KR20200028819A - The Beauty art-soap of The composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it. - Google Patents

The Beauty art-soap of The composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it. Download PDF

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KR20200028819A
KR20200028819A KR1020190046462A KR20190046462A KR20200028819A KR 20200028819 A KR20200028819 A KR 20200028819A KR 1020190046462 A KR1020190046462 A KR 1020190046462A KR 20190046462 A KR20190046462 A KR 20190046462A KR 20200028819 A KR20200028819 A KR 20200028819A
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weight
soap
oil
mixed
palm
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KR102166300B1 (en
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김관형
김희웅
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김관형
김희웅
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P19/00Drugs for skeletal disorders
    • A61P19/08Drugs for skeletal disorders for bone diseases, e.g. rachitism, Paget's disease
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/02Boiling soap; Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/26Drying
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes

Abstract

The present invention relates to a multifunctional beauty soap composition and a method of manufacturing a multifunctional beauty soap by using the composition. The purpose of the present invention is to provide a multifunctional soap composition which can obtain a hard soap that is not easily swollen or dissolved in water, can prevent various diseases and has effects of preventing and treating various skin diseases by performing a strong antibacterial function, and can delay skin aging by antioxidant synergistic effects due to antioxidant activities; and a method of manufacturing a multifunctional soap by using the composition. The multifunctional beauty soap composition according to the present invention comprises: 86 wt% of a soap base prepared by adding 2 wt% of glycerin to a reactant obtained by reacting caustic acid of a saturated aqueous solution with a vegetable mixed oil obtained by mixing a mixed palm oil with coconut oil at a mixing ratio of 78 : 6, wherein the mixed palm oil is obtained by mixing pulp palm oil obtained from palm pulp of Elaeis guineesis with palm kernels oil obtained from seeds of Elaeis guineesis at the ratio of reducing abrasion of the soap; 1 wt% of peanut oil, olive oil, galactose fermentation liquid, salicylic acid, aloe fermentation liquid, and Opuntia ficus-indica, respectively; 0.5 wt% of soapnut, allantoin, and bamboo salt, respectively; 5.5 wt% of a mixed extraction concentrate obtained by mixing an extract prepared by extracting botanical medicinal herbs with a 30% aqueous ethanol solution with an extract prepared by extracting a botanical medicinal herb-pressed residue separated from the extract with high temperature and high pressure water, wherein the botanical medicinal herbs are prepared by mixing Loranthus parasiticus Merr, Houttuynia cordata, Parthenocissus tricuspidata, Aralia elata, and Rumex acetosa L. to a weight ratio of 2 : 1.5 : 0.5 : 0.5 : 0.5 : 0.5; 0.3 wt% of lecithin; 0.3 wt% of ascorbic acid; 0.2 wt% of sorbic acid; and 0.2 wt% of Jasmine scent.

Description

다기능성 미용비누 조성물 및 그 조성물을 이용한 다기능성 미용비누의 제조방법{The Beauty art-soap of The composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it.}The beauty art-soap of the composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it.}

본 발명은 다기능성 미용비누 조성물 및 그 조성물을 이용한 다기능성 비누의 제조 방법에 관한 것으로, 구체적으로는 기름야자나무(Elaeis guineensis)의 야자과육을 증기로 쪄서 지방분해효소를 불활성화 시킨 다음 압착해서 얻어진 과육팜유와 기름야자 속에 있는 씨앗에서 짜낸 팜핵유를 일정비율로 혼합해서된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로 한 혼합유를 포화수용액의 가성소다와 반응시킨 반응물에 2중량%의 글리세린이 첨가된 비누소지 86중량%, 낙화생유 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5 되도록 혼합한 식물약재를 30%의 알콜 수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물과 그 조성물을 이용한 다기능성 미용비누의 제조방법에 관한 것이다.The present invention relates to a multi-functional cosmetic soap composition and a method for manufacturing a multi-functional soap using the composition, specifically, the coconut meat of the oil palm tree (Elaeis guineensis) is steamed with steam to inactivate the lipolytic enzyme and then compressed. The obtained pulp palm oil and palm kernel oil squeezed from the seeds in the oil palm were mixed at a constant ratio, and the mixed oil having a mixed weight ratio of 78: 6 mixed palm oil and coconut oil was reacted with caustic soda in a saturated aqueous solution. 86% by weight of soap with glycerin, 1% by weight of peanut olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and palm cactus, 0.5% by weight of soapnut, alatoin and bamboo salt respectively, and mulberry mistletoe, fish vinegar, pine ivy, 30% of alcohol is contained in the mixed medicinal plants so that the weight ratio of each of the elm, main tree and mother is 2: 1.5: 0.5: 0.5: 0.5: 0.5. Mixed extract concentrated with the extract extracted with the extract and the extract extracted with high pressure and high pressure water of the plant medicine 5.5 wt%, lecithin 0.3 wt%, ascorbic acid 0.3 wt%, sorbic acid 0.2 wt%, jasmine flavor 0.2 wt% It relates to a multifunctional cosmetic soap composition to be formed and a method for manufacturing a multifunctional cosmetic soap using the composition.

오래전부터 비누는 세수, 세안이나 목욕 시, 피부의 각질 노폐물 및 때와 같은 이물질을 제거하거나 직물지로 된 의류나 이불세탁을 위한 세정제로서 기본적으로 요구되는 기능은 세정력이라 할 수 있다.Since long ago, soap is a detergent for washing clothes, washing faces or baths, removing foreign substances such as keratin wastes and grime from the skin, or for washing clothes or quilts made of textile paper.

그러나 근년에 이르러 경제 성장과 더불어 삶의 질이 향상됨에 따라, 미용에 대한 관심도가 지나치게 높아지고, 이에따라 성형수술을 비롯하여 주름제거를 위한 시술과 피부관리를 위한 고급 화장품, 피부 영양제 구입에 주저하지 않으며 피부와 관련된 비누에 있어서도 탄력성의 피부, 피부의 노화방지, 피부질환의 예방 및 방지 등의 다기능성을 갖는 비누를 선호하고 있다.However, as the quality of life has improved along with economic growth in recent years, the interest in beauty becomes too high, and accordingly, it is not hesitant to buy cosmetic surgery, wrinkle removal, high-quality cosmetics for skin care, and skin nutrition. In the related soap, soap having multifunctionality such as elastic skin, prevention of skin aging, prevention and prevention of skin diseases is preferred.

종래의 비누에 첨가되는 미용제의 예로서, 미국특허 제4.335.125호에 개재된 케토코나졸 및 이트라코나졸 등은 칸디나 피부사상균에 의한 백선(무좀), 지루성 피부염, 전풍 등에 사용하는 항진균제로서, 심재성 진균증 및 표재성 진균증에 유효한 것으로 알려져 있고, 국내특허공개 제90-1790호에는 국소투여에 의한 진균성 피부질환 치료에 적합한 약학적 조성물로서, 용액제, 페이스트제, 연고제의 조성물 및 화장품류인 스킨, 밀크로션 등의 조성물제제가 소개되고 있다. 이와 같은 화학합성제제들은 장기간 경구투여하면 간독성과 위장장애 등의 부작용이 발생하며, 많은 항진균제제들이 일반적으로 비극성물질로서 물이나 극성용매에는 녹지않는 문제점이 있다.As an example of a cosmetic agent added to a conventional soap, ketoconazole and itraconazole, etc., disclosed in U.S. Patent No.4.335.125, are antifungal agents used for ringworm (athlete's foot) caused by canna dermatophytes, seborrheic dermatitis, electric shock, and cardiomycosis And it is known to be effective for superficial mycosis, and in Korean Patent Publication No. 90-1790, a pharmaceutical composition suitable for the treatment of fungal skin diseases by topical administration, the composition of solutions, pastes, ointments and skins and milk lotions as cosmetics Composition formulations, such as, have been introduced. These chemical synthetic agents have side effects such as hepatotoxicity and gastrointestinal disorders when administered orally for a long time, and many antifungal agents are generally non-polar substances, which are insoluble in water or polar solvents.

이상과 같은 화학합성제를 첨가한 미용제들의 문제점들로 최근에는 쳔연물질을 첨가한 미용제를 선호하는 경향으로 나타나, 천연재료를 이용한 미용제들도 함께 연구개발되어 출시되는 제품이 있으며, 이와 같은 종래 미용제들의 예를들면, 국내등록특허공보 등록번호 제446542호에는 "홍삼허브 비누의 제조방법"에 관한 기술이 소개되고 있다. 기술의 내용인즉, 물 13%을 함유하는 코코넛유, 팜유의 식물성유지 80.38%의 조성비로, 80℃로 용해시키고 이 혼합물에 유성성분인 스쿠알렌, 알로에, 토코페롤, 조조바오일 1.42%를 혼합하여 자연상태로 숙성시키며, 숙성된 혼합물에 에탄올로 추출한 홍삼농축액 12.5% 첨가한 혼합물을 65℃까지 가열하여 진공상태에서 배합한 배합물에 참깨오일, 허브에센스오일 5.7%를 투입하여 -65℃로 급냉시키고, 진공압으로 인출하여 성형비누를 제조하는 기술이라 할 수 있으나, 알카리와의 금화반응 없이 주원료인 각종 지방산유지 그리고 그밖에 첨가되는 유동성의 지방산오일을 고형화시키기 어려우므로 재형성이 문제될 수 있고, 비누로서 사용할 수 있는 강도를 유지하기 곤란한 비누라 할 수 있다.As a result of the problems of the cosmetic agents added with the above-mentioned chemical synthetic agents, it has recently been shown to prefer a cosmetic agent containing a non-flammable substance, and there are also products that are researched and developed together with cosmetic agents using natural materials. As an example of the same conventional cosmetic agents, the technology related to "the manufacturing method of red ginseng herb soap" is introduced in Korean Patent Registration No. 446542. The content of the technology, that is, the composition ratio of coconut oil and palm oil containing 13% of water, 80.38% of vegetable oil, dissolved at 80 ° C., and mixed with 1.42% of squalene, aloe, tocopherol, and jojoba oil as an oily component in this mixture The mixture was added with 12.5% of red ginseng extract extracted with ethanol to the aged mixture, heated to 65 ° C, and 5.7% of sesame oil and herbal essence oil were added to the blended mixture under vacuum to rapidly cool to -65 ° C. It can be said to be a technology to manufacture molded soap by pneumatic drawing, but it can be difficult to solidify various fatty acid oils and other fatty acids that are the main raw materials without gold reaction with alkali, so reformation may be a problem. Soap can be said to be difficult to maintain the strength.

다른 종래 예로서 국내특허공보(등록번호 제743830호)에 "화장비누 조성물"이 소개되고 있으며 기술의 구성은 세정성분으로서 음이온 계면활성제를 포함하는 비누에 있어서, 4급 암모늄 양이온 계면활성제를 포함하는 화장비누 조성물에 관한 것으로, 세정력 및 피부의 보습력은 기대할 수 있는 비누라 할 수 있으나, 피부를 보호하는 작용이나 항균작용 약리적인 기능 등은 기대할 수 없는 비누라 하겠다.As another conventional example, "Hwagi-no-nu composition" is introduced in Korean Patent Publication (Registration No. 743830), and the composition of the technology includes a quaternary ammonium cation surfactant in a soap containing an anionic surfactant as a cleaning component. Regarding the cosmetic soap composition, the cleaning power and the moisturizing power of the skin may be expected soap, but the action of protecting the skin or the pharmacological function of antibacterial action may be expected to be a soap.

1. 미국특허공보 제4.335.125호1. United States Patent Publication No. 4.35.125 2. 대한민국 특허공개공보 제90-1790호2. Republic of Korea Patent Publication No. 90-1790 3. 대한민국 등록특허공보 제446542호3. Republic of Korea Registered Patent Publication No. 446542 4. 대한민국 등록특허공보 제743830호4. Republic of Korea Registered Patent Publication No. 743830

수중에서 쉽게 팽윤되거나 풀어지지 않는 단단한 비누를 얻을 수 있고, 대장균, 티프스균, 파라티스프균, 적라균, 비병원성 곰팡이는 물론 백선균 무좀균, 포도상균, 림균, 항산성세균에 대해 강력한 항균작용이 있어 각종 질병을 예방할 수 있고, 피부병, 피부염증, 옴, 습진, 피부암 등 각종 피부병의 예방 및 치료효과가 있으며 항산화작용에 의한 항산화 시너지스트 효과로 피부의 노화를 지연시킬 수 있는 다기능성 비누 조성물과 이 조성물을 이용한 다기능성 비누의 제조방법을 제공함에 있다.You can get a solid soap that does not swell or loosen easily in water, and has a strong antibacterial effect against E. coli, typhus, paratisif, mycobacterium, non-pathogenic fungi, as well as ringworm, athlete's foot, staphylococcus, staphylococcus aureus, and antibacterial It is a multifunctional soap composition that can prevent various diseases, prevent and treat various skin diseases such as skin disease, skin inflammation, scabies, eczema, and skin cancer, and delay aging of the skin by anti-oxidant synergistic effect due to antioxidant action. It is to provide a method for producing a multifunctional soap using the composition.

기름야자나무(Elaeis guineensis)의 야자과육에서 얻은 과육팜유와 씨앗에서 얻은 핵팜유의 중량비율을 4:1~5:1로한 혼합팜유와 코코넛유의 혼합비를 78:6으로 해서된 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 글리세린을 첨가시킨 비누소지 86중량%에 낙화생유 올리브유 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5 되도록 혼합한 천연식물약재를 알콜 수용액으로 추출한 추출액과 천연 식물약재의 압착잔사를 고온고압수로 추출한 추출액을 혼합한 식물약재 혼합추출액을 농축시킨 0.2~0.3포이즈의 식물약재 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물 및 아래와 같이 그 조성물을 이용한 다기능성 미용비누의 제조방법을 제공함으로서 본 발명 과제를 해결할 수 있었다.Caustic soda is a mixed plant oil with a mixed palm oil and coconut oil ratio of 78: 6 with a weight ratio of 4: 1 to 5: 1 of the palm oil obtained from the palm of the palm tree (Elaeis guineensis) and the nuclear palm oil obtained from the seeds. 86% by weight of soap with 2% by weight of glycerin added to the reactant reacted with saturated aqueous solution. 1% by weight of peanut olive oil galactose fermentation solution, salicylic acid, aloe fermentation solution, and palm cactus, respectively, 0.5% by weight of soap, alatoin, and bamboo salt % And compress natural extracts extracted with alcoholic aqueous solution and natural plant medicinal materials mixed with mulberry mistletoe, eoseongcho, pine ivy, elm, main tree and maternal weight ratio of 2: 1.5: 0.5: 0.5: 0.5: 0.5 Botanical herb mixture extract concentrate of 0.2 ~ 0.3 poise, which concentrated the plant extract mixture extract with the extract extracted from the high temperature and high pressure water, 5.5 wt%, lecithin 0.3 wt%, ah The present invention could be solved by providing a multifunctional cosmetic soap composition composed of 0.3% by weight of scorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine flavor, and a method of manufacturing a multifunctional cosmetic soap using the composition as follows. .

상기 다기능성 미용비누 조성물을 이용한 다기능성 비누의 제조방법은 기름야자나무(Elaeis guineensis Jacq)의 야자과육에서 얻은 과육팜유와 씨에서 얻은 핵팜유의 혼합중량비율을 4:1~5:1로한 혼합팜유와 코코넛유 혼합비를 78:6으로 해서된 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 그리세린을 첨가 균질화시켜 비누소지를 얻는 1단계 공정;The manufacturing method of the multi-functional soap using the multi-functional cosmetic soap composition is a mixture of pulp palm oil obtained from palm pulp of an oil palm tree (Elaeis guineensis Jacq) and nuclear palm oil obtained from seeds in a ratio of 4: 1 to 5: 1. A first step of obtaining a soap base by homogenizing 2% by weight of griserin to the reactant obtained by reacting a mixed vegetable oil having a palm oil and coconut oil mixing ratio of 78: 6 with a caustic soda saturated aqueous solution;

상기 비누소지 86중량%, 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알란토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무담쟁이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 알콜수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압수로 추출한 추출액을 혼합한 혼합 추출액을 0.2~0.3 포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민 0.2중량%로 다기능성 미용비누 조성물을 조성하는 2단계 공정;The soap base 86% by weight, peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and palm cactus, respectively 1% by weight, soapnut, allantoin and bamboo salt 0.5% by weight respectively, and mulberry mistletoe, eoseongcho, pine ivy, elm, Mixed extracts obtained by extracting the extracted herbal extracts with alcohol aqueous solution and the extracts obtained by extracting the squeezed residues of the herbal extracts with high temperature and high pressure water so that the weight ratio of each of the main leaves and mothers is 2: 1.5: 0.5: 0.5: 0.5: 0.5. A two-step process of forming a multi-functional cosmetic soap composition with 0.2-0.3 poise mixed extract concentrate 5.5 wt%, lecithin 0.3 wt%, ascorbic acid 0.3 wt%, sorbic acid 0.2 wt%, jasmine 0.2 wt%;

상기 다기능성 미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 비누원료를 얻는 3단계 공정;A three-step process of reacting for 1 hour in a state where the multifunctional cosmetic soap composition is heated to a temperature of 80 to 85 ° C and maintained while stirring to obtain a colloidal soap raw material;

상기 비누 원료의 수소이온 농도(PH)를 유기산 또는 유기알카리로 PH6~7범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the soap raw material to a pH range of 6 to 7 with an organic acid or an organic alkali; And

PH를 조절한 비누원료를 온도 80~85℃로 유지시켜 감압시킨 상태에서 열처리하여 수분함량 8~10% 건조시킨 후 3~4일간 숙성 안정화시킨 다음 성형하는 5단계 공정으로 구성되는 다기능성 비누의 제조방법이다.It is a multi-functional soap consisting of a 5-step process of forming and then stabilizing the aged 3 ~ 4 days after drying the 8 ~ 10% moisture content by heat treatment under reduced pressure by maintaining the pH adjusted soap raw material at a temperature of 80 ~ 85 ℃. It is a manufacturing method.

본 발명 다기능성 미용비누 조성물 및 그 조성물을 이용한 다기능성 미용비누의 제조방법으로 얻어진 비누는 물에 쉽게 용해되거나, 팽윤되지 않는 내마모성의 단단한 비누로 오래 사용할 수 있는 잇점이 있고, 우수한 항균성, 항바이러스성, 항염증 및 살균작용이 있어 피부질병의 예방은 물론 각종 염증, 부스럼, 가려움증, 아토피성 피부질환, 옴, 습진, 무좀, 검버섯, 주근깨, 기미, 백선, 피부암 치유효과가 있고 항산화 시너지스트 효과로 지속적으로 사용 시, 피부의 노화 진행을 지연시킬 수 있고 항산화제 및 보존재로 비누변질을 방지할 수 있는 다기능성 미용비누 조성물 및 그 비누 조성물을 이용한 다기능성 미용비누라 할 수 있다.Soap obtained by the multifunctional cosmetic soap composition of the present invention and a method for manufacturing a multifunctional cosmetic soap using the composition has the advantage of being a long-lasting abrasion-resistant soap that does not easily dissolve in water or swell, and has excellent antibacterial and antiviral properties. It has sex, anti-inflammatory and antiseptic action, and prevents skin diseases as well as various inflammations, swelling, itchiness, atopic skin diseases, scabies, eczema, athlete's foot, blotch, freckles, blemishes, ringworm, skin cancer, and antioxidant synergistic effects. With continuous use, it can be said to be a multifunctional cosmetic soap composition that can delay the progress of aging of the skin and prevent soap deterioration with antioxidants and preservatives, and a multifunctional cosmetic soap using the soap composition.

본 발명 다기능성 비누 조성물 및 그 조성물을 이용한 다기능성 비누의 제조방법에 관한 것으로 이를 구체적으로 설명하면 본 발명 다기능성 미용비누 조성물을 기름야자나무(Elaeis guineensis Jacq)의 기름야자 과육에서 얻은 과육팜유와 씨로부터 얻은 핵팜유의 혼합중량비율을 4:1~5:1로 혼합한 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 글리세린을 첨가하여 균질화시킨 비누소지 86중량%에 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비로 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 천연식물약재 100중량부를 30%의 에타놀 수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압 수용액으로 추출한 추출액을 혼합한 2~3포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물에 관한 것이며 그 조성물을 이용한 다기능성 미용비누의 제조방법은 기름야자의 과육팜유와 씨앗에서 짜낸 핵팜유의 혼합중량비를 4:1~5:1로 혼합해서된 혼합팜유와 코코넛유의 배합중량비를 78:6의 혼합식물유를 가성소다 포화수용액과 반응시킨 2중량%의 글리세린을 첨가해서 균질화시킨 비누소지를 얻는 1단계 공정; The present invention relates to a multifunctional soap composition and a method for manufacturing a multifunctional soap using the composition. Specifically, the present invention provides a multifunctional cosmetic soap composition obtained from the oil palm pulp of an oil palm tree (Elaeis guineensis Jacq). 2% by weight of glycerin in the reaction mixture obtained by mixing the mixed palm oil obtained from the seed with a mixed palm oil ratio of 4: 1 to 5: 1 and a mixed vegetable oil with coconut oil of 78: 6 with a saturated aqueous sodium hydroxide solution. Addition of homogenized soap base to 86% by weight of peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and palm cactus, respectively 1% by weight, soapnut, alatoin, and bamboo salt 0.5% by weight respectively, and mulberry mistletoe, eoseongcho, pine 30% by weight of 100 parts by weight of natural plant medicines mixed in a ratio of 2: 1.5: 0.5: 0.5: 0.5: 0.5 by weight ratio of each of ivy, elm, maple, and mother Mixed extract concentrate of 2 ~ 3 poise which mixed the extract extracted with ethanol solution of ethanol and the extract extracted with the high pressure and high pressure aqueous solution of the plant medicine 5.5 wt%, lecithin 0.3 wt%, ascorbic acid 0.3 wt%, sorbic acid 0.2 wt %, Jasmine fragrance is a multi-functional cosmetic soap composition composed of 0.2% by weight, and the method of manufacturing the multi-functional cosmetic soap using the composition is a mixture weight ratio of pulp palm oil and nuclear palm oil squeezed from seeds from 4: 1 to 5 A 1-step process to obtain a homogeneous soap base by adding 2% by weight of glycerin reacted with a saturated aqueous solution of caustic soda with a mixed vegetable oil of 78: 6 with a mixed palm oil and coconut oil ratio of 1: 1;

상기 비누소지 86중량% 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 알콜 수용액으로 추출한 추출액과 식물약재의 추출잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출액을 농축하여 얻은 2~3포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물을 조성하는 2단계 공정;The soap base 86% by weight peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and palm cactus, respectively 1% by weight, soapnut, alatoin and bamboo salt 0.5% by weight respectively, and mulberry mistletoe, eoseongcho, pine ivy, elm, A mixture extract of a mixture of plant extracts extracted with an aqueous alcohol solution and an extract extracted with high-temperature and high-pressure water was mixed with a mixture of plant drugs so that the weight ratio of each of the main leaves and mothers was 2: 1.5: 0.5: 0.5: 0.5: 0.5. 2 to 3 poise obtained by concentrating 2% to create a multifunctional cosmetic soap composition composed of 5.5% by weight of a concentrated extract, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine flavor Step process;

상기 다기능성 미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 비누원료를 얻는 3단계 공정;A three-step process of reacting for 1 hour in a state where the multifunctional cosmetic soap composition is heated to a temperature of 80 to 85 ° C and maintained while stirring to obtain a colloidal soap raw material;

상기 비누 원료의 수소이온 농도(PH)를 유기산 또는 유기알카리로 PH6~7범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the soap raw material to a pH range of 6 to 7 with an organic acid or an organic alkali; And

수소이온농도를 PH6~7로 조절한 비누원료를 온도 80~85℃로 유지시키면서 감압시킨 상태에서 수분함량 8~10%될때까지 건조시킨 후 3~4일간 숙성 안정화시킨후 성형하는 5단계 공정으로 구성되는 다기능성 비누의 제조방법이다.This is a five-step process of drying the soap raw material with the hydrogen ion concentration adjusted to PH6 ~ 7 while maintaining the temperature at 80 ~ 85 ℃, reducing the pressure to 8 ~ 10% of moisture content, stabilizing aging for 3 ~ 4 days, and then shaping. It is a method for manufacturing a multifunctional soap.

상기 본 발명 미용비누 제조방법에 있어서, 다른 실시예로서, 혼합 식물유에 가성소다 대신 유기 알카리인 트리에타놀아민과 반응시켜 다기능성 미용 크림비누를 제조할 수 있으며 이를 구체적으로 설명하면 기름야자의 과육으로부터 얻은 과육팜유와 씨에서 얻은 핵팜유 혼합비를 2:1~3:1로 혼합해서된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 식물혼합유를 트리에타놀아민 포화수용액과 반응시킨 반응물에 2중량%의 그리세린을 첨가 균질화시킨 다기능성 크림비누 소지를 얻는 1단계 공정;In the method for manufacturing a cosmetic soap of the present invention, as another embodiment, a multifunctional cosmetic cream soap can be prepared by reacting a mixed vegetable oil with triethanolamine, an organic alkali, instead of caustic soda. 2 to the reaction product obtained by mixing the mixed palm oil and coconut oil obtained by mixing the obtained pulp palm oil and seeds in a ratio of 2: 1 to 3: 1 with a mixed vegetable oil ratio of 78: 6 and a saturated aqueous solution of triethanolamine. A one-step process of obtaining a multifunctional cream soap base with homogenization by addition of weight percent griserin;

상기 크림비누소지 86중량%, 낙화생유, 올리브유, 갈락토즈발효액, 살리실산, 알로에발효액 및 손바닥선인장 각각 1중량%, 소프넛, 알란토인, 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무담쟁이, 두릅나무, 주엽나무 및 산모의 혼합중량비를 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합된 천연식물약재의 추출농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 크림미용비누 조성물을 조성하는 2단계 공정;The cream soap base 86% by weight, peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution and palm cactus, respectively 1% by weight, soapnut, allantoin, bamboo salt 0.5% by weight each, and mulberry mistletoe, eoseongcho, pine ivy, elm , Extract weight of 5.5% by weight of the natural plant medicinal mixture mixed so that the mixed weight ratio of main leaves and mothers is 2: 1.5: 0.5: 0.5: 0.5: 0.5, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid %, A two-step process of forming a multifunctional cream beauty soap composition composed of 0.2% by weight of jasmine;

상기 다기능성 크림미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 크림미용비누 원료를 얻는 3단계 공정;A three-step process of reacting for 1 hour while maintaining the temperature of the multifunctional cream beauty soap composition heated to 80 to 85 ° C while stirring to obtain a raw material for cream beauty soap;

상기 교질상 크림미용비누 원료의 수소이온 농도(PH)를 유기산, 유기알카리로 PH6~7의 범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the creamy beauty soap raw material in the range of PH6 to 7 with organic acid and organic alkali; And

PH를 조절한 크림미용비누 원료를 온도 80~85℃로 유지시킨 상태에서 감압처리하여 수분함량 60~65%될때까지 열처리한 후 냉각시킨 후 3~4일간 숙성 안정화시키는 5단계 공정으로 구성되는 다기능성 크림미용비누 제조방법이라 할 수 있다.It consists of a five-step process that stabilizes aging for 3 to 4 days after cooling after heat treatment until the moisture content is 60 to 65% by subjecting the PH beauty cream soap raw material to reduced pressure while maintaining the temperature at 80 to 85 ℃. It can be said to be a functional cream beauty soap manufacturing method.

상기 본 발명 비누소지 원료로 사용하고 있는 기름야자나무(Elaeis guineensis Jacq)의 기름야자의 열매에 24~34%, 열매살에 50~67%, 속씨에 50~55%의 기름이 있으며 기름을 구성하고 있는 지방산은 팔미틴산 40%, 올레인산 45%, 스테아린산 3.6%, 리놀산 8%, 미스트린산 3.6%로 이루어져 있고 기름에는 0.06%카로틴이 있으며 열매의 과육을 과열수증기로 쪄서 지방분해 효소를 비활성화시킴과 동시에 단백질을 응고시키고 압착하여 기름을 얻게 되는데 이를 과육팜유라 하고 열매 속씨를 압착하여 얻어진 기름을 핵팜유라고 하며 과육(열매살)팜유와 핵팜유는 성분에서 큰 차이가 있고 과육팜유는 핵팜유에 비해 비누 사용시 물에서 쉽게 팽윤되거나 물러지지 않으므로 비누를 오래 사용할 수 있으며 반면 핵팜유는 항균 보습효과가 우수하고 과육팜유에 비해 고급유라 할 수 있다.The oil palm tree (Elaeis guineensis Jacq) used as a raw material for soaps of the present invention has 24-34% in the fruit of the oil palm, 50-67% in the fruit flesh, and 50-55% in the seed, and constitutes oil The fatty acid you are doing consists of 40% palmitic acid, 45% oleic acid, 3.6% stearic acid, 8% linoleic acid, 3.6% myristic acid, and 0.06% carotene in the oil, and it deactivates lipolytic enzymes by boiling the flesh of the fruit with superheated steam. The protein is solidified and compressed to obtain oil. This is called pulp palm oil, and the oil obtained by squeezing the fruit seed is called nuclear palm oil, and the pulp (fruit flesh) palm oil and nuclear palm oil have a large difference in composition, and the pulp palm oil is compared to the nuclear palm oil. When using soap, soap can be used for a long time because it does not swell or swell easily in water. There.

낙화생유는 성분으로 알카로이드 아미노산이 함유되어 있고 보습효과 아토피성 피부질환 땀띠 여드름 치유에 효과가 있고 항균 기능을 갖는 식물유이며 올리브유는 감람나무의 열매살에 50~70%, 씨에 20%기름을 함유하고 있으며 기름의 7~10%는 팔미틴, 2~4%는 스테아린, 20~84%는 올레인, 4~12%는 리놀레인을 함유하고 있으며 작용으로는 보습효과 가려움증해소 여드름진정, 항암효과가 있는 것으로 알려져 있다.The peanut oil contains alkaloid amino acids as a component, has a moisturizing effect, is effective in healing acne, atopic skin disease, and has antibacterial function. Olive oil contains 50-70% in the flesh of olive trees and 20% oil in seeds. 7 ~ 10% of oil contains palmitin, 2 ~ 4% of stearin, 20 ~ 84% of olein, 4 ~ 12% of linolein, and its action has a moisturizing effect to relieve itching, acne soothing, and anticancer effects. It is said to be.

갈락토즈 발효액은 생연초 추출물로서 부틸렌그리콜, 펜틸렌그리콜, 소디움벤죠이트가 함유되어 있고 작용으로는 항암효과가 있고 죽은깨, 기미, 검버섯제거 효과가 있는 것으로 알려져 있다.Galactose fermentation broth is a raw tobacco extract that contains butylene glycol, pentylene glycol, and sodium benzoate, and is known to have anti-cancer effects and action to remove sesame seeds, spots, and black spots.

알란토인은 방울풀의 잎과 씨에는 알리스톨톤, 알란토인(C4H6O3N4), 마그노플로린, 알칼로이드인 아리스톨로킨과 사포닌, 유기산, 탄닌질이 함유되어 있는데 알란토인 성분을 분리 추출한 추출액으로 여드름, 아토피성 알러지 염증에 효과가 있고 향균성이 우수하며 살리신산은 조팜나무 잎에 함유되어 있는 아스코르빈산 살리실산메틸 성분을 함유하고 있으며 이로부터 추출 분리한 쳔연의 살리실산으로 여드름을 진정시키고 피부미용, 습성습진에 효과가 있는 것으로 알려져 있다.Allantoin contains allistoltone, allantoin (C 4 H 6 O 3 N 4 ), magnoflorin, alkaloid aristolokine, saponin, organic acid, tannin, etc. in the leaves and seeds of lily of the valley. As it is effective for acne and atopic allergic inflammation, and has excellent antibacterial properties, salicylic acid contains methyl ascorbic acid salicylate component contained in the leaves of the palm tree, and it is extracted and separated from the salicylic acid, soothing acne and skin care , It is known to be effective in wet eczema.

죽염은 대나무에 소금을 넣어 1500℃ 이상의 고온에서 3회 구운 죽염으로 미네랄성분이 풍부하며 가려움즘, 아토피성 피부염, 건선억제, 항균 및 방부효과가 있다.Bamboo salt is a bamboo salt baked three times at a high temperature of 1500 ℃ or more with salt in bamboo. It is rich in minerals and has itch, atopic dermatitis, psoriasis inhibition, antibacterial and antiseptic properties.

소피넛은 무환자나무의 열매살에 얻은 추출액으로 추출액에는 무환자사포닌(사핀두스 사포닌)이 다량 함유되어 있어 물과 만나면 다량의 거품이 발생하고 천연세제로 사용되며 종래 민간에서도 세척제 그리고 피부와 머리를 감는데 사용해온 것으로 작용으로는 얼굴의 죽은 깨, 몸에서 발산하는 냄새를 없애는데 효과가 있다.Soapnut is an extract obtained from the fruit of the fruitless tree, and the extract contains a large amount of the patient-free saponin (sapindus saponin), which causes a large amount of bubbles when used with water and is used as a natural detergent. It has been used to help remove dead sesame from the face and the odor emitted from the body.

알로에 속 식물은 약 170종이 있고, 잎은 살져있고 변두리에 가시가 있으며, 흰색, 노란색, 붉은색 꽃이 이삭처럼 모여 핀다. 열대지방에 자라는 것은 높이 4m이고, 잎의 길이는 65cm에 달하고, 알로에는 산지에 따라 기원식물이 다르며 케이프(cape)알로에, 나탈(nathal)알로에, 소코트린(socotrine)알로에, 잔지바르(zanzibar)알로에, 구라카오(curacao)알로에, 자파라바드(jaffarabad)알로에가 있고, 우리나라에는 긴 잎 알로에, 얼룩 잎 알로에, 넓은 잎 알로에가 있다. 알로에의(잎즙)에는 알로인 C20 H18 O9(알로에-에모딘-d-아라비노시드) 16~20%, 알로에-에모딘, 나탈로인, 라바르베론(이소에모딘), 수지 12%(알로레시탄놀 C22 H26 O6의 계파산에스테르)가 함유되어 있다. 알로에 잎즙 말린 것은 소화 및 식욕 항진약으로 사용하고 있고 알로에 생즙은 소량의 에타놀을 첨가 항균약으로 상처를 관장하거나, 썩는 염증부위를 씻는데 사용하며, 또한 본 발명에서 사용되는 알로에 생잎을 썰어서 암실에서 온도 4~8℃를 유지시켜 12~15일간 발효시킨 것은, 약해지는 생명활동을 자극하는 생물원 자극소라고 하는 물질이 생성되는데, 그 화학조성은 아직 밝혀지지 않았으나 대체로 지방족디카르본산, 분자량이 큰 방향족유기산으로 보고있으며 생물원자 극소라하는 생성물질을 환자의 면역기능을 향상시키며, 방사선 피해 시, 피부손상을 방지하는데 사용되고 상처, 화상피부와 점막 염증치료에 바르기도 하며 민간요법으로 피부암, 땀띠, 여드름 치유에 사용되고 있고 미용효과로서는 보습효과가 크다.There are about 170 aloe plants, the leaves are fleshy, there are thorns on the edges, and white, yellow, and red flowers gather like spikes. Growing in the tropics is 4m high, the leaves are 65cm long, and aloes have different origins depending on the mountainous region, cape aloe, nathal aloe, socotrine aloe, zanzibar aloe , Curacao aloe, jaffarabad aloe, long leaf aloe, spot leaf aloe, broad leaf aloe. Aloe vera (leaf juice) contains alloin C20 H18 O9 (aloe-emodine-d-arabinoside) 16-20%, aloe-emodine, nataloin, labarone (isoemodine), resin 12% ( Allorecitanol C22 H26 O6). Dried aloe leaf juice is used as an anti-digestion and appetite suppressant, and aloe juice is used as an antibacterial drug to add a small amount of ethanol to wash wounds or to wash out rotting inflammation, and also cut aloe leaves used in the present invention in the dark. Maintaining the temperature of 4 ~ 8 ℃ and fermenting for 12 ~ 15 days, a substance called a biostimulant that stimulates weakening life activities is produced. Its chemical composition has not been revealed yet, but generally has an aliphatic dicarboxylic acid and molecular weight. It is considered to be a large aromatic organic acid, and it is used to improve the immune function of patients by generating substances called micro-atomics, and to prevent skin damage in case of radiation damage. It is also applied to the treatment of wounds, burn skin and mucosal inflammation. , It is used for acne healing and has a great moisturizing effect as a cosmetic effect.

또한 손바닥선인장 진액은 무질소물로서 프라보노이드 성분이 함유되어 있고 악성피부염, 염증 치유에 효과가 있다.In addition, palmar cactus essence is a nitrogen-free substance that contains flavonoids and is effective in healing malignant dermatitis and inflammation.

그 밖에 뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무 및 산모의 천연 식물약재들은 피부병에 대한 항균성을 가지거나 피부질병을 예방, 치유할 수 있는 천연 식물약재들로서 그 성분과 작용을 알아보면, 뽕나무 겨우살이의 잎이 붙은 가지에서 알칼로이드, 플라보노이드, 사포닌이 확인 되었으며, 또한 올레아놀산(C30 H48 O3), b-아미린(C10 H50 O), 메소이노시톨, 비스찐, 옥시다제, 세릴알콜, 미리스틴산, 아라킨, 고무질(점액), 페닐아민, 프로피오콜린, 아세틸콜린, 수지가 있다.In addition, natural plant drugs of Mulberry mistletoe, pine ivy, Eoseongcho, elm tree, jujube tree, and mother are natural plant drugs that have antibacterial properties against skin diseases or prevent and heal skin diseases. Alkaloids, flavonoids, and saponins have been identified in the leaves of the Mulberry mistletoe, and also oleanolic acid (C30 H48 O3), b-amirin (C10 H50 O), mesoinositol, bischin, oxidase, seryl alcohol, myristic acid , Arachine, rubber (mucus), phenylamine, propiocholine, acetylcholine, and resin.

구라파에서 자라는 겨우살이에는 흰 무정형 물질인 비스코톡신, 시린기린, 고무질과 수지가 들어 있으며, 비스코톡신은 3가지 물질 즉, 비스코톡신 A2, A3, B로 순수하게 분리되었으며 이 3 물질은 모두 46개 아미노산으로 이루어졌으나, 배열순서에서 다르다. 비스코톡신 A3은 유황을 가교로 한 연결이 3곳에 있고, 즉 16과 26번 사이 그리고 3과 40번, 4와 32번 사이에 유황연결이 있으며 이 펩티드는 항암활성이 있다. The mistletoe that grows in Europe has a white amorphous substance, biskotoxin, sirin giraffe, rubber and resin. Biskotoxins are purely separated into three substances: biskotoxins A2, A3, and B, all of which are 46 amino acids It is made, but it is different in the order of arrangement. Biscotoxin A3 has three bridging bridging links, namely, bridging bridging between 16 and 26, and bridging between 3 and 40, 4 and 32, and this peptide has anticancer activity.

씨에는 응집소인 아그글루티닌이 있는데 미량에서 항암작용을 하며 여기에는 N-모노메틸리진이 0.10~0.25그람분자%, N-디메틸리진이 0.15~0.30그람분자%, N-트리메틸리진이 0.05~0.12그람분자%이 있으며 활성은 뒤의 것이 세다.Ag has agglutinin, an agglutinin, which has anti-cancer activity in a trace amount. N-monomethyl lysine is 0.10 to 0.25 gram molecule%, N-dimethyl lysine is 0.15 to 0.30 gram molecule%, and N-trimethyl lysine is 0.05 ~. There is 0.12 gram molecule% and the activity is strong.

또한 이 천연 식물약재는 11종의 항암활성 단백질이 분리되었으며, 이것들은 0.006~0.05mg/kg에서 암세포의 디핵산 합성을 억제하며, 항암 단백질이 약간이라도 변질되면 항암활성이 없어지며 4종의 단백질 성분은 센 항원성이 있는데, 10ug 아래에서 항체를 생산하고, 비스코톡신 A는 사르코마 180 암을 일으킨 흰 생쥐의 생존기간을 대조에 비하여 98%로 더 늘이였다.In addition, 11 kinds of anticancer activity proteins were isolated from this natural plant medicine, and they inhibited the synthesis of dinucleic acid in cancer cells at 0.006 to 0.05 mg / kg. The component has strong antigenicity, producing antibodies below 10 ug, and biscotoxin A further increased the survival time of the white mice that caused Sarcoma 180 cancer to 98% compared to the control.

작용으로는 항균, 항바이러스, 항암 기능이 있다. 소나무 담쟁이의 줄기와 잎은 사포닌(용혈지수 100), 찌아니딘과 말비딘의 3.5-디글루코시드, 말비딘-3-글루코시드, 씨에 알카로이드가 있다. 종양 흡수약, 응종, 벤 상처, 피부 염증, 여드름 억제 효과가 있다.Actions include antibacterial, antiviral and anticancer functions. The stems and leaves of pine ivy have saponins (hemolysis index 100), 3.5-diglucosides of guanidine and malvidin, malvidin-3-glucoside, and alkaloids in seeds. It has the effect of absorbing tumors, coping, burning wounds, skin inflammation, and acne.

소나무담쟁이의 줄기와 잎에는 사포닌(용혈지수 100), 찌아니딘, 말비딘 3.5-디 글루코시드, 말비딘-3-글르코시드, 씨에는 알카로이드가 들어 있으며 작용으로는 종양흡수약으로 옹종치료에 사용하며 가려움증, 여드름 치료에 효능이 있고 피부미용에 효과적이다.The stems and leaves of pine ivy contain saponins (hemolytic index 100), guanidine, malvidin 3.5-di glucoside, malvidin-3-glycoside, and alkaloids in seeds. Used for itching, it is effective in treating acne and is effective for skin beauty.

어성초의 생전초에는 정유가 함유되어 있다. 그 주성분은 메틸노닐케톤, 미르센, 라우린알데히드, 카프린알데히드, 카프르산이고 이 밖에도 기체 크로마토그래피에 의해 28개의 성분이 밝혀졌다.Eoseongcho's raw vinegar contains essential oils. Its main components are methylnonyl ketone, myrcene, laurinaldehyde, caprinaldehyde, and capric acid. In addition, 28 components have been identified by gas chromatography.

이 식물의 비린내와 같은 불쾌한 냄새는 데카노일아세트알데히드와 라우릴알데히드에 의한 것으로, 이 성분은 신선한 어성초에만 들어있으며 100℃ 이상의 고온 처리시는 그의 변화 생성물인 메틸노닐케톤, 미르센, 카프르산이 있다.The unpleasant smell like this fishy smell is due to decanoyl acetaldehyde and lauryl aldehyde, which is contained only in fresh fish, and when it is processed at a temperature higher than 100 ℃, its products of change are methylnonyl ketone, myrcene, and capric acid. have.

잎에는 쿠에르찌트린과 물에 용해되는 무기성분 2.7%가 들어있고 그의 주성분은 칼리움염이다. 꽃과 열매 이삭에는 쿠에르찌트린이 없고 이소쿠에르찌트린이 들어있다.The leaves contain 2.7% of quercitrin and an inorganic component that dissolves in water, and its main component is kalium salt. The flowers and berries of Isaac do not contain quercitrin, but contain isoquercerin.

작용으로는 대장균, 티푸스균, 파라티푸스균, 적리균, 림균, 포도상균 및 사상균에 대한 항균작용이 있고, 데카노일아세트알데히드는 비병원성 곰팡이는 물론 백선균, 무좀균 등에 대한 항균작용이 있으며, 포도상균, 임균, 항산성세균에도 억균작용이 있고, 포도상균에 대한 항균력은 슬파민보다 훨씬 세다.Actions include antibacterial activity against E. coli, typhoid bacteria, paratyphoid bacteria, antagonistic bacteria, rim bacteria, staphylococcus and filamentous bacteria, and decanoyl acetaldehyde has antibacterial activity against non-pathogenic fungi, as well as ringworm and athlete's foot, staphylococcus, gonorrhea, Antimicrobial bacteria also have antibacterial properties, and the antibacterial activity against staphylococcus is much stronger than that of sphamin.

전초는 피부염증약, 무좀치루, 아토피, 여드름, 피부질환, 가려움증에 효과가 있다.Outpost is effective for skin irritation, athlete's foot, atopy, acne, skin disease, and itching.

두릅나무의 껍질에는 사포닌 배당체인 아랄로시드(타랄린)가 들어있다. 아랄로시드 A는 물 분해하면 올레아놀산과 포도당, 아라비노즈, 2분자의 글루쿠론산이 되고, 아랄로시드 B는 물 분해하면 올레놀산과 포도당, 아라비노즈, 2분자의 글루쿠론산이 되며 아랄로시드 C를 가수분해하면 올레아놀산과 포도당, 아라비노즈, 글루쿠론산, 갈락토즈가 되고 그 밖에 정유 0.05% 푸로토카테킨산, 콜린이 함유되어 있으며, 또한 알카로이드 반응에 양성인 물질도 있다.The bark of the elm tree contains araloseid (taralin), a saponin glycoside. When decomposing water, araloxide A becomes oleanolic acid, glucose, arabinose, and two molecules of glucuronic acid. When water is decomposed into water, araloxide B becomes olenolic acid, glucose, arabinose, and two molecules of glucuronic acid. Hydrolysis of seed C results in oleanolic acid, glucose, arabinose, glucuronic acid, and galactose. Other essential oils contain 0.05% furocatechinic acid and choline, and there are also substances that are positive for alkaloid reactions.

사포닌은 줄기보다 뿌리껍질에 많으며, 씨에는 약 5%의 기름이 있고 이 기름에는 페트로셀린산, 팔매틴산, 리놀산, 페트로셀리딘산이 있으며, 뿌리에는 스티그마스테린, 탄닌질, 꽃 이삭에는 크산틴, 구아닌, 어린 싹에는 로이진, 아스파라긴산, 글루타민산, 아스파라긴, 알라닌, 티로신, 히스티딘 등이 많다.Saponins are more in the roots of the bark than the stems, with about 5% oil in the seeds, and petrolic acid, palmitic acid, linoleic acid and petrocelidic acid in the oil, and stigmasterin, tannin in the root, and xanthine in the ear of the flower. , Guanine, young shoots are high in leucine, aspartic acid, glutamic acid, asparagine, alanine, tyrosine, and histidine.

작용으로는 뿌리껍질의 물 또는 알콜 추출물은 흥분작용이 있으며, 메디날에 대한 길항작용과 함께 강심작용이 있다.As an action, the water or alcoholic extract of the root bark has an excitatory action, and has an antagonistic action along with an antagonism to the Medinal.

또한 두릅나무 껍질의 약리작용 성분은 아랄로시드로서, 아랄로시드 조직의 산화환원 과정과 신상선 피질의 글루코코르티코이드 분비기능을 높이며, 유기체의 저항성과 백혈구의 탐식기능도 높히며, 잇발지지 조직층(치주층) 치료에도 좋은 효과가 있으며 그 밖에도 부종, 수종, 피부의 상처를 치유하는 효과가 있다.In addition, the pharmacological action component of the bark of the elm tree is araloside, which enhances the oxidation-reduction process of the arloside tissue and the glucocorticoid secretion function of the thyroid cortex, enhances the resistance of the organism and the gluttony function of the white blood cells, and supports the tissue layer ( Periodontal layer) It has a good effect on treatment, and also has the effect of healing edema, edema, and wounds on the skin.

주염나무의 어린 잎에는 알칼로이드 함량이 높고, 열매는 조협이라 하여 가을에 따서 말린 것이고, 씨는 조협지라 하여 여문 씨를 증기에 쪄서 말린 것이며, 가시를 따서 말린 것을 조각자라 한다.The young leaves of the main tree have high alkaloid content, and the fruit is called Johyup and dried in autumn, and the seed is called Johyupji and dried by steaming Yeomun seeds in steam, and dried after picking the thorns.

주염나무의 어린 줄기와 잎, 열매, 씨에 알칼로이드가 있고 알칼로이드의 대부분은 트리아칸틴이고 아직 밝혀지지 않은 다른 하나의 알칼로이드가 들어 있으며, 알콜에 용해되나 물, 에테르, 벤졸에는 용해되지 않는다.The main stem has alkaloids on young stems, leaves, fruits, and seeds, and most of the alkaloids are triacanthin and another alkaloid that has not yet been identified. It is soluble in alcohol, but not in water, ether, or benzole.

알칼로이드 함량은 열매에서 0.12%, 꽃에서 0.11%, 잎에서 0.01~1.02%이며 잎에는 아스코르빈산, 목부에는 플라본 화합물인 푸스틴, 피세린, 몰리사카찌딘(로이코안로찌아니딘)이 들어있고, 새로운 카테콜로 알려졌던 글레디트신은 몰리사카찌딘이다.The alkaloid content is 0.12% in the fruit, 0.11% in the flower, and 0.01 ~ 1.02% in the leaf, and contains ascorbic acid in the leaves, and flavone compounds such as fustin, physerine, and molysaccharidine (roicoanrochianidine) in the neck. There is a new catechol, known as gleditsin, is molisacachidine.

열매에는 안트라퀴논 약 2~3%, 탄닌질, 열매 살에는 당분 약 20~30%가 있으며, 씨의 눈젖에는 만노갈락탄이 들어있다.The fruit contains about 2 to 3% of anthraquinone, tannins, and about 20 to 30% of sugar to the flesh of the fruit. Mannogalactan is contained in the milk of the seed.

씨는 라력, 종창, 종독의 피부질병, 가시는 항염증, 곪긴데, 부스럼, 피부암, 혀암에 효과가 있다고하며, 민간에서는 열매를 피부를 매끈하게 하는 욕탕료 또는 비누 대용으로 쓴 흔적이 남아있다.Seeds are said to be effective for skin diseases of rash, swelling, and poison, anti-inflammatory thorns, swelling, swelling, skin cancer, and tongue cancer. In the private sector, traces of fruit used as a bath or soap substitute to smooth the skin remain.

산모는 여러 해살이 풀로서, 뿌리와 줄기에 유리형 및 결합형의 크리소파놀, 에모딘, 옥시 메틸안트라키논인 루미찐, 크리소파네인, 크리소판산, 크리소파놀안트론, 탄닌질, 네포딘과 그 배당체 네포시드가 있다.The mother is a multi-year-old herb, free and bound chrysopanol, emodine, oxymethylanthrakinone, lumichin, chrysopanane, chrysopanic acid, chrysopanol anthrone, tannin, yes Podin and its glycoside neposide.

전초에는 산성 싱아산 칼리움 1.1%, 마른 잎에 아스코르빈산 750~1200mg이 들어있다. 잎에는 카페산, 몰식자산, 프로토 키테킨산, 클로로겐산, p-크마르산, 페를라산, 쿠에르쩨틴, 델피니딘, 찌아니딘, 루틴, 히페로시드, 철염, 루미찐이 들어있다.The outpost contains 1.1% of acid sodium kalium and 750-1200mg of ascorbic acid in dry leaves. The leaves contain caffeic acid, oleic acid, proto-chitenic acid, chlorogenic acid, p-xmaric acid, perlaic acid, querchentin, delphinidin, chiaanidine, rutin, hyperoside, iron salt, and lumichin.

뿌리 달임약은 설사, 적리, 장무력증, 위염에 먹으며 설사약, 오줌내기약, 땀내기약으로도 먹으며 전초는 신석류, 황달, 비타민 결핍증에 사용하고 피멋이약으로 장궁출혈, 열내림약으로 열병과 폐결핵약으로 쓰며, 잎즙은 아픔멋이약으로 류마치스 및 허리 아픔에 사용하고 뱀이나 벌레, 동물에 물렸을 때 해독약으로 사용하고 피부병·피부염증·옴·습진에도 효과가 있다.Root decoction is used for diarrhea, antagonism, intestinal ailment, gastritis, diarrhea, urinary medicine, and sweating medicine. Outpost is used for nephrite, jaundice, and vitamin deficiency. Used as a pulmonary tuberculosis drug, leaf juice is a pain-reducing drug, used for rheumatism and lower back pain, and is used as a detoxifying agent when bitten by snakes, insects, and animals, and is also effective for skin diseases, skin inflammation, scabies, and eczema.

위에서 설명한 천연 식물약재로서 뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무 및 산모는 피부질병의 예방 및 치유기능과 작용이 있는 천연 식물약재들이므로, 한꺼번에 1단계로 알콜 수용액으로 처리하여 추출액을 얻고 그 압착잔사를 2단계로 고압 고온수로 처리한 각 추출액을 혼합하여 혼합추출액을 농축한 혼합추출액을 얻는 방법이다.Mulberry mistletoe, pine ivy, Eoseongcho, elm tree, juniper tree, and mother are natural plant medicines that have the function of preventing and healing skin diseases and are treated with an aqueous alcohol solution in one step at a time. It is a method to obtain a mixed extract obtained by mixing each extract obtained by treating the compressed residue with high pressure and hot water in two stages and concentrating the mixed extract.

상기 식물약재들의 혼합추출농축액의 제조방법을 구체적으로 설명하면,When explaining in detail the method for producing the mixed extract concentrate of the plant drugs,

뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무, 산모 2.8:1:1:1:1:1의 비율중량으로 혼합한 천연 식물약재 100중량부와 30%의 에타놀 수용액 300중량부를 밀폐용기에 투입, 75~77℃로 유지시킨 상태에서 12~15시간 열처리하여 추출물을 얻고, 이 추출물을 압착하여 에타놀 수용액의 추출액과 1차 식물약재 잔사를 분리하고, 분리된 1차 식물약재 잔사에 잔사 중량의 3배의 물을 첨가, 온도 150~160℃로 유지된 밀폐 고압부에서 4~5시간 열처리하여 추출물을 얻고, 이 추출물을 압착하여 물 추출액과 2차 식물약재 잔사를 분리하고, 분리된 물 추출액을 상기 에타놀 수용액 추출액에 혼합하여 혼합추출액을 얻고, 이 혼합추출액을 온도 80℃로 유지시킨 상태에서 감압 농축하여 에타놀을 완전히 회수하고, 계속 가열하여 농축시키므로서 2~3포이즈의 식물약재 농축추출액을 제조한다.Mulberry mistletoe, pine ivy, Eoseongcho, elm, jum tree, maternal 2.8: 1: 1: 1: 1: 1 mixed in a ratio weight of 100 parts by weight of natural plant medicine and 300 parts by weight of 30% ethanol aqueous solution in a sealed container Input, heat-treated for 12 to 15 hours while maintaining at 75 to 77 ° C to obtain an extract, and the extract is squeezed to separate the extract of the ethanol solution and the primary plant medicine residue, and the weight of the residue in the separated primary plant medicine residue 3 times of water is added, heat-treated in a sealed high-pressure section maintained at a temperature of 150 to 160 ° C for 4 to 5 hours to obtain an extract, and the extract is squeezed to separate the water extract and the secondary plant medicine residue, and the separated water extract Is mixed with the ethanol aqueous solution extract to obtain a mixed extract, and concentrated under reduced pressure while maintaining the mixed extract at a temperature of 80 ° C to completely recover ethanol, and continues to heat and concentrate to concentrate 2 to 3 poise plant drugs. To produce a concentrated extract.

상기 농축된 농축추출액을 얻는 방법에 있어서, 에타놀 수용액의 온도를 77℃ 이상으로 하면 에타놀의 비점 이상의 온도가 되므로, 에타놀의 많은 량이 증발하므로 에타놀의 손실이 커지며 또한, 천연 식물약재들 중에는 알콜에 용해되는 성분과, 물에 용해되는 성분이 있고, 알콜 및 물 양측 모두에 용해되는 성분이 있으며, 고온의 물에 의해 용해되는 성분이 있고, 물과 알콜에 용해되지 않으나 아세트산(식초산) 또는 에텔에만 용해되는 성분도 있다. 그러나 공정의 난이성, 경제성, 유효특성 등 종합적인 여건을 고려할 때, 에타놀 수용액에서 추출하는 공정과 고압 고온의 물에서 추출하는 공정을 분리해서 추출하는 방법이 천연 식물약재로부터 유용한 약리적인 성분을 효율적으로 추출하는 방법이라 할 수 있다.In the method of obtaining the concentrated concentrated extract, when the temperature of the aqueous ethanol solution is 77 ° C or higher, the temperature becomes higher than the boiling point of ethanol, so a large amount of ethanol is evaporated, so the loss of ethanol increases, and among natural plant medicines, it is dissolved in alcohol. There are components that are soluble in water, components that are soluble in both alcohol and water, and components that are soluble in hot water, and are not soluble in water and alcohol, but only in acetic acid (vinegar) or ether Some ingredients are soluble. However, considering the overall conditions such as process difficulty, economic efficiency, and effective characteristics, the process of extracting from the ethanol solution and the process of extracting from high-pressure and high-temperature water separately extracts useful pharmacological ingredients from natural plant medicines efficiently. It can be said to be an extraction method.

항산화제는 레시친을 사용하며 아스코르빈산을 함께 사용하므로서, 시너지스트 항산화 효과를 얻을 수 있어 지방산을 주성분으로 하는 비누와 산화에 의한 산폐를 방지하므로서, 비누의 변질을 방지할 수 있고, 산폐에 의하여 발생되는 악취를 방지할 수 있으며, 피부에도 지속적으로 사용 시, 항산화 작용으로 피부의 노화진행을 지연시킬 수 있고, 또한 보존제로서 소르빈산(sorbic acid) 또는 그의 염류를 사용하고 이들의 방부제로서의 작용기작은 탈수소 효소계의 작용을 저해하고, 항균작용으로서 기작은 미생물포자의 발아와 성장과정을 억제하므로서, 미생물 생세포의 증식을 방지하게 되고, 미생물 세포 내 효소계 기능을 저해하므로서 정상적인 미생물 생육을 억제하게 된다.Antioxidants use lecithin and use ascorbic acid together, so that synergistic antioxidant effect can be obtained, preventing soap from acidic acid and acid oxidation, and preventing the deterioration of soap. It can prevent the generated odor, and when used continuously on the skin, it can delay the aging process of the skin due to its antioxidant action, and also uses sorbic acid or salts thereof as a preservative, and the mechanism of action as their preservative is dehydrogenation. By inhibiting the action of the enzyme system, the mechanism as an antibacterial action inhibits the germination and growth process of microbial spores, thereby preventing the proliferation of microbial live cells and inhibiting the normal microbial growth by inhibiting the enzyme system function in microbial cells.

또한 전술한 죽염 등의 용해도가 높은 성분을 함께 첨가하는 경우, 솔베이트(sorbate)의 용해도가 상대적으로 감소하고, water phase의 축적되는 양이 많으므로, 미생물에 대한 항균효과가 상승하며 항산화제와 함께 첨가하면 솔베이트의 항균효과가 상승하게 된다.In addition, when high-solubility components such as bamboo salt are added together, the solubility of sorbate decreases relatively and the amount of water phase accumulates, so the antimicrobial effect on microorganisms increases and antioxidants and When added together, the antibacterial effect of the sorbate increases.

본 발명의 구성을 보다 명확하게 하고 다기능성 미용비누의 효과를 알아보기 위해 실시예를 들기로 한다.In order to make the configuration of the present invention clearer and to find out the effect of multi-functional cosmetic soap, examples will be given.

본 발명 비누소지 86kg, 낙화생유, 올리브유, 알락토즈 발효액, 살리실산, 알로에발효액 및 손바닥선인장엑기스 각각 1kg, 소프넛, 알란토인 및 죽염 각각 0.5kg, 그리고 뽕나무 겨우살이, 어성초 담장이, 소나무 담장이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 30중량%의 알콜수용액으로 추출한 추출액과 그 추출액을 얻고 난 식물약재 잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출 농축액 5.5kg, 레시친 0.3kg, 아스코르빈산 0.3kg, 소르브산 0.2kg, 자스민향 0.2kg으로 조성한 다기능성 미용비누 조성물로 본 발명 다기능성 미용비누 제조방법에 따라 다기능성 미용비누를 제조하였다.Soap base 86kg, peanut oil, olive oil, alactose fermentation liquid, salicylic acid, aloe fermentation liquid and palm cactus extract 1kg, soapnut, allantoin and bamboo salt 0.5kg each, and mulberry mistletoe, fish vinegar fence, pine fence, elm, main leaf Extraction of extracted herbal extracts with 30% by weight of alcohol aqueous solution and the extracted herbal extracts with high temperature and high pressure water to obtain a mixed weight ratio of each of the trees and mothers to be 2: 1.5: 0.5: 0.5: 0.5: 0.5 Multifunctional cosmetic soap composition composed of mixed extract concentrate 5.5kg, lecithin 0.3kg, ascorbic acid 0.3kg, sorbic acid 0.2kg, and jasmine 0.2kg. Multifunctional beauty soap according to the present invention Soap was prepared.

실험예 1Experimental Example 1

본 발명 비누의 사용기간을 알아보기 위해 목욕탕A 및 B를 찾아가 종래 사용하는 비누의 사용하는 기간을 알아본 결과 3일을 사용하면 비누의 3/4이 닳아 버리고 1/4이 남게 되나 사용할 수 없는 상태로 된다고 하였다.In order to find out the period of use of the present invention, we went to bathrooms A and B and found out the period of use of the conventional soap. As a result, if 3 days are used, 3/4 of the soap will be worn out and 1/4 will remain, but cannot be used. It was said to be in a state.

실시예(1)에서 제조한 비누 100식을 A목욕탕과 B목욕탕에 주면서 사용할 수 있는 기간을 측정해 달라고 부탁하고 일주일 후 찾아가 결과를 알아본 결과 5일까지는 사용할 수 있다고 한다.It is said that 100 soaps prepared in Example (1) were given to A baths and B baths to measure the period of use, and after a week they went and checked the results.

실험예 2Experimental Example 2

여드름이 심하게 돋은 고등학교 남학생 10명을 대상으로 각자 실시예(1)에서 제조한 10개식의 비누를 제공하고 아침 저녁 2회에 걸쳐 세수 하도록 하고 20일 간격으로 치유 상태를 조사한 결과 다음 표(1)을 얻을 수 있었다.Ten high school boys with severe acne were provided with 10 soaps prepared in Example (1), and they were washed twice in the morning and evening, and the healing condition was examined every 20 days. The following table (1) Was able to get

여드름 실험결과표Acne test result table 기간경과구분\     Period elapsed classification\ 20일 후20 days later 40일 후40 days later 60일 후60 days later 80일 후80 days later 100일 후100 days later 학생 AStudent A 반응 없음no response 반응 없음no response 줄어듦Shrink 재발Relapse 재발Relapse 학생 BStudent B 줄어듦Shrink 더 줄어듦Less 없어짐Disappear 없어짐Disappear 없어짐Disappear 학생 CStudent C 반응 없음no response 반응 없음no response 반응 없음no response 줄어듦Shrink 없어짐Disappear 학생 DStudent D 좀 줄어듦Shrink 줄어듦Shrink 더 줄어듦Less 흔적만 있음Traces only 없어짐Disappear 학생 EStudent E 줄어듦Shrink 더 줄어듦Less 흔적만 있음Traces only 없어짐Disappear 없어짐Disappear 학생 FStudent F 반응 없음no response 반응 없음no response 반응 없음no response 조금 줄어듦Slightly reduced 재발Relapse 학생 GStudent G 반응 없음no response 반응 없음no response 반응 없음no response 반응 없음no response 반응 없음no response 학생 HStudent H 연락 두절Lost contact -- -- -- -- 학생 IStudent I 없어짐Disappear 없어짐Disappear 없어짐Disappear 없어짐Disappear 없어짐Disappear 학생 JStudent J 반응 없음no response 연락 두절Lost contact -- -- --

Claims (5)

기름야자나무의 야자 과육으로부터 얻은 과육팜유와 기름야자의 속에 있는 씨에서 짜낸 팜 핵유의 혼합중량비를 4:1~5:1로 혼합해서 된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 혼합유를 포화수용액의 가성소다와 반응시킨 반응물에 2중량%의 그리세린을 첨가해서 균질화시킨 비누소지 86중량%, 낙화생유, 올리브유, 갈라토즈 발효액, 살리실산, 알로에발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재를 30%의 알콜수용액으로 추출한 추출액과 추출액을 얻고 남은 압축잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출액을 농축시킨 2~3포이즈의 농축 혼합추출액 5.5중량%, 레시친 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물.
Mixing the weight ratio of palm oil obtained from the palm of the palm tree oil and palm kernel oil squeezed from seeds in the oil palm in a ratio of 4: 1 to 5: 1, and mixing palm oil and coconut oil in a weight ratio of 78: 6. 86% by weight of soap base homogenized by adding 2% by weight of griserin to the reactant reacted with caustic soda in saturated aqueous solution, 1% by weight of each of peanut oil, olive oil, galatose fermentation solution, salicylic acid, aloe fermentation solution and palm cactus, Soapnut, alatoin, and bamboo salt 0.5% by weight, respectively, and mulberry mistletoe, Eoseongcho, pine ivy, elm, oleander, and maternal mixed weight ratio of each of 2: 1.5: 0.5: 0.5: 0.5: 0.5 Concentrated mixed extract of 2 ~ 3 poise concentrated with the mixed extract obtained by mixing the extract extracted with 30% alcohol aqueous solution and the extracted liquid obtained by extracting the remaining compressed residue with high temperature and high pressure 5.5% by weight , Lecithin 0.3% by weight, 0.2% by weight of sorbic acid, 0.2% by weight of jasmine fragrance Multifunctional cosmetic soap composition.
기름 야자나무의 기름야자의 과육으로부터 얻어진 과육팜유와 씨로부터 얻어진 팜 핵유의 혼합중량비를 4:1~5:1로 해서된 혼합팜유와 코코넛유의 배합중량비를 78:6으로한 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 글리세린을 첨가하여 균질화시킨 비누소지를 얻는 1단계 공정;
1단계 공정에서 얻어진 비누소지 86중량% 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합된 천연식물약재의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물을 조성하는 2단계 공정;
상기 다기능성 미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 비누원료를 얻는 3단계 공정;
상기 비누 원료의 수소이온 농도를 유기산 또는 유기성 알카리로 PH6~7의 범위로 조절하는 4단계 공정; 및
PH를 조절한 비누원료를 온도 80~85℃로 유지시키면서 감압시킨 상태에서 수분함량 8~10%될때까지 열처리 한 다음 상온에서 3~4일간 숙성한 후 성형하는 5단계 공정으로 구성되는 다기능성 비누의 제조방법.
Caustic soda is a mixed plant oil with a blending weight ratio of 78: 6 mixed palm oil and coconut oil with a mixed weight ratio of pulp palm oil obtained from the pulp of an oil palm tree and palm kernel oil obtained from a seed of 4: 1 to 5: 1. A first step of obtaining a homogenized soap base by adding 2% by weight of glycerin to the reactant reacted with the saturated aqueous solution;
Soap base obtained in the first step process 86% by weight peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and palm cactus, respectively 1% by weight, soapnut, alatoin, and bamboo salt 0.5% by weight respectively, and mulberry mistletoe, eoseongcho, pine ivy Mixture extract concentrate of 5.5% by weight, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, so that the mixed weight ratio of each of the elm, elder, and mother trees is 2: 1.5: 0.5: 0.5: 0.5: 0.5 , Sorbic acid 0.2% by weight, a two-step process of forming a multifunctional cosmetic soap composition composed of 0.2% by weight of jasmine;
A three-step process of reacting for 1 hour in a state where the multifunctional cosmetic soap composition is heated to a temperature of 80 to 85 ° C and maintained while stirring to obtain a colloidal soap raw material;
A four-step process of adjusting the hydrogen ion concentration of the soap raw material to an organic acid or an organic alkali in a range of PH6 to 7; And
A multifunctional soap consisting of a 5-step process that heat-treats until the moisture content is 8-10% under reduced pressure while maintaining the pH-adjusted soap raw material at a temperature of 80-85 ° C, and then aged at room temperature for 3-4 days and then molded. Method of manufacturing.
청구항 제2항에 있어서,
상기 알로에발효액은 알로에 생잎을 썰어서 암실에서 온도 4~8℃오 유지하여 12~15일간 발효시켜 생물원 자극소가 생성된 알로에 발효액임을 특징으로 하는 다기능성 미용비누의 제조방법.
The method according to claim 2,
The aloe fermentation solution is a method of manufacturing a multifunctional cosmetic soap, characterized in that the aloe fermentation broth is produced by slicing fresh aloe leaves and fermenting for 12-15 days at a temperature of 4-8 ° C in the darkroom.
청구항 제2항에 있어서,
상기 천연식물약재의 혼합추출 농축액은, 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 천연식물약재 100중량부와 30%의 에타놀수용액 300중량부를 밀폐용기에 투입하고 온도 75~77℃로 유지시킨 상태에서 12~15시간 열처리하여 추출물을 얻고 이 추출물을 압착하며 에타놀 수용액의 추출액과 1차식물 약재 잔사를 분리하고 분리된 1차식물 약재 잔사에 잔사중량의 3배의 물을 첨가 온도 150~160℃로 유지된 밀폐 고압부에서 4~5시간 열처리하여 추출물을 얻고 이 추출물을 압착하여 물추출액과 2차 식물약재 잔사를 분리하고 분리된 물추출액을 상기에 타 놀 수용액 추출액에 혼합하여 혼합추출액을 얻고 이 혼합추출액을 온도 80℃로 유지시킨 상태에서 감압농축함과 동시에 에타놀을 회수하고 계속 가열하여 농축하여서된 2~3포이즈의 식물약재 혼합추출 농축액임을 특징으로 하는 다기능성 미용비누의 제조방법.
The method according to claim 2,
The mixed extract concentrate of the natural plant medicinal material is 100 weight of the natural plant medicinal material mixed so that the mixed weight ratio of each of the mulberry mistletoe, Eoseongcho, pine ivy, elm, oleander, and mother is 2: 1.5: 0.5: 0.5: 0.5: 0.5 300 parts by weight of ethanol and 30% of ethanol aqueous solution was put in a closed container and heat-treated for 12 to 15 hours while maintaining the temperature at 75 to 77 ° C to obtain an extract, and the extract was compressed to extract the extract of ethanol aqueous solution and the residue of the primary plant medicine. After separating and separating the primary plant medicinal residue, 3 times the weight of the residue is added, heat-treated in a sealed high-pressure section maintained at a temperature of 150 ~ 160 ℃ for 4 ~ 5 hours to obtain an extract, squeezing the extract to extract water and a secondary plant After separating the medicinal herb residue, the separated water extract was mixed with the above aqueous solution of ethanol to obtain a mixed extract, and the mixture was concentrated under reduced pressure while maintaining the temperature at 80 ° C. And recovering the production method of the functional beauty soap, it characterized in that the heating continued concentrated hayeoseo a medicinal plant mixed extract concentrate of 2-3 poise to.
기름야자나무의 과육팜유와 핵팜유의 혼합비를 2:1~3:1로 혼합해서 된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 식물혼합유를 트리에타놀아민 포화수용액과 반응시킨 반응물에 2중량%의 그리세린을 첨가 균질화시켜 다기능성 크림비누소지를 얻는 1단계 공정;
크림비누소지 86중량%, 낙화생유, 올리브유, 갈라토즈 발효액, 살리실산, 알로에발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모의 혼합중량비를 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합된 천연식물약재의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 크림미용비누 조성물을 조성하는 2단계 공정;
다기능성 크림비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 크림미용비누 원료를 얻는 3단계 공정;
교질상 크림비누 원료의 수소이온 농도를 유기산 또는 유기성 알카리로 PH6~7의 범위로 조절하는 4단계 공정; 및
PH를 조절한 비누원료를 온도 80~85℃로 유지시킨 상태에서 감압처리하여 수분함량 60~65%될때까지 열처리 한 후 상온에서 냉각시켜 3~4일간 숙성 안정화 시키는 5단계 공정으로 구성되는 다기능성 크림비누의 제조방법.
To the reactants reacted with saturated palm oil and palm oil palm oil and palm oil of 2: 2 to 3: 1 mixture of palm oil and coconut oil mixed plant ratio of 78: 6 with triethanolamine saturated aqueous solution A first step process to obtain a multifunctional cream soap base by homogenizing the addition of 2% by weight of griserin;
86% by weight of cream soap, 1% by weight of peanut oil, olive oil, fermentation solution of saliva, fermented salicylic acid, aloe fermentation and palm cactus, 0.5% by weight of soap, alatoin and bamboo salt, respectively, and mulberry mistletoe, eoseongcho, pine ivy, and elm , Mixed extract concentrate of natural plant medicinal herbs mixed so that the mixed weight ratio of main leaves and mothers is 2: 1.5: 0.5: 0.5: 0.5: 0.5 5.5% by weight, lecithin 0.3% by weight, ascorbic acid 0.3% by weight, sorbic acid 0.2 A two-step process of forming a multifunctional cream beauty soap composition composed of weight% and jasmine fragrance 0.2% by weight;
A three-step process of reacting for 1 hour while maintaining the temperature of the multifunctional cream soap composition heated to 80-85 ° C while stirring to obtain a creamy beauty soap raw material in colloidal form;
Four-step process of adjusting the hydrogen ion concentration of the cream soap raw material in the range of PH6 ~ 7 with organic acid or organic alkali; And
Multi-functionality consisting of a 5-step process that stabilizes aging for 3-4 days by heating at room temperature after heat treatment until the moisture content is 60-65% by depressurizing while maintaining the PH-adjusted soap raw material at a temperature of 80-85 ℃. Cream soap manufacturing method.
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