KR840007597A - N-포스포노메틸글리신의 염류의 제법 - Google Patents

N-포스포노메틸글리신의 염류의 제법 Download PDF

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KR840007597A
KR840007597A KR1019830005425A KR830005425A KR840007597A KR 840007597 A KR840007597 A KR 840007597A KR 1019830005425 A KR1019830005425 A KR 1019830005425A KR 830005425 A KR830005425 A KR 830005425A KR 840007597 A KR840007597 A KR 840007597A
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South Korea
Prior art keywords
phosphonomethylglycine
salt
manufacturing
compound
carbon atoms
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KR1019830005425A
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KR900003454B1 (ko
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데이비드 브로오드허스트(외 1) 디카엘
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죤 마일즈 활우퍼
스타우퍼 케리칼 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

내용 없음.

Description

N-포스포노메틸글리신의 염류의 제법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (16)

  1. 하기 구조식,
  3. 의 N-포스포노메탈글리신 화합물과, 구조식(a)
  5. (식중, R1, R2및 R3은 동일하거나 또는 다르며 그리고 1∼4개의 탄소원자를 가진 알킬 그루우프 또는 방향족 알킬 그루우프이고, X는 염화물, 취화물 또는 요오드화물이며, Z는 전자대 또는 산소이다), 또는 구조식(b)
  7. (식중 R1, R2및 R3은 동일하거나 또는 다르며, 그리고 1∼4개의 탄소원자를 가진 알킬 그루우프이고 R4는 1∼12개의 탄소원자를 가진 알킬 그루우프, 방향족 또는 방향족알킬 그루우프이며, X는 염화물, 취화물 요오드화물이고, 그리고 Y는 질소 또는 인이다)을 가진 것들로 구성된 그루우프로부터 선택된 화합물을 물 및 물내에서 불혼합성의 극성유기용제의 존재하에서 구조식(R)3N(식중, R은 동일하거나 또는 다르며, 4∼13개의 탄소원자를 가진 알킬 그루우프이다)의 트리알킬아민의 존재하에, 반응을 완료시키기에 충분한 온도 및 기간동안 반응시킨 후에, (2)상 유리에 의하여 최종생성물을 유리시킴으로써 이루어지는 N-포스포노메틸글리신의 염류의 제법.
  8. 아민은 C8∼C10알킬 그루우프를 가진 것들로 이루어지는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  9. 유기용제는 톨루엔 및 아밀코올의 혼합물로 이루어지는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  10. N-포스포노메틸글리신 및 화합물(a) 또는 (b)는 실질적으로 화학량론 적양으로 존재하는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  11. 알킬아민은 과잉량으로 존재하는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  12. 반응온도는 약 10∼40℃의 범위내의 온도로 유지되는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  13. 반응시간은 약∼4시간의 범위내에서 변동되는 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  14. 화합물(a)은 트리메틸술포늄 클로라이드인 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  15. 화합물(a)은 트리메틸술폭소늄클로라이드인 특허청구의 범위 1기재의 N-포스포노메틸글리신의 염류의 제법.
  16. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019830005425A 1981-01-13 1983-11-15 N-포스포노메틸글리신의 염류의 제법 KR900003454B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US457812 1983-01-13
US06/457,812 US4431594A (en) 1983-01-13 1983-01-13 Method for preparation of salts of N-phosphonomethylglycine

Publications (2)

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KR840007597A true KR840007597A (ko) 1984-12-08
KR900003454B1 KR900003454B1 (ko) 1990-05-19

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KR1019830005425A KR900003454B1 (ko) 1981-01-13 1983-11-15 N-포스포노메틸글리신의 염류의 제법

Country Status (26)

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US (1) US4431594A (ko)
EP (1) EP0117337B1 (ko)
JP (1) JPS59128396A (ko)
KR (1) KR900003454B1 (ko)
AR (1) AR246088A1 (ko)
AT (1) ATE37030T1 (ko)
AU (1) AU562827B2 (ko)
BG (2) BG60165A3 (ko)
BR (1) BR8306690A (ko)
CA (1) CA1213903A (ko)
CS (1) CS235988B2 (ko)
DD (1) DD234273A5 (ko)
DE (1) DE3377913D1 (ko)
DK (1) DK167358B1 (ko)
ES (1) ES8504693A1 (ko)
FI (1) FI80045C (ko)
HU (1) HU193534B (ko)
IL (1) IL70036A (ko)
MX (1) MX158972A (ko)
NO (1) NO169288C (ko)
NZ (1) NZ206020A (ko)
PL (1) PL146421B1 (ko)
PT (1) PT77710B (ko)
RO (1) RO88471A (ko)
YU (1) YU43199B (ko)
ZA (1) ZA838049B (ko)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0376508U (ko) * 1989-11-29 1991-07-31
IL101539A (en) * 1991-04-16 1998-09-24 Monsanto Europe Sa Mono-ammonium salts of the history of N phosphonomethyl glycyl which are not hygroscopes, their preparations and pesticides containing
GB9111974D0 (en) * 1991-06-04 1991-07-24 Ici Plc Novel process
GB9525956D0 (en) * 1995-12-19 1996-02-21 Zeneca Ltd Manufacture of glyphosate salts
AU746589B2 (en) * 1997-07-30 2002-05-02 Monsanto Company Process and compositions promoting biological effectiveness of exogenous chemical substances in plants
EP1135024B1 (en) 1998-11-30 2004-12-29 Flamel Technologies Promoting biological effectiveness of exogenous chemical substances in plants
AUPR682201A0 (en) 2001-08-03 2001-08-30 Nufarm Limited Glyphosate composition
MX2009008934A (es) * 2007-02-26 2009-08-28 Dow Agrosciences Llc Proceso para la preparacion de algunas sulfiliminas sustituidas.
WO2010053385A1 (en) 2008-11-06 2010-05-14 Sn Biotech Technologies Sp. Z O.O. Sp. K. A liquid, homogenous herbicide composition, a method of weed control, a method of production of liquid, homogenous herbicide composition and use of a liquid, homogenous herbicide composition for weed control

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2271707A (en) * 1937-06-24 1942-02-03 Gen Aniline & Film Corp Wetting agent
US2831019A (en) * 1956-07-27 1958-04-15 California Ink Company Inc Method of preparing quaternary ammonium naphthenates
US4196143A (en) * 1974-07-01 1980-04-01 The Dow Chemical Company Substituted phenoxyalkyl quaternary ammonium compounds
ES465139A1 (es) * 1976-12-20 1978-10-01 Monsanto Co Un procedimiento para preparar una mono-o disal de n-fosfo- nometilglicina.
US4340761A (en) * 1980-11-24 1982-07-20 The Dow Chemical Company Preparation of phosphonium phenoxide salts
US4315765A (en) * 1980-12-04 1982-02-16 Stauffer Chemical Company Trialkylsulfonium salts of n-phosphonomethylglycine and their use as plant growth regulators and herbicides
US4341549A (en) * 1981-08-24 1982-07-27 Stauffer Chemical Company Phosphonium salts of N-phosphonomethylglycine and their use as herbicides and plant growth regulants

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Publication number Publication date
DK491083A (da) 1984-07-14
ATE37030T1 (de) 1988-09-15
EP0117337B1 (en) 1988-09-07
CS235988B2 (en) 1985-05-15
RO88471A (ro) 1986-07-30
JPS59128396A (ja) 1984-07-24
NO169288B (no) 1992-02-24
FI833872A (fi) 1984-07-14
NO169288C (no) 1992-06-03
NO833828L (no) 1984-07-16
IL70036A0 (en) 1984-01-31
BG60165A3 (en) 1993-11-15
AU562827B2 (en) 1987-06-18
NZ206020A (en) 1986-07-11
JPH0225918B2 (ko) 1990-06-06
PL244495A1 (en) 1984-10-08
IL70036A (en) 1987-01-30
FI80045B (fi) 1989-12-29
PL146421B1 (en) 1989-02-28
DK491083D0 (da) 1983-10-26
DE3377913D1 (en) 1988-10-13
AU2058783A (en) 1984-07-19
MX158972A (es) 1989-04-04
KR900003454B1 (ko) 1990-05-19
PT77710B (en) 1986-03-27
DK167358B1 (da) 1993-10-18
AR246088A1 (es) 1994-03-30
US4431594A (en) 1984-02-14
ES526880A0 (es) 1985-05-01
HU193534B (en) 1987-10-28
DD234273A5 (de) 1986-03-26
EP0117337A1 (en) 1984-09-05
BR8306690A (pt) 1984-07-31
ZA838049B (en) 1984-09-26
PT77710A (en) 1983-12-01
YU43199B (en) 1989-04-30
FI80045C (fi) 1990-04-10
CA1213903A (en) 1986-11-12
ES8504693A1 (es) 1985-05-01
YU229983A (en) 1986-04-30
FI833872A0 (fi) 1983-10-24
BG60103A3 (en) 1993-10-15

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