1-피라졸일]페닐-N´-2-플루오로벤조 일우레아
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870002415A 1986-03-18 1987-03-16 페닐우레아 및 그 제조방법 KR910000042B1 (ko)

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DE3712934A1 (de) * 1987-04-16 1988-11-03 Bayer Ag Substituierte 1-arylpyrazole
DE3715703A1 (de) * 1987-05-12 1988-11-24 Bayer Ag 1-aryl-3-halogenalkyl-4-halogen-pyrazole
DE3927483A1 (de) * 1989-08-19 1991-02-21 Boehringer Ingelheim Kg Neue substituierte heterocyclische fuenfringe, ihre herstellung und verwendung
JP2002516909A (ja) * 1998-06-05 2002-06-11 ベーリンガー インゲルハイム ファーマシューティカルズ インコーポレイテッド 置換１−（４−アミノフェニル）ピラゾール及び抗炎症剤としてのそれらの使用
DE50312261D1 (de) * 2002-07-12 2010-02-04 Sanofi Aventis Deutschland Heterozyklisch substituierte benzoylharnstoffe, verfahren zu ihrer herstellung und ihre verwendung als arzneimittel
DK2672819T3 (en) * 2011-02-07 2018-02-26 Dow Agrosciences Llc PESTICIDE COMPOSITIONS AND PROCEDURES RELATED TO IT
CN107176951A (zh) * 2016-03-11 2017-09-19 恩瑞生物医药科技（上海）有限公司 一种脲类化合物、其制备方法及其医药用途

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EP0242322B1 (en) 1992-12-16
DK134587D0 (da) 1987-03-16
ES2053579T3 (es) 1994-08-01
PT84498B (pt) 1989-11-10
EP0242322A2 (en) 1987-10-21
CN87102145A (zh) 1987-09-30
DK134587A (da) 1987-09-19
EP0242322A3 (en) 1989-03-22
EG18296A (en) 1992-10-30
ZA871996B (en) 1988-10-26
ATE83477T1 (de) 1993-01-15
DE3783070D1 (en) 1993-01-28
NZ219623A (en) 1990-09-26
PT84498A (en) 1987-04-01
CN1017397B (zh) 1992-07-15
AU602884B2 (en) 1990-11-01
JPS62230765A (ja) 1987-10-09
BR8701205A (pt) 1988-01-12
HU203945B (en) 1991-11-28
KR910000042B1 (ko) 1991-01-19
IE60258B1 (en) 1994-06-29
TR23211A (tr) 1989-06-21
GR3007051T3 (ko) 1993-07-30
DE3783070T2 (de) 1993-05-13
SU1491333A3 (ru) 1989-06-30
MY101169A (en) 1991-07-31
AU7004887A (en) 1987-09-24
HUT43941A (en) 1988-01-28
IE870681L (en) 1987-09-18
IL81900A0 (en) 1987-10-20

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