KR20220030029A - Manufacturing Method of Cosmetic Composition for Improving Acne Containing Wild Ginseng essential oil - Google Patents
Manufacturing Method of Cosmetic Composition for Improving Acne Containing Wild Ginseng essential oil Download PDFInfo
- Publication number
- KR20220030029A KR20220030029A KR1020200111719A KR20200111719A KR20220030029A KR 20220030029 A KR20220030029 A KR 20220030029A KR 1020200111719 A KR1020200111719 A KR 1020200111719A KR 20200111719 A KR20200111719 A KR 20200111719A KR 20220030029 A KR20220030029 A KR 20220030029A
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- South Korea
- Prior art keywords
- wild ginseng
- essential oil
- weight
- extract
- cosmetic composition
- Prior art date
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Abstract
Description
본 발명은 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법에 관한 것이다.The present invention relates to a method for preparing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
피부 세포의 분화, 노화 현상의 규명, 인공 세포의 개발 등 피부 과학에 대한 연구가 활발해짐에 따라 이러한 소비 트렌드를 맞추기 위해 향상된 여러 기능성 천연 화장품이 개발되었으며, 미백, 보습, 자외선 차단 및 흡수, 유해 산소 제거, 콜라겐 합성, 주름 방지 등 다양한 효능을 가진 천연 소재에 대한 관심도 증대되고 있다.As research on skin science such as differentiation of skin cells, identification of aging phenomena, and development of artificial cells has become active, various functional natural cosmetics have been developed to meet these consumption trends, whitening, moisturizing, UV protection and absorption, and harmful effects. Interest in natural materials with various effects, such as oxygen removal, collagen synthesis, and anti-wrinkle, is also increasing.
이러한 피부는 각종 오염 물질과 스트레스 등으로 인해 손상을 입게 되며 피부 탄력이 저하되고 수분이 상실되며 주름이 생성될 수 있다. 또한, 피부가 노화되면 진피는 피부의 수분을 유지하기 어렵게 되고 피부는 거칠어지고 피지샘과 땀샘의 기능도 감소한다. 이로 인해 피지막이 적당히 생성되지 못하고 피부 수화에 대한 보호력을 잃게 되어 결국 피부는 건조하게 되며 투명성을 잃게 되어 피부 단백질의 탄력이 감소되고 주름이 생성된다. 그리고피부의 보습력 상실은 피부 노화의 중요한 요인이 되고 있다.Such skin is damaged due to various pollutants and stress, and the skin elasticity is reduced, moisture is lost, and wrinkles can be generated. In addition, as the skin ages, it becomes difficult for the dermis to retain moisture in the skin, the skin becomes rough, and the functions of the sebaceous and sweat glands decrease. Due to this, the sebum film is not properly formed and the protective power against skin hydration is lost, and eventually the skin becomes dry and loses transparency, which reduces the elasticity of the skin protein and creates wrinkles. And the loss of moisture in the skin is an important factor in skin aging.
여기서, 여드름은 사춘기의 남성호르몬 기능 항진으로 인해 피지선의 분비가 왕성해지고 모낭의 상피세포가 이상각화증을 일으켜 모낭이 막히게 되면 이로 인해 여드름의 기본 병변인 면포가 형성되며, 모낭 내에 상주하는 혐기성 피부 상재균인 프로피오니박테리움 아크네가 활발히 증식하여 유리 지방산(free fatty acid)을 생성하고 이것이 모낭을 자극하여 여드름이라는 염증을 유발하는 것으로 알려져 있다. Here, acne is due to the hyperactivity of male hormones during puberty, which leads to active secretion of sebaceous glands and epithelial cells of the hair follicles causing dyskeratosis and clogging of the hair follicles. It is known that the bacterium Propionibacterium acnes actively proliferates to produce free fatty acid, which stimulates hair follicles to cause inflammation called acne.
여드름을 치료 또는 완화시키기 위한 방법으로서는, 피지 과분비 억제를 위해 남성호르몬 억제제인 에스트로겐 등의 여성호르몬을 사용하거나 또는 항균제를 사용하여 왔다.As a method for treating or alleviating acne, a female hormone such as estrogen, which is a male hormone inhibitor, has been used or an antibacterial agent has been used to suppress the hypersecretion of sebum.
그러나 이러한 여성호르몬제를 사용하는 방법은 과다한 피부 염증이 있을 수 있고 부작용이 많이 발생할 수 있다. 이 외에 피지의 배출을 촉진시켜 여드름을 치유할 수는 있으나 각질을 부드럽게 해줄 수 있는 보습제와 알파히드록산(α-hydroxy acid; AHA)은 피부를 필요 이상으로 용해시켜 상처를 남길 수 있으며 피부 자극성 등의 문제를 야기할 수 있다.However, this method of using female hormones may cause excessive skin inflammation and cause many side effects. In addition, although acne can be cured by accelerating the discharge of sebum, a moisturizer that can soften dead skin cells and α-hydroxy acid (AHA) can dissolve the skin more than necessary and leave a wound, and can cause skin irritation, etc. may cause problems with
따라서 본 발명의 목적은 피부의 부작용이 매우 낮으며 산양삼 내 함유된 효소의 활성을 증대시켜 여드름 개선, 피부 재생, 피부 주름 방지, 피부 노화 방지, 피부 염증 개선, 미백 개선을 향상시킬 수 있는 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법을 제공하는 것이다.Therefore, it is an object of the present invention to have very low side effects on the skin and to improve the activity of enzymes contained in wild ginseng to improve acne improvement, skin regeneration, skin wrinkle prevention, skin aging prevention, skin inflammation improvement, and whitening improvement. It is to provide a method for preparing a cosmetic composition for improving acne comprising a.
상기 목적을 달성하기 위한 본 발명에 따른 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법은, 상기 산양삼의 증숙공정, 동결공정, 기화공정 및 상기 기화공정에서 얻어진 기체를 정제 및 회수하는 공정 중 적어도 하나의 공정을 이용하여 산양삼 정유를 획득하는 단계; 상기 산양삼에 당류를 상기 산양삼의 중량대비 15% ~ 240%를 혼합한 후 숙성하여 산양삼 숙성액을 제조하는 단계; 제조된 상기 산양삼 숙성액을 감압 추출하여 산양삼 추출액을 제조하는 단계; 및 상기 산양삼 정유 5 ~ 10중량%, 상기 산양삼 추출액 5 ~ 10중량%을 포함하여 콜라겐, 에탄올, 글리세린 및 정제수를 혼합하는 단계를 포함한다. 산양삼 정유와 산양삼 숙성 및 추출액을 이용하여 화장료 조성물을 제조하므로 여드름 개선, 피부 재생, 피부 주름 방지, 피부 노화 방지, 피부 염증 개선, 미백 개선을 향상시킬 수 있다.According to the present invention for achieving the above object, the method for producing a cosmetic composition for improving acne comprising wild ginseng essential oil is a process of purifying and recovering the gas obtained in the steaming process, freezing process, vaporization process and the vaporization process of wild ginseng. Obtaining wild ginseng essential oil using at least one process of; preparing a matured solution of wild ginseng by mixing 15% to 240% of saccharides with the wild ginseng based on the weight of the wild ginseng and then aging; preparing a wild ginseng extract by extracting the prepared wild ginseng aged liquid under reduced pressure; And 5 to 10% by weight of the wild ginseng essential oil, 5 to 10% by weight of the wild ginseng extract, and mixing collagen, ethanol, glycerin and purified water. Since the cosmetic composition is prepared using wild ginseng essential oil and wild ginseng aging and extract, it can improve acne, skin regeneration, skin wrinkle prevention, skin aging prevention, skin inflammation improvement, and whitening improvement.
여기서, 상기 증숙공정은, 80 ~ 120℃의 스팀을 5 ~ 20 분 동안 처리하고, 상기 동결공정은, -50℃이하에서 4~6시간 동안 진행하며, 상기 기화공정은, -10 ~ 20℃로 유지되며 압력은 -500 mmHg 이하의 진공상태로 유지되는 상태에서 24~96시간 동안 기화를 진행하고, 상기 정제 및 회수하는 공정은 20℃ 이하에서 1~10 시간 동안 수행되면 저온의 진공조건에서 기화(또는 승화)되는 기체에서 정유회수트랩을 이용하여 효율적으로 수분을 제거하고 식물성 정유를 회수할 수 있어 바람직하다.Here, the steaming process is, 80 ~ 120 ℃ steam is treated for 5 to 20 minutes, the freezing process is performed at -50 ℃ or less for 4 to 6 hours, the vaporization process is, -10 ~ 20 ℃ is maintained and the pressure is maintained in a vacuum state of -500 mmHg or less, and vaporization is carried out for 24 to 96 hours, and the purification and recovery process is carried out at 20 ° C. or less for 1 to 10 hours under vacuum conditions at low temperature. It is preferable because it is possible to efficiently remove moisture from the vaporized (or sublimated) gas using an essential oil recovery trap and to recover vegetable essential oil.
그리고 상기 산양삼 숙성액을 제조하는 단계는, 산양삼을 정제수로 세척하여 이물질을 제거하는 단계; 상기 산양삼의 표면에 부착된 물기를 제거하는 단계; 상기 산양삼과 설탕, 꿀, 수크로오스(sucrose), 글루코오스(glucose), 알룰로오스(Allulose), 타가토오스(Tagatose), 물엿, 올리고당, 과당, 포도당 중 적어도 하나를 포함하는 당류를 혼합하는 단계; 상기 산양삼과 당류의 혼합물의 중량대비 Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, Se 중 적어도 하나를 포함하는 미네랄혼합물을 5 ~ 15중량% 혼합하는 단계; 및 미네랄과 당류가 혼합된 산양삼 혼합물을 숙성하는 단계를 포함하면 산양삼 내 함유된 효소의 활성을 증대시켜 피부 재생용, 피부 주름 방지 또는 개선용, 피부 노화 방지 또는 개선용, 피부 염증 개선용 또는 피부 미백 개선용 화장료 조성물을 제공할 수 있어 바람직하다.And the step of preparing the wild ginseng aged liquid, washing the wild ginseng with purified water to remove foreign substances; removing the water attached to the surface of the wild ginseng; Mixing the wild ginseng with sugar, honey, sucrose, glucose, allulose, tagatose, starch syrup, oligosaccharide, fructose, and sugar containing at least one of glucose; 5 to 15% by weight of a mineral mixture containing at least one of Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, and Se based on the weight of the mixture of wild ginseng and saccharides; And when it includes the step of aging the wild ginseng mixture in which minerals and sugars are mixed, by increasing the activity of the enzyme contained in wild ginseng, for skin regeneration, skin wrinkle prevention or improvement, skin aging prevention or improvement, skin inflammation improvement or skin It is preferable to provide a cosmetic composition for improving whitening.
여기서, 상기 산양삼 혼합물을 숙성하는 단계는, 20 ~ 30℃에서 20주 내지 24주 숙성한 후 용출액을 제조하면 산양삼 숙성액이 피부 재생 효과가 최적의 효과에 도달할 수 있어 바람직하다.Here, in the step of aging the wild ginseng mixture, if the extract is prepared after aging for 20 to 24 weeks at 20 to 30° C., it is preferable that the aged wild ginseng liquid can reach an optimal skin regeneration effect.
그리고 상기 산양삼 추출액을 1주 내지 4주 숙성시키는 단계를 더 포함하면 산양삼 숙성액의 항산화 및 미백 효과가 최적이 될 수 있어 바람직하다.And when the step of aging the wild ginseng extract for 1 to 4 weeks is further included, the antioxidant and whitening effects of the aged wild ginseng extract can be optimal, which is preferable.
여기서, 상기 정제수를 혼합하는 단계는, 피부 보호, 피부 진정, 항산화, 주름개선, 피부 자극 완화, 보습 및 미백으로 이루어지는 군 중 적어도 하나의 조성물을 더 포함하여 혼합하면 보습, 미백, 항노화, 피부 조직 개선, 피부 탄력 개선 및 피부 진정 효과를 동시에 구현할 수 있어 바람직하다.Here, the step of mixing the purified water comprises at least one composition from the group consisting of skin protection, skin soothing, antioxidant, wrinkle improvement, skin irritation alleviation, moisturizing and whitening, moisturizing, whitening, anti-aging, skin It is preferable because it can simultaneously implement tissue improvement, skin elasticity improvement, and skin soothing effect.
그리고 상기 선택되는 조성물은, 위치하젤수 5중량%, 동백 오일 5중량%, 올리브오일 1중량%, 산자나무 추출물 5중량%, 오렌지 오일 5중량%, 들깨잎 추출물 5중량%, 접시꽃 추출물 1.5중량%, 삼칠 추출물 5중량%, 캐모마일 추출물0.5중량%, 서양 민들레잎 추출물 0.5중량%, 감초 추출물 0.5중량% 및 병풀 추출물 0.5중량% 중 적어도 하나를 포함하면 천연 재료로부터 추출되어 피부에 대한 부작용 우려가 낮으므로 바람직하다.And the selected composition is, witch hazel water 5% by weight, camellia oil 5% by weight, olive oil 1% by weight, sea buckthorn extract 5% by weight, orange oil 5% by weight, perilla leaf extract 5% by weight, hollyhock extract 1.5% by weight %, 5% by weight of ginseng extract, 0.5% by weight of chamomile extract, 0.5% by weight of western dandelion leaf extract, 0.5% by weight of licorice extract, and 0.5% by weight of Centella asiatica extract is extracted from natural materials, so there is a risk of side effects on the skin It is low, so it is preferable.
여기서, 상기 산양삼 추출액을 제조하는 단계는, 상기 산양삼을 식용알콜에 침지하여 용출시키면 산양삼 주요 성분이 효율적으로 추출될 수 있어 바람직하다. Here, the step of preparing the wild ginseng extract is preferable because the main components of wild ginseng can be efficiently extracted when the wild ginseng is immersed in edible alcohol and eluted.
그리고 상기 산양삼 정유를 획득하는 단계는, 상기 기화 공정을 통해 얻어진 기체에서 정유회수 트랩을 이용하여 수분을 분리하고 정유를 정제 및 회수하며, 정유회수 트랩에 사용되는 물질은 비극성의 식물성 오일, 비극성의 동물성 오일, 극성의 식물성오일 또는 이들 중 적어도 2종 이상을 혼합한 오일이면 저온에서 식물성 정유를 정제 및 회수를 진행하기 때문에 매우 인체 친화적이며 열에 의한 분해 또는 변성을 억제할 수 있어 바람직하다.And in the step of obtaining the essential oil of wild ginseng, water is separated from the gas obtained through the vaporization process using an essential oil recovery trap, and the essential oil is purified and recovered, and the material used for the essential oil recovery trap is a non-polar vegetable oil, a non-polar If it is an animal oil, a polar vegetable oil, or an oil mixed with at least two or more of them, it is very human-friendly because the vegetable essential oil is purified and recovered at a low temperature, and it is preferable because it can suppress decomposition or denaturation by heat.
한편, 상기 목적을 달성하기 위한 본 발명에 따른 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물은, 상기의 방법 중 어느 하나의 방법에 의해 제조된다.On the other hand, the cosmetic composition for improving acne comprising essential oil of wild ginseng according to the present invention for achieving the above object is prepared by any one of the above methods.
본 발명에 따르면 피부의 부작용이 매우 낮으며 산양삼 내 함유된 효소의 활성을 증대시켜 여드름 개선, 피부 재생, 피부 주름 방지, 피부 노화 방지, 피부 염증 개선, 미백 개선을 향상시킬 수 있는 효과가 있다.According to the present invention, the side effects of the skin are very low and the activity of enzymes contained in wild ginseng is increased to improve acne, skin regeneration, skin wrinkle prevention, skin aging prevention, skin inflammation improvement, and whitening improvement.
도 1은 본 발명에 따른 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법의 흐름도.1 is a flowchart of a method for preparing a cosmetic composition for improving acne comprising essential oil of wild ginseng according to the present invention.
이하, 첨부된 도면들을 참조하면서 본 발명의 바람직한 실시 예에 따른 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법을 상세히 설명한다.Hereinafter, a method for preparing a cosmetic composition for improving acne comprising essential oil of wild ginseng according to a preferred embodiment of the present invention will be described in detail with reference to the accompanying drawings.
첫째로, 산양삼의 증숙공정, 동결공정, 기화공정 및 기화공정에서 얻어진 기체를 정제 및 회수하는 공정 중 적어도 하나의 공정을 이용하여 산양삼 정유를 획득한다. First, wild ginseng essential oil is obtained by using at least one of the steaming process, freezing process, vaporization process, and the process of purifying and recovering the gas obtained in the vaporization process of wild ginseng.
여기서, 증숙공정은 80 ~ 120℃의 스팀을 5 ~ 20 분 동안 처리한다.Here, in the steaming process, steam at 80 to 120° C. is treated for 5 to 20 minutes.
동결공정은 -50℃이하에서 4~6시간 동안 진행한다. 이러한 과정에 의해 대상 내부에 함유된 수분이 급속동결된다.The freezing process is carried out at -50°C or lower for 4 to 6 hours. By this process, the moisture contained inside the object is rapidly frozen.
기화공정은 -10 ~ 20℃로 유지되며 압력은 -500 mmHg 이하의 진공상태로 유지되는 상태에서 24 ~ 96시간 동안 기화를 진행한다. 동결한 산양삼은 진공챔버에서 기화 과정이 진행된다. 기화 과정에서 냉동된 수분은 기화되어 다양한 방향성 성분과 함께 대상의 내부로부터 외부로 방출되게 되며, 이러한 기화물은 후단에서 수분 분리와 식물성 정유를 정제 및 회수하기 위하여 정유회수 트랩으로 유입된다.The vaporization process is maintained at -10 ~ 20 ℃ and the pressure is maintained in a vacuum state of -500 mmHg or less, and the vaporization proceeds for 24 ~ 96 hours. Frozen wild ginseng is vaporized in a vacuum chamber. In the vaporization process, the frozen moisture is vaporized and released from the inside of the object to the outside together with various aromatic components, and these vaporized substances are introduced into the essential oil recovery trap in order to separate water and purify and recover vegetable essential oil at the rear end.
정제 및 회수하는 공정은 20℃ 이하에서 1~10 시간 동안 수행되는데 기화 공정을 통해 얻어진 기체에서 정유회수 트랩을 이용하여 수분을 분리하고 정유를 정제 및 회수하며, 정유회수 트랩에 사용되는 물질은 비극성의 식물성 오일(옥수수, 콩, 카놀라, 올리브, 해바라기, 야자, 호두, 땅콩, 아마, 홍화, 포도씨, 아보카도, 헴프씨, 면실유 등), 비극성의 동물성 오일(라드, 우지, 유지방 등), 극성의 식물성오일(마카다미아, 코커넛, 해바라기씨, 피마자, 아몬드 유 등) 또는 이들 중 적어도 2종 이상을 혼합한 오일이다. 이때 사용하는 지질은 항산화제(예로, 비타민E, 셀레늄 등)를 함유하고 있을 수 있다.The purification and recovery process is carried out at 20° C. or lower for 1 to 10 hours. Water is separated from the gas obtained through the vaporization process using an oil recovery trap, and the essential oil is purified and recovered. The material used for the oil recovery trap is non-polar. of vegetable oils (corn, soybean, canola, olive, sunflower, palm, walnut, peanut, flax, safflower, grape seed, avocado, hemp seed, cottonseed oil, etc.), non-polar animal oils (lard, tallow, milk fat, etc.), polar It is vegetable oil (macadamia, coconut, sunflower seed, castor, almond oil, etc.) or a mixture of at least two or more of them. In this case, the lipid used may contain antioxidants (eg, vitamin E, selenium, etc.).
오일을 함유한 비극성트랩에 수분과 정유의 혼합물이 유입되면, 정유성분은 오일에 용해되고, 오일층의 상부로 확산된다. 이때, 후단의 진공펌프에 의해 확산된 수분이 수분회수트랩으로 이동하면, 여기서 수분의 동결이 이루어지면서 회수된다. 상기와 같이 트랩내 함유되는 오일로써 화장품에 일반적으로 사용되는 오일성분을 이용할 경우 별도로 정유성분을 추가적으로 분리할 필요없이 트랩내 오일성분을 그대로 회수하여 화장품의 성분으로 활용할 수 있다. 또한, 순수한 정유성분만을 분리하고자 할 때에는, 기존의 표준적인(혹은 공시된) 분리방법에 의해 트랩용 오일성분으로부터 정유성분을 분리할 수 있다. When a mixture of water and essential oil flows into a non-polar trap containing oil, the essential oil component is dissolved in the oil and diffuses to the upper part of the oil layer. At this time, when the moisture diffused by the vacuum pump at the rear end moves to the moisture recovery trap, the moisture is recovered while being frozen. As described above, when an oil component generally used in cosmetics is used as the oil contained in the trap, the oil component in the trap can be recovered and used as a cosmetic component without the need to additionally separate the essential oil component. In addition, when it is desired to separate only the pure essential oil component, the essential oil component can be separated from the trap oil component by the existing standard (or published) separation method.
상기와 같이 회수한 정유는 분별 증류법을 이용하여 트랩내 함유된 오일과 얻고자하는 식물성 정유를 분리 및 정제한다. 이때, 분별 증류기의 온도는 바람직하게는 40~60℃의 범위이며, 기화된 식물성 정유는 응축기를 통과시킴으로써 회수할 수 있다. 이때의 응축기의 온도는 바람직하게는 0-10℃ 범위이다.The essential oil recovered as described above is separated and purified from the oil contained in the trap and the vegetable essential oil to be obtained by fractional distillation. At this time, the temperature of the fractionator is preferably in the range of 40 to 60 ℃, the vaporized vegetable essential oil can be recovered by passing through the condenser. The temperature of the condenser at this time is preferably in the range of 0-10 °C.
둘째로, 산양삼에 당류를 상기 산양삼의 중량대비 15% ~ 240%를 혼합한 후 숙성하여 산양삼 숙성액을 제조한다. Second, a fermented wild ginseng liquid is prepared by mixing 15% to 240% of saccharides with the wild ginseng based on the weight of the wild ginseng and then aging it.
여기서, 산양삼을 정제수로 세척하여 이물질을 제거하며 산양삼의 표면에 부착된 물기를 제거한다. 세척 및 물기가 제거된 산양삼에 설탕, 꿀, 수크로오스(sucrose), 글루코오스(glucose), 알룰로오스(Allulose), 타가토오스(Tagatose), 물엿, 올리고당, 과당, 포도당 중 적어도 하나를 포함하는 당류를 혼합한다. 산양삼과 당류의 혼합물의 중량대비 Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, Se 중 적어도 하나를 포함하는 미네랄혼합물을 5 ~ 15중량% 혼합한다. 미네랄과 당류가 혼합된 산양삼 혼합물을 20 ~ 30℃에서 20주 내지 24주 숙성한 후 용출액을 제조한다.Here, the wild ginseng is washed with purified water to remove foreign substances and moisture attached to the surface of the wild ginseng is removed. Sugar containing at least one of sugar, honey, sucrose, glucose, allulose, tagatose, starch syrup, oligosaccharide, fructose, and glucose in wild ginseng that has been washed and dried mix 5 to 15% by weight of a mineral mixture containing at least one of Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, and Se based on the weight of the mixture of wild ginseng and saccharides is mixed. A mixture of wild ginseng mixed with minerals and sugars is aged at 20 to 30° C. for 20 to 24 weeks, and then an eluate is prepared.
여기서, 당의 함량은 70 초과일 경우 용출효과는 다소 용이할 수 있으나 도리어 엔자임의 활성을 저하시켜 최적의 조건보다 효능이 낮게 나오는 경향이 있으며 반면 15 미만의 경우에는 미생물에 오염되어 발효되거나 부패가 발생된다. 당과 미네랄의 비율은 효능결과에서 볼 수 있듯이 산양삼의 활성엔자임이 동일하지 않다는 전제하에 비율에 따른 적용실험 결과, 산양삼의 경우 미네랄 함량이 더 높을 때, 전반적인 효능이 보다 우수하게 확인되는 것을 알 수 있었다. 이에 미네랄의 비율은 적용되는 당류 대비 0.1%이하의 경우에는 숙성과정에서 엔자임의 활성에 거의 영향력을 나타내지 못하며, 50%이상의 과량일 경우 역시도 숙성이 원활하지 못해, 효능 및 화장품 제형으로의 응용에 원활하지 못하는 역효과를 나타낸다.Here, if the sugar content is more than 70, the dissolution effect may be somewhat easy, but on the contrary, it lowers the activity of the enzyme and thus the efficacy is lower than the optimal condition. do. As can be seen from the efficacy results, as can be seen from the efficacy results, as a result of the application test according to the ratio under the premise that the active enzymes of wild ginseng are not the same, in the case of wild ginseng, it can be seen that the overall efficacy is better confirmed when the mineral content is higher. there was. Therefore, if the ratio of minerals is less than 0.1% compared to the applied sugar, it has little effect on enzyme activity during the aging process, and if it is in excess of 50%, aging is also not smooth, so it is smooth for efficacy and application to cosmetic formulations. It has the adverse effect of not being able to.
여기서, 숙성기간이 20주 미만인 경우, 숙성기간이 지나치게 짧아 산양삼 숙성액에서 효소 및 파이토뉴트리언트(phytonutrient)성분의 용출이 적어 피부 재생 효과가 나타나지 않았고, 숙성기간이 24주를 초과하면, 피부 재생 효과의 증가폭이 미미해지는 것을 확인할 수 있었다. 즉, 본 발명의 산양삼 숙성액이 최적의 효과에 도달하는 시점은 20 내지 24주라 할 수 있고, 숙성과정에서의 균에 의한 오염이 없었기 때문에, 24주를 초과하여 숙성하더라도 산양삼 숙성액이 변질되는 문제는 없음을 확인할 수 있었다. 다만, 24주를 초과할 경우 효소 및 파이토뉴트리언트(phytonutrient)성분의 수득율이 둔화되므로 이는 경제적으로 비효율적이다.Here, when the aging period is less than 20 weeks, the aging period is too short and the elution of enzymes and phytonutrients from the aged wild ginseng liquid is small, so that the skin regeneration effect does not appear, and when the aging period exceeds 24 weeks, the skin regeneration It was confirmed that the increase in the effect was insignificant. That is, the time point at which the mature wild ginseng liquid of the present invention reaches the optimal effect can be said to be 20 to 24 weeks, and since there was no contamination by bacteria during the aging process, the aged wild ginseng liquid deteriorates even if it is aged for more than 24 weeks. It was confirmed that there were no problems. However, if it exceeds 24 weeks, it is economically inefficient because the yield of enzymes and phytonutrients is slowed.
또한, 숙성기간이 20 내지 24주 일 때, 산양삼 숙성액의 항산화 및 주름개선 효과가 가장 우수하게 나타난다. 숙성기간이 24주를 초과하면 숙성기간의 증가대비 산양삼 숙성 용출액의 수득률이 크게 증가되지 않지 않으며, 산양삼 숙성액의 항산화 및 주름개선 효과가 향상되는 정도가 미미하다. 숙성단계는 20 내지 40℃의 온도에서 수행되는 것이 바람직하며, 20 내지 40℃의 온도일 때 산양삼의 효소 및 파이토뉴트리언트(phytonutrient) 성분이 변질되거나 파괴되지 않으면서 생성 및 용출되어 산양삼 숙성액의 항산화 및 주름개선 효과가 가장 우수하다. In addition, when the aging period is 20 to 24 weeks, the antioxidant and anti-wrinkle effects of the aged wild ginseng liquid are most excellent. When the aging period exceeds 24 weeks, the yield of the aged wild ginseng extract does not increase significantly compared to the increase in the aging period, and the degree of improvement in the antioxidant and wrinkle improvement effects of the aged wild ginseng liquid is insignificant. The aging step is preferably performed at a temperature of 20 to 40 ℃, and when the temperature is 20 to 40 ℃, the enzyme and phytonutrient components of wild ginseng are generated and eluted without being altered or destroyed, so that It has the best antioxidant and anti-wrinkle effects.
셋째로, 제조된 상기 산양삼 숙성액을 감압 추출하여 산양삼 추출액을 제조한다. 가압여과기 또는 감압여과기를 사용하여 수행할 수 있으며 산양삼 추출액을 1주 내지 4주 숙성시킬 수 있고 밀폐용기에서 수행하는 것이 좋다. 1주 미만으로 숙성하면 숙성이 제대로 진행되지 않아 산양삼 숙성액의 항산화 및 미백 효과가 미미하며, 4주를 초과하여 숙성하면, 과도한 숙성으로 인해 산양삼 숙성액의 항산화 및 미백 효과가 감소하는 문제가 있다. 여기서, 산양삼을 식용알콜에 침지하여 용출시킬 수도 있다. 이에 의해 보다 빠르게 추출액을 획득할 수 있다.Third, the prepared wild ginseng aged liquid is extracted under reduced pressure to prepare a wild ginseng extract. It can be carried out using a pressure filter or a reduced pressure filter, and the wild ginseng extract can be aged for 1 to 4 weeks, and it is preferable to perform it in an airtight container. If it is aged for less than 1 week, the antioxidative and whitening effect of the aged wild ginseng liquid is insignificant because aging does not proceed properly. . Here, wild ginseng may be eluted by immersing it in edible alcohol. Thereby, it is possible to obtain an extract more quickly.
넷째로, 산양삼 정유 5 ~ 10중량%, 상기 산양삼 추출액 5 ~ 10중량%을 포함하여 콜라겐, 에탄올, 글리세린 및 정제수를 혼합한다. 여기서 혼합하는 과정은 고속 균질기를 이용하여 모든 성분들이 균일하며 균질하게 혼합되도록 한다.Fourth, 5 to 10% by weight of wild ginseng essential oil and 5 to 10% by weight of the wild ginseng extract are mixed with collagen, ethanol, glycerin and purified water. The mixing process uses a high-speed homogenizer so that all components are uniformly and homogeneously mixed.
여기서, 피부 보호, 피부 진정, 항산화, 주름개선, 피부 자극 완화, 보습 및 미백으로 이루어지는 군 중 적어도 하나의 조성물을 더 포함하여 혼합할 수 있다. 이에 의해 보습, 미백, 항노화, 피부 조직 개선, 피부 탄력 개선 및 피부 진정 효과를 동시에 구현할 수 있다. 적어도 하나는 위치하젤수 5중량%, 동백 오일 5중량%, 올리브오일 1중량%, 산자나무 추출물 5중량%, 오렌지 오일 5중량%, 들깨잎 추출물 5중량%, 접시꽃 추출물 1.5중량%, 삼칠 추출물 5중량%, 캐모마일 추출물0.5중량%, 서양 민들레잎 추출물 0.5중량%, 감초 추출물 0.5중량% 및 병풀 추출물 0.5중량% 중 적어도 하나를 포함할 수 있다.Here, at least one composition from the group consisting of skin protection, skin soothing, antioxidant, wrinkle improvement, skin irritation alleviation, moisturizing and whitening may be further included and mixed. Thereby, moisturizing, whitening, anti-aging, skin tissue improvement, skin elasticity improvement, and skin soothing effects can be realized at the same time. At least one is witch hazel water 5% by weight, camellia oil 5% by weight, olive oil 1% by weight, sea buckthorn extract 5% by weight, orange oil 5% by weight, perilla leaf extract 5% by weight, hollyhock flower extract 1.5% by weight, ginseng extract 5% by weight, 0.5% by weight of chamomile extract, 0.5% by weight of western dandelion leaf extract, 0.5% by weight of licorice extract, and 0.5% by weight of Centella asiatica extract may include at least one.
여기서, 위치하젤수는 위치하젤 잎(Hamamelis Virginiana(Witch Hazel) Leaf)을 열수 추출하여 수득하였다. 위치하젤은 아열대에 서식하는 낙엽수의 일종으로 우리말로는 풍년화라고 하는 나무의 잎으로부터 추출된 것으로 모공축소, 피부보습 및 진정 성분으로 사용된다. 산자나무 추출물은 산자나무 잎과 산자나무 열매의 유효성분을 각각 추출한 추출물로 이루어진다. 산자나무 추출물은 50% 에탄올로 추출한 산자나무 잎 추출물, 70% 에탄올로 추출한 산자나무 잎 추출물, 그리고 열수 추출한 산자나무 열매 추출물을 혼합하는 것이 바람직하며, 산자나무의 우수한 보습 활성을 얻기 위하여 상기 산자나무 잎은 건조시켜 잘게 잘라 삼각플라스크에 넣고, 70% 에탄올을 첨가한 후 상온에서 24시간 동안 침적 후 여과하여 추출하는 에탄올 추출 방법을 이용할 수 있다.Here, witch hazel water was obtained by hot water extraction of witch hazel leaves (Hamamelis Virginiana (Witch Hazel) Leaf). Witch hazel is a kind of deciduous tree that lives in the subtropics. It is extracted from the leaves of a tree called Pungnyunhwa in Korean, and is used as a pore-reducing, skin moisturizing and soothing ingredient. Sea buckthorn extract is composed of extracts obtained by extracting active ingredients from the leaves of the sea buckthorn tree and the fruit of the sea buckthorn, respectively. It is preferable that the sea buckthorn extract is mixed with a sea buckthorn leaf extract extracted with 50% ethanol, a sea buckthorn leaf extract extracted with 70% ethanol, and a sea buckthorn fruit extract extracted with hot water. The leaves are dried, cut into small pieces, put in an Erlenmeyer flask, and 70% ethanol is added thereto, immersed at room temperature for 24 hours, then filtered and extracted using an ethanol extraction method.
추출에 사용하기 위한 식물 재료를 물로 세척하여 이물질을 제거한 후 그늘에서 건조하고 각각 분쇄한다. 분쇄된 각각의 식물 재료의 분말에 적당한 양의 용매를 첨가하여 완전히 침지되도록 한다. 각각의 식물 재료의 분말 분말은 통상의 추출용매를 이용하여 추출할 수 있으며, 바람직하게는, (a)탄소수 1~4의 무수 또는 함수 저급 알코올(예: 메탄올, 에탄올, 프로판올, 부탄올, 노말-프로판올, 이소-프로판올 및 노말-부탄올 등), (b)상기 저급 알코올과 물과의 혼합용매, (c)아세톤, (d)에틸 아세테이트, (e)클로로포름, (f)1,3-부틸렌글리콜, (g) 헥산, (h)디에틸에테르, (i)부틸아세테이트 또는 (j)물을 이용하여 추출할 수 있으나, 에탄올, 메탄올, 부탄올, 프로판올, 부틸렌글리콜, 프로필렌글리콜, 클로로포름, 에틸아세테이트, 디클로로메탄, 핵산, 페트로레움에테르 또는 디에틸에테르를 사용할 수 있다.The plant material used for extraction is washed with water to remove foreign substances, dried in the shade, and each crushed. An appropriate amount of solvent is added to the powder of each pulverized plant material to ensure complete immersion. Powder powder of each plant material can be extracted using a common extraction solvent, preferably, (a) anhydrous or water-containing lower alcohols having 1 to 4 carbon atoms (e.g., methanol, ethanol, propanol, butanol, normal- propanol, iso-propanol and normal-butanol), (b) a mixed solvent of the lower alcohol and water, (c) acetone, (d) ethyl acetate, (e) chloroform, (f) 1,3-butylene It can be extracted using glycol, (g) hexane, (h) diethyl ether, (i) butyl acetate or (j) water, but ethanol, methanol, butanol, propanol, butylene glycol, propylene glycol, chloroform, ethyl Acetate, dichloromethane, nucleic acid, petroleum ether or diethyl ether can be used.
상기의 방법을 이용하여 산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물을 제조할 수 있다.By using the above method, it is possible to prepare a cosmetic composition for improving acne comprising essential oil of wild ginseng.
화장료 조성물은 미스트 조성물은 추가로 지방 물질, 유기 용매, 용해제, 농축제 및 겔화제, 연화제, 항산화제, 현탁화제, 안정화제, 발포제(foaming agent), 방향제, 계면활성제, 물, 이온형 또는 비이온형 유화제, 충전제, 금속이온 봉쇄제 및 킬레이트화제, 보존제, 비타민, 차단제, 습윤화제, 필수 오일, 염료, 안료, 친수성 또는 친유성활성제, 지질 소낭 등의 보조제를 포함할 수 있다.The cosmetic composition may include a mist composition, in addition to a fatty substance, an organic solvent, a solubilizing agent, a thickening agent and a gelling agent, an emollient, an antioxidant, a suspending agent, a stabilizer, a foaming agent, a fragrance, a surfactant, water, an ionic or non-toxic agent. adjuvants such as ionic emulsifiers, fillers, sequestering and chelating agents, preservatives, vitamins, blocking agents, wetting agents, essential oils, dyes, pigments, hydrophilic or lipophilic active agents, lipid vesicles and the like.
이 외의 각종 식물의 추출물을 포함할 수 있으며, 삭기의 식물성 정유는 β-panasinsene, cyclopropeazulene, spathulenol, alloaromadendrene, *?*-selinene, isopropyllidene, isospathulenol 등이 함유될 수 있다.It may contain extracts of various other plants, and the vegetable essential oil of Sakgi may contain β-panasinsene, cyclopropeazulene, spathulenol, alloaromadendrene, *?*-selinene, isopropyllidene, isospathulenol, and the like.
또한, 식물성 정유는 신양삼을 비롯한 인삼, 참깻잎, 당귀잎, 고삼, 창포, 또는 감초를 더 포함할 수 있으며, 오미자, 라벤더 등의 여드름에 효과가 있는 식물을 증숙, 동결, 기화 및 정화. 회수하여 활용할 수도 있다.In addition, the vegetable essential oil may further include ginseng, sesame leaf, angelica leaf, ginseng, iris, or licorice, including Shinyangsam, and steam, freeze, vaporize and purify plants that are effective against acne, such as omija and lavender. It can be retrieved and used.
Claims (10)
상기 산양삼의 증숙공정, 동결공정, 기화공정 및 상기 기화공정에서 얻어진 기체를 정제 및 회수하는 공정 중 적어도 하나의 공정을 이용하여 산양삼 정유를 획득하는 단계;
상기 산양삼에 당류를 상기 산양삼의 중량대비 15% ~ 240%를 혼합한 후 숙성하여 산양삼 숙성액을 제조하는 단계;
제조된 상기 산양삼 숙성액을 감압 추출하여 산양삼 추출액을 제조하는 단계; 및
상기 산양삼 정유 5 ~ 10중량%, 상기 산양삼 추출액 5 ~ 10중량%을 포함하여 콜라겐, 에탄올, 글리세린 및 정제수를 혼합하는 단계를 포함하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
In the method for preparing a cosmetic composition for improving acne comprising essential oil of wild ginseng,
obtaining wild ginseng essential oil by using at least one of a process for purifying and recovering the gas obtained in the steaming process, freezing process, vaporization process and the vaporization process of wild ginseng;
preparing a matured solution of wild ginseng by mixing 15% to 240% of saccharides with the wild ginseng based on the weight of the wild ginseng and then aging;
preparing a wild ginseng extract by extracting the prepared wild ginseng aged liquid under reduced pressure; and
5 to 10% by weight of the wild ginseng essential oil, 5 to 10% by weight of the wild ginseng extract comprising the step of mixing collagen, ethanol, glycerin and purified water,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 증숙공정은, 80 ~ 120℃의 스팀을 5 ~ 20 분 동안 처리하고,
상기 동결공정은, -50℃이하에서 4~6시간 동안 진행하며,
상기 기화공정은, -10 ~ 20℃로 유지되며 압력은 -500 mmHg 이하의 진공상태로 유지되는 상태에서 24~96시간 동안 기화를 진행하고,
상기 정제 및 회수하는 공정은 20℃ 이하에서 1~10 시간 동안 수행되는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
The steaming process, 80 ~ 120 ℃ steam for 5 ~ 20 minutes,
The freezing process is carried out at -50 ° C. or lower for 4 to 6 hours,
The vaporization process is maintained at -10 to 20 ℃ and the pressure is maintained in a vacuum state of -500 mmHg or less, and the vaporization proceeds for 24 to 96 hours,
The purification and recovery process is carried out at 20 ° C. or less for 1 to 10 hours,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 산양삼 숙성액을 제조하는 단계는,
산양삼을 정제수로 세척하여 이물질을 제거하는 단계;
상기 산양삼의 표면에 부착된 물기를 제거하는 단계;
상기 산양삼과 설탕, 꿀, 수크로오스(sucrose), 글루코오스(glucose), 알룰로오스(Allulose), 타가토오스(Tagatose), 물엿, 올리고당, 과당, 포도당 중 적어도 하나를 포함하는 당류를 혼합하는 단계;
상기 산양삼과 당류의 혼합물의 중량대비 Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, Se 중 적어도 하나를 포함하는 미네랄혼합물을 5 ~ 15중량% 혼합하는 단계; 및
미네랄과 당류가 혼합된 산양삼 혼합물을 숙성하는 단계를 포함하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
The step of preparing the aged wild ginseng liquid,
Washing wild ginseng with purified water to remove foreign substances;
removing the water attached to the surface of the wild ginseng;
Mixing the wild ginseng with sugar, honey, sucrose, glucose, allulose, tagatose, starch syrup, oligosaccharide, fructose, and sugar containing at least one of glucose;
5 to 15% by weight of a mineral mixture containing at least one of Ca, Mg, Cu, Zn, Na, K, Fe, P, Cl, Ge, Pt, and Se based on the weight of the mixture of wild ginseng and saccharides; and
Including the step of aging a mixture of wild ginseng in which minerals and sugars are mixed,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 산양삼 혼합물을 숙성하는 단계는,
20 ~ 30℃에서 20주 내지 24주 숙성한 후 용출액을 제조하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
4. The method of claim 3,
The step of aging the wild ginseng mixture,
After 20 to 24 weeks of aging at 20 ~ 30 ℃ to prepare an eluate,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 산양삼 추출액을 1주 내지 4주 숙성시키는 단계를 더 포함하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
Further comprising the step of aging the wild ginseng extract for 1 to 4 weeks,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 정제수를 혼합하는 단계는,
피부 보호, 피부 진정, 항산화, 주름개선, 피부 자극 완화, 보습 및 미백으로 이루어지는 군 중 적어도 하나의 조성물을 더 포함하여 혼합하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
The step of mixing the purified water,
Mixing by further including at least one composition from the group consisting of skin protection, skin soothing, antioxidant, wrinkle improvement, skin irritation relief, moisturizing and whitening,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 적어도 하나는,
위치하젤수 5중량%, 동백 오일 5중량%, 올리브오일 1중량%, 산자나무 추출물 5중량%, 오렌지 오일 5중량%, 들깨잎 추출물 5중량%, 접시꽃 추출물 1.5중량%, 삼칠 추출물 5중량%, 캐모마일 추출물0.5중량%, 서양 민들레잎 추출물 0.5중량%, 감초 추출물 0.5중량% 및 병풀 추출물 0.5중량% 중 적어도 하나를 포함하는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
7. The method of claim 6,
said at least one,
Witch hazel water 5% by weight, camellia oil 5% by weight, olive oil 1% by weight, sea buckthorn extract 5% by weight, orange oil 5% by weight, perilla leaf extract 5% by weight, hollyhock extract 1.5% by weight, ginseng extract 5% by weight , Containing at least one of 0.5% by weight of chamomile extract, 0.5% by weight of western dandelion leaf extract, 0.5% by weight of licorice extract and 0.5% by weight of Centella asiatica extract,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 산양삼 추출액을 제조하는 단계는,
상기 산양삼을 식용알콜에 침지하여 용출시키는,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
The step of preparing the wild ginseng extract,
Elution by immersing the wild ginseng in edible alcohol,
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
상기 산양삼 정유를 획득하는 단계는,
상기 기화 공정을 통해 얻어진 기체에서 정유회수 트랩을 이용하여 수분을 분리하고 정유를 정제 및 회수하며,
정유회수 트랩에 사용되는 물질은 비극성의 식물성 오일, 비극성의 동물성 오일, 극성의 식물성오일 또는 이들 중 적어도 2종 이상을 혼합한 오일인,
산양삼 정유를 포함하는 여드름 개선을 위한 화장료 조성물의 제조방법.
According to claim 1,
The step of obtaining the essential oil of wild ginseng is,
Separating moisture from the gas obtained through the vaporization process using an essential oil recovery trap, and purifying and recovering essential oil,
The material used for the oil recovery trap is a non-polar vegetable oil, a non-polar animal oil, a polar vegetable oil, or a mixture of at least two of them.
A method of manufacturing a cosmetic composition for improving acne comprising essential oil of wild ginseng.
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KR20190136189A (en) * | 2018-05-30 | 2019-12-10 | 농업회사법인 주식회사 우리두 | Recovering Method of Essential Oil of Plant, Essential Oil Obtained therefrom, and Cosmetic Composition Comprising The Same |
KR20200019303A (en) * | 2018-08-13 | 2020-02-24 | 주식회사 제주볼케이노 | Wood cultivated ginseng Matured solution and manufacturing method |
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Publication number | Priority date | Publication date | Assignee | Title |
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KR20190136189A (en) * | 2018-05-30 | 2019-12-10 | 농업회사법인 주식회사 우리두 | Recovering Method of Essential Oil of Plant, Essential Oil Obtained therefrom, and Cosmetic Composition Comprising The Same |
KR20200019303A (en) * | 2018-08-13 | 2020-02-24 | 주식회사 제주볼케이노 | Wood cultivated ginseng Matured solution and manufacturing method |
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Publication number | Priority date | Publication date | Assignee | Title |
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KR102623104B1 (en) * | 2023-08-23 | 2024-01-11 | 에프아이씨씨주식회사 | A cosmetic composition for skin regeneration and wrinkle improvement containing botulinum toxin conjugates and stem cell exosome complexes as active ingredients, and a method of manufacturing the same |
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