KR20220052990A - 식물성 오일로부터 미세유체 추출 방법 - Google Patents
식물성 오일로부터 미세유체 추출 방법 Download PDFInfo
- Publication number
- KR20220052990A KR20220052990A KR1020227010039A KR20227010039A KR20220052990A KR 20220052990 A KR20220052990 A KR 20220052990A KR 1020227010039 A KR1020227010039 A KR 1020227010039A KR 20227010039 A KR20227010039 A KR 20227010039A KR 20220052990 A KR20220052990 A KR 20220052990A
- Authority
- KR
- South Korea
- Prior art keywords
- extraction
- vegetable oil
- microfluidic chip
- interest
- molecule
- Prior art date
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- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 64
- 239000008158 vegetable oil Substances 0.000 title claims abstract description 64
- 238000000034 method Methods 0.000 title claims abstract description 48
- 238000000605 extraction Methods 0.000 claims abstract description 130
- 239000012530 fluid Substances 0.000 claims abstract description 96
- 239000002904 solvent Substances 0.000 claims abstract description 59
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 238000004891 communication Methods 0.000 claims abstract description 9
- 150000003626 triacylglycerols Chemical class 0.000 claims abstract description 8
- 238000001704 evaporation Methods 0.000 claims abstract description 5
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims abstract description 3
- 238000000926 separation method Methods 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 3
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 2
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 claims description 2
- 238000004987 plasma desorption mass spectroscopy Methods 0.000 claims description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 229920005992 thermoplastic resin Polymers 0.000 claims description 2
- 239000003921 oil Substances 0.000 description 30
- 235000019198 oils Nutrition 0.000 description 30
- 238000000199 molecular distillation Methods 0.000 description 27
- 238000004128 high performance liquid chromatography Methods 0.000 description 14
- 239000010635 coffee oil Substances 0.000 description 13
- 239000000284 extract Substances 0.000 description 11
- 240000005481 Salvia hispanica Species 0.000 description 9
- 235000001498 Salvia hispanica Nutrition 0.000 description 9
- 239000000469 ethanolic extract Substances 0.000 description 9
- 238000000622 liquid--liquid extraction Methods 0.000 description 9
- 238000000638 solvent extraction Methods 0.000 description 9
- 235000012377 Salvia columbariae var. columbariae Nutrition 0.000 description 8
- 239000004480 active ingredient Substances 0.000 description 8
- 235000014167 chia Nutrition 0.000 description 8
- 239000002537 cosmetic Substances 0.000 description 8
- 238000010586 diagram Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 4
- 239000010779 crude oil Substances 0.000 description 4
- 238000009792 diffusion process Methods 0.000 description 4
- 238000000746 purification Methods 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 125000004494 ethyl ester group Chemical group 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 235000021588 free fatty acids Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000010908 decantation Methods 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 229930004069 diterpene Natural products 0.000 description 2
- 150000004141 diterpene derivatives Chemical class 0.000 description 2
- 230000009977 dual effect Effects 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- QNRATNLHPGXHMA-XZHTYLCXSA-N (r)-(6-ethoxyquinolin-4-yl)-[(2s,4s,5r)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]methanol;hydrochloride Chemical compound Cl.C([C@H]([C@H](C1)CC)C2)CN1[C@@H]2[C@H](O)C1=CC=NC2=CC=C(OCC)C=C21 QNRATNLHPGXHMA-XZHTYLCXSA-N 0.000 description 1
- 241000723377 Coffea Species 0.000 description 1
- 235000007460 Coffea arabica Nutrition 0.000 description 1
- 240000007154 Coffea arabica Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000020235 chia seed Nutrition 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 244000013123 dwarf bean Species 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000021331 green beans Nutrition 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229930013686 lignan Natural products 0.000 description 1
- 150000005692 lignans Chemical class 0.000 description 1
- 235000009408 lignans Nutrition 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- -1 phytosterols Chemical class 0.000 description 1
- 229940068065 phytosterols Drugs 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 150000003421 squalenes Chemical class 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0496—Solvent extraction of solutions which are liquid by extraction in microfluidic devices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/46—Coffee flavour; Coffee oil; Flavouring of coffee or coffee extract
- A23F5/48—Isolation or recuperation of coffee flavour or coffee oil
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0484—Controlling means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/006—Refining fats or fatty oils by extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Health & Medical Sciences (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Extraction Or Liquid Replacement (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP19306206.4A EP3797846B1 (fr) | 2019-09-26 | 2019-09-26 | Extraction microfluidique a partir d'extrait vegetal |
| EP19306206.4 | 2019-09-26 | ||
| PCT/EP2020/077011 WO2021058806A1 (fr) | 2019-09-26 | 2020-09-25 | Extraction microfluidique à partir d'huile végétale |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20220052990A true KR20220052990A (ko) | 2022-04-28 |
Family
ID=68281350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020227010039A KR20220052990A (ko) | 2019-09-26 | 2020-09-25 | 식물성 오일로부터 미세유체 추출 방법 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20220395766A1 (ja) |
| EP (2) | EP3797846B1 (ja) |
| JP (1) | JP7399273B2 (ja) |
| KR (1) | KR20220052990A (ja) |
| CN (1) | CN114450077A (ja) |
| ES (1) | ES2981103T3 (ja) |
| WO (1) | WO2021058806A1 (ja) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113588558B (zh) * | 2021-08-09 | 2024-01-19 | 中国石油大学(华东) | 一种原油快速定量表征的在线式光谱检测系统及其方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK0790849T3 (da) * | 1994-10-22 | 2003-07-21 | Central Research Lab Ltd | Fremgangsmåde og apparat til diffusionsoverførsel mellem ikke-blandbare væsker |
| SE504664C2 (sv) * | 1995-09-22 | 1997-03-24 | Scotia Lipidteknik Ab | Sätt att framställa fraktionerad olja, oljan, dess användning samt emulsionskomposition innehållande oljan |
| JP4470402B2 (ja) | 2002-07-12 | 2010-06-02 | 東ソー株式会社 | 微小流路構造体及びそれを用いた流体の化学操作方法 |
| JP4517381B2 (ja) | 2003-08-04 | 2010-08-04 | 曽田香料株式会社 | チエノピリジン系化合物の香料における使用、および新規チエノピリジン系化合物 |
| JP4765373B2 (ja) | 2005-03-31 | 2011-09-07 | 栗田工業株式会社 | フッ素含有排水の処理方法及び処理装置 |
| EP2366450A4 (en) | 2008-11-26 | 2016-03-23 | Sumitomo Bakelite Co | MICRO CHANNEL DEVICE |
| AU2010221833C1 (en) * | 2009-03-11 | 2015-09-24 | Swedish Oat Fiber Ab | Method for separating neutral and polar lipids and an oil rich in polar lipids |
| JP2011032217A (ja) | 2009-08-03 | 2011-02-17 | Morishita Jintan Co Ltd | 脂肪吸収抑制剤 |
| JP6026785B2 (ja) | 2011-10-31 | 2016-11-16 | 富士フイルム株式会社 | 水性組成物 |
| KR102411228B1 (ko) | 2014-06-27 | 2022-06-20 | 소시에떼 데 프로듀이 네슬레 소시에떼아노님 | 커피 음료 조성물 및 그를 생성하는 방법 |
| WO2017096414A1 (en) * | 2015-12-07 | 2017-06-15 | University Of South Australia | Microfluidic chips and uses thereof |
| FR3049472B1 (fr) * | 2016-03-31 | 2021-05-21 | Oleon N V | Procede d'extraction de glycolipides et glycolipides obtenus |
| CN206372553U (zh) * | 2016-12-15 | 2017-08-04 | 贵州维仙果有限公司 | 基于微流体的快速萃取装置 |
| CN206372554U (zh) * | 2016-12-15 | 2017-08-04 | 贵州维仙果有限公司 | 能直接显示结果的微流体快速萃取装置 |
| CN109856278B (zh) * | 2019-02-01 | 2022-01-04 | 广东药科大学 | 一种基于三相层流微流控芯片的筛选中药活性成分的方法 |
-
2019
- 2019-09-26 ES ES19306206T patent/ES2981103T3/es active Active
- 2019-09-26 EP EP19306206.4A patent/EP3797846B1/fr active Active
-
2020
- 2020-09-25 WO PCT/EP2020/077011 patent/WO2021058806A1/fr unknown
- 2020-09-25 EP EP20775365.8A patent/EP4034275A1/fr active Pending
- 2020-09-25 KR KR1020227010039A patent/KR20220052990A/ko not_active Application Discontinuation
- 2020-09-25 CN CN202080066821.9A patent/CN114450077A/zh active Pending
- 2020-09-25 JP JP2022519298A patent/JP7399273B2/ja active Active
- 2020-09-25 US US17/642,851 patent/US20220395766A1/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| EP3797846B1 (fr) | 2024-05-22 |
| US20220395766A1 (en) | 2022-12-15 |
| EP3797846A1 (fr) | 2021-03-31 |
| ES2981103T3 (es) | 2024-10-07 |
| JP7399273B2 (ja) | 2023-12-15 |
| WO2021058806A1 (fr) | 2021-04-01 |
| JP2022550101A (ja) | 2022-11-30 |
| EP4034275A1 (fr) | 2022-08-03 |
| CN114450077A (zh) | 2022-05-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E902 | Notification of reason for refusal |