KR102166300B1 - The Beauty art-soap of The composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it. - Google Patents
The Beauty art-soap of The composition of beauty art-soap having multi-fuction and the method of preparing the beauty art-soap of multi-function using it. Download PDFInfo
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- KR102166300B1 KR102166300B1 KR1020190046462A KR20190046462A KR102166300B1 KR 102166300 B1 KR102166300 B1 KR 102166300B1 KR 1020190046462 A KR1020190046462 A KR 1020190046462A KR 20190046462 A KR20190046462 A KR 20190046462A KR 102166300 B1 KR102166300 B1 KR 102166300B1
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Classifications
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- C—CHEMISTRY; METALLURGY
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P19/00—Drugs for skeletal disorders
- A61P19/08—Drugs for skeletal disorders for bone diseases, e.g. rachitism, Paget's disease
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/02—Boiling soap; Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/10—Mixing; Kneading
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/26—Drying
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
Abstract
기름야자나무의 야자의 과육에서 얻은 과육팜유와 씨에서 얻은 팜 핵유를 비누 마모가 적은 비율로 혼합한 혼합팜유와 코코넛유의 혼합비율을 78:6으로해서 된 식물혼합유를 포화수용액의 가성소다와 반응시킨 반응물에 2중량%의 글리세린을 첨가해서 된 비누소지 86중량% 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합해서 된 식물약재들을 30%의 에타놀 수용액으로 추출한 추출액과 이 추출액과 분리된 식물약재 압착잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물과 그 조성물을 이용한 다기능성 미용비누의 제조방법에 관한 것이다.Mixed palm oil obtained from the pulp of the palm of the oil palm tree and palm kernel oil obtained from the seeds are mixed in a ratio of less abrasion of soap, and a plant mixture with a mixture ratio of 78:6 with caustic soda in a saturated aqueous solution. 86% by weight of soap, prepared by adding 2% by weight of glycerin to the reacted product, 1% by weight each of peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth, and opuntia cactus, 0.5% by weight each of soapnut, allatoin and bamboo salt And the extract obtained by mixing the plant medicinal materials obtained by mixing so that the weight ratio of mulberry mistletoe, Eoseongcho, pine ivy, aralia, main leaf tree, and mother is 2:1.5:0.5:0.5:0.5:0.5 with 30% ethanol aqueous solution and this extract A mixture of 5.5% by weight of a mixed extract concentrate obtained by mixing the extract obtained by extracting the compressed residue of the plant medicinal material separated with high temperature and high pressure water, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, 0.2% by weight of jasmine flavor. It relates to a multifunctional cosmetic soap composition and a method of manufacturing a multifunctional cosmetic soap using the composition.
Description
본 발명은 다기능성 미용비누 조성물 및 그 조성물을 이용한 다기능성 비누의 제조 방법에 관한 것으로, 구체적으로는 기름야자나무(Elaeis guineensis)의 야자과육을 증기로 쪄서 지방분해효소를 불활성화 시킨 다음 압착해서 얻어진 과육팜유와 기름야자 속에 있는 씨앗에서 짜낸 팜핵유를 일정비율로 혼합해서된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로 한 혼합유를 포화수용액의 가성소다와 반응시킨 반응물에 2중량%의 글리세린이 첨가된 비누소지 86중량%, 낙화생유 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5 되도록 혼합한 식물약재를 30%의 알콜 수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물과 그 조성물을 이용한 다기능성 미용비누의 제조방법에 관한 것이다.The present invention relates to a multifunctional cosmetic soap composition and a method for producing a multifunctional soap using the composition, and specifically, the palm meat of Elaeis guineensis is steamed with steam to inactivate lipolytic enzyme and then compressed. 2% by weight of a mixed oil obtained by mixing the obtained pulp palm oil and palm kernel oil squeezed from the seeds in the oil palm at a certain ratio, and the mixture weight ratio of the mixed palm oil and coconut oil being 78:6, reacted with caustic soda in a saturated aqueous solution. 86% by weight of soap with glycerin added, peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution and 1% by weight of opuntia cactus, each 0.5% by weight of soft nut, allatoin and bamboo salt, and mulberry mistletoe, Eoseongcho, pine ivy, The extract obtained by extracting the plant medicinal material mixed so that the weight ratio of each of the Araliaceae trees, the main leaf tree and the mother is 2:1.5:0.5:0.5:0.5:0.5 with a 30% aqueous alcohol solution, and the compressed residue of the plant medicine with high temperature and high pressure water A multifunctional beauty soap composition composed of 5.5% by weight of mixed mixed extract concentrate, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine flavor, and a multifunctional beauty soap using the composition It relates to a manufacturing method.
오래전부터 비누는 세수, 세안이나 목욕 시, 피부의 각질 노폐물 및 때와 같은 이물질을 제거하거나 직물지로 된 의류나 이불세탁을 위한 세정제로서 기본적으로 요구되는 기능은 세정력이라 할 수 있다.From a long time, soap has been used as a cleaning agent for washing, washing, or bathing, removing dead skin impurities and grime from the skin, or washing clothes or blankets made of fabric.
그러나 근년에 이르러 경제 성장과 더불어 삶의 질이 향상됨에 따라, 미용에 대한 관심도가 지나치게 높아지고, 이에따라 성형수술을 비롯하여 주름제거를 위한 시술과 피부관리를 위한 고급 화장품, 피부 영양제 구입에 주저하지 않으며 피부와 관련된 비누에 있어서도 탄력성의 피부, 피부의 노화방지, 피부질환의 예방 및 방지 등의 다기능성을 갖는 비누를 선호하고 있다.However, in recent years, as the quality of life improves along with economic growth, interest in beauty has increased excessively. Accordingly, we do not hesitate to purchase cosmetic surgery, wrinkle removal procedures, high-quality cosmetics for skin care, and skin nutrients. As for soaps related to related products, soaps with multifunctional properties such as elastic skin, skin aging prevention, and skin disease prevention and prevention are preferred.
종래의 비누에 첨가되는 미용제의 예로서, 미국특허 제4.335.125호에 개재된 케토코나졸 및 이트라코나졸 등은 칸디나 피부사상균에 의한 백선(무좀), 지루성 피부염, 전풍 등에 사용하는 항진균제로서, 심재성 진균증 및 표재성 진균증에 유효한 것으로 알려져 있고, 국내특허공개 제90-1790호에는 국소투여에 의한 진균성 피부질환 치료에 적합한 약학적 조성물로서, 용액제, 페이스트제, 연고제의 조성물 및 화장품류인 스킨, 밀크로션 등의 조성물제제가 소개되고 있다. 이와 같은 화학합성제제들은 장기간 경구투여하면 간독성과 위장장애 등의 부작용이 발생하며, 많은 항진균제제들이 일반적으로 비극성물질로서 물이나 극성용매에는 녹지않는 문제점이 있다.As examples of cosmetic agents added to conventional soaps, ketoconazole and itraconazole disclosed in U.S. Patent No.4.335.125 are antifungal agents used for ringworm (athlete's foot), seborrheic dermatitis, and epidemic diseases caused by candina skin bacterium. And it is known to be effective against superficial mycosis, and Korean Patent Publication No. 90-1790 discloses that as a pharmaceutical composition suitable for the treatment of fungal skin diseases by topical administration, the composition of solutions, pastes, ointments, and cosmetics such as skin and milk lotion. Composition formulations such as, etc. are introduced. If such chemically synthesized preparations are administered orally for a long period of time, side effects such as liver toxicity and gastrointestinal disorders occur, and many antifungal agents are generally non-polar substances and are not soluble in water or polar solvents.
이상과 같은 화학합성제를 첨가한 미용제들의 문제점들로 최근에는 쳔연물질을 첨가한 미용제를 선호하는 경향으로 나타나, 천연재료를 이용한 미용제들도 함께 연구개발되어 출시되는 제품이 있으며, 이와 같은 종래 미용제들의 예를들면, 국내등록특허공보 등록번호 제446542호에는 "홍삼허브 비누의 제조방법"에 관한 기술이 소개되고 있다. 기술의 내용인즉, 물 13%을 함유하는 코코넛유, 팜유의 식물성유지 80.38%의 조성비로, 80℃로 용해시키고 이 혼합물에 유성성분인 스쿠알렌, 알로에, 토코페롤, 조조바오일 1.42%를 혼합하여 자연상태로 숙성시키며, 숙성된 혼합물에 에탄올로 추출한 홍삼농축액 12.5% 첨가한 혼합물을 65℃까지 가열하여 진공상태에서 배합한 배합물에 참깨오일, 허브에센스오일 5.7%를 투입하여 -65℃로 급냉시키고, 진공압으로 인출하여 성형비누를 제조하는 기술이라 할 수 있으나, 알카리와의 금화반응 없이 주원료인 각종 지방산유지 그리고 그밖에 첨가되는 유동성의 지방산오일을 고형화시키기 어려우므로 재형성이 문제될 수 있고, 비누로서 사용할 수 있는 강도를 유지하기 곤란한 비누라 할 수 있다.Due to the problems of cosmetic agents added with chemical synthesis agents as described above, recently, there has been a tendency to prefer cosmetic agents added with chemical substances, and cosmetic agents using natural ingredients are also researched and developed and released. As an example of the same conventional cosmetic agents, a technique related to a "method of manufacturing red ginseng herb soap" is introduced in Korean Patent Publication No. 446542. In other words, in the composition ratio of 80.38% of vegetable oil of coconut oil and palm oil containing 13% of water, it is dissolved at 80℃, and the oily components of squalene, aloe, tocopherol, and jojoba oil 1.42% are mixed in this mixture in a natural state. The mixture containing 12.5% of the red ginseng concentrate extracted with ethanol was added to the aged mixture, heated to 65℃, and 5.7% of sesame oil and herbal essence oil were added to the mixture in a vacuum state, and then quenched to -65℃. It can be said that it is a technology to manufacture shaping soap by pneumatic extraction, but it is difficult to solidify various fatty acid oils, which are the main raw materials, and other fluid fatty oils without gold reaction with alkali, so reformation may be a problem and can be used as soap. It can be said that it is difficult to maintain the strength as possible.
다른 종래 예로서 국내특허공보(등록번호 제743830호)에 "화장비누 조성물"이 소개되고 있으며 기술의 구성은 세정성분으로서 음이온 계면활성제를 포함하는 비누에 있어서, 4급 암모늄 양이온 계면활성제를 포함하는 화장비누 조성물에 관한 것으로, 세정력 및 피부의 보습력은 기대할 수 있는 비누라 할 수 있으나, 피부를 보호하는 작용이나 항균작용 약리적인 기능 등은 기대할 수 없는 비누라 하겠다.As another conventional example, the "Fire composition" is introduced in Korean Patent Publication (Registration No. 743830), and the composition of the technology is in soap containing anionic surfactant as a cleaning component, including quaternary ammonium cationic surfactant. Regarding a cosmetic soap composition, it can be said that soap can be expected for cleansing power and moisturizing power of the skin, but it is a soap that cannot be expected for its protective action or antibacterial action and pharmacological function.
수중에서 쉽게 팽윤되거나 풀어지지 않는 단단한 비누를 얻을 수 있고, 대장균, 티프스균, 파라티스프균, 적라균, 비병원성 곰팡이는 물론 백선균 무좀균, 포도상균, 림균, 항산성세균에 대해 강력한 항균작용이 있어 각종 질병을 예방할 수 있고, 피부병, 피부염증, 옴, 습진, 피부암 등 각종 피부병의 예방 및 치료효과가 있으며 항산화작용에 의한 항산화 시너지스트 효과로 피부의 노화를 지연시킬 수 있는 다기능성 비누 조성물과 이 조성물을 이용한 다기능성 비누의 제조방법을 제공함에 있다.You can obtain a hard soap that does not swell or loosen easily in water, and it has strong antibacterial action against E. coli, Typhos bacteria, Paratyps bacteria, red larvae, non-pathogenic fungi, as well as Typhoid fungus, Staphylococcus aureus, Lymphobacteria, and acidic bacteria. It can prevent various diseases, has the effect of preventing and treating various skin diseases such as skin diseases, skin inflammation, scabies, eczema, and skin cancer, and is a multifunctional soap composition that can delay skin aging through antioxidant synergistic effects. To provide a method of manufacturing a multifunctional soap using the composition.
기름야자나무(Elaeis guineensis)의 야자과육에서 얻은 과육팜유와 씨앗에서 얻은 핵팜유의 중량비율을 4:1~5:1로한 혼합팜유와 코코넛유의 혼합비를 78:6으로 해서된 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 글리세린을 첨가시킨 비누소지 86중량%에 낙화생유 올리브유 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5 되도록 혼합한 천연식물약재를 알콜 수용액으로 추출한 추출액과 천연 식물약재의 압착잔사를 고온고압수로 추출한 추출액을 혼합한 식물약재 혼합추출액을 농축시킨 0.2~0.3포이즈의 식물약재 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물 및 아래와 같이 그 조성물을 이용한 다기능성 미용비누의 제조방법을 제공함으로서 본 발명 과제를 해결할 수 있었다.Caustic soda is a mixed vegetable oil in which the weight ratio of the palm oil obtained from the palm of the oil palm tree (Elaeis guineensis) and the nuclear palm oil obtained from the seeds is 4:1-5:1, and the mixing ratio of the palm oil and coconut oil is 78:6. 1% by weight of fermented peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth, and opuntia cactus, respectively, 0.5% by weight of soap nut, allatoin, and bamboo salt to 86% by weight of soap containing 2% by weight of glycerin added to the reaction product reacted with saturated aqueous solution % And natural plant medicinal materials mixed so that the weight ratio of each of mulberry mistletoe, Eoseongcho, pine ivy, aralia, main leaf tree and mother is 2:1.5:0.5:0.5:0.5:0.5, extracted with an alcoholic aqueous solution, and natural plant medicinal materials. 5.5% by weight of mixed extract concentrate of plant medicinal herbs of 0.2 to 0.3 poise, which was obtained by concentrating the mixed extract of plant medicines obtained by mixing the extract obtained by extracting the residue with high temperature and high pressure water, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, It was possible to solve the present invention by providing a multifunctional beauty soap composition composed of 0.2% by weight of jasmine fragrance and a method of manufacturing a multifunctional beauty soap using the composition as follows.
상기 다기능성 미용비누 조성물을 이용한 다기능성 비누의 제조방법은 기름야자나무(Elaeis guineensis Jacq)의 야자과육에서 얻은 과육팜유와 씨에서 얻은 핵팜유의 혼합중량비율을 4:1~5:1로한 혼합팜유와 코코넛유 혼합비를 78:6으로 해서된 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 그리세린을 첨가 균질화시켜 비누소지를 얻는 1단계 공정;The manufacturing method of the multifunctional soap using the multifunctional beauty soap composition is a mixture in which the weight ratio of the mixture of the pulp palm oil obtained from the palm flesh of the oil palm tree (Elaeis guineensis Jacq) and the nuclear palm oil obtained from the seeds is 4:1-5:1 A step 1 step of obtaining a soap base by adding and homogenizing 2% by weight of greaserin to a reaction product obtained by reacting a mixture of palm oil and coconut oil in a mixture ratio of 78:6 with a saturated aqueous caustic soda solution;
상기 비누소지 86중량%, 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알란토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무담쟁이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 알콜수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압수로 추출한 추출액을 혼합한 혼합 추출액을 0.2~0.3 포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민 0.2중량%로 다기능성 미용비누 조성물을 조성하는 2단계 공정;86% by weight of the soap base, peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution, and 1% by weight of opuntia cactus, each 0.5% by weight of soft nut, allantoin and bamboo salt, and mulberry mistletoe, Eoseongcho, pine ivy, aralia, A mixed extract obtained by mixing the extract obtained by extracting the mixed plant medicines with an alcoholic aqueous solution so that the mixing weight ratio of each of the main leaves and mothers was 2:1.5:0.5:0.5:0.5:0.5 and the extract obtained by extracting the compressed residue of the plant medicine with high temperature and high pressure water A two-step process of forming a multifunctional cosmetic soap composition with 5.5% by weight of mixed extract concentrate of 0.2-0.3 poise, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine;
상기 다기능성 미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 비누원료를 얻는 3단계 공정;A three-step process of obtaining a colloidal soap raw material by reacting for 1 hour while stirring the multifunctional cosmetic soap composition and maintaining the temperature up to 80 to 85°C;
상기 비누 원료의 수소이온 농도(PH)를 유기산 또는 유기알카리로 PH6~7범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the soap raw material to a pH range of 6 to 7 with an organic acid or an organic alkali; And
PH를 조절한 비누원료를 온도 80~85℃로 유지시켜 감압시킨 상태에서 열처리하여 수분함량 8~10중량% 건조시킨 후 3~4일간 숙성 안정화시킨 다음 성형하는 5단계 공정으로 구성되는 다기능성 비누의 제조방법이다.Multifunctional soap consisting of a 5-step process of aging and stabilizing for 3 to 4 days after heat treatment in a state where the pH-adjusted soap raw material is maintained at 80-85°C and reduced pressure, dried by 8-10% by weight, and then stabilized for 3-4 days. It is a manufacturing method of.
본 발명 다기능성 미용비누 조성물 및 그 조성물을 이용한 다기능성 미용비누의 제조방법으로 얻어진 비누는 물에 쉽게 용해되거나, 팽윤되지 않는 내마모성의 단단한 비누로 오래 사용할 수 있는 잇점이 있고, 우수한 항균성, 항바이러스성, 항염증 및 살균작용이 있어 피부질병의 예방은 물론 각종 염증, 부스럼, 가려움증, 아토피성 피부질환, 옴, 습진, 무좀, 검버섯, 주근깨, 기미, 백선, 피부암 치유효과가 있고 항산화 시너지스트 효과로 지속적으로 사용 시, 피부의 노화 진행을 지연시킬 수 있고 항산화제 및 보존재로 비누변질을 방지할 수 있는 다기능성 미용비누 조성물 및 그 비누 조성물을 이용한 다기능성 미용비누라 할 수 있다.The soap obtained by the multifunctional beauty soap composition of the present invention and the method of manufacturing a multifunctional beauty soap using the composition has the advantage that it can be used for a long time as a wear-resistant hard soap that does not easily dissolve or swell in water, and has excellent antibacterial properties and antiviral properties. As it has sex, anti-inflammatory and bactericidal effects, it prevents skin diseases, as well as various inflammations, swelling, itching, atopic skin diseases, scabies, eczema, athlete's foot, age spots, freckles, melasma, ringworm, and skin cancer healing effects, and has antioxidant synergistic effects. When used continuously, it can be said to be a multifunctional beauty soap composition that can delay the progression of aging of the skin and prevent soap deterioration with antioxidants and preservatives, and a multifunctional beauty soap using the soap composition.
본 발명 다기능성 비누 조성물 및 그 조성물을 이용한 다기능성 비누의 제조방법에 관한 것으로 이를 구체적으로 설명하면 본 발명 다기능성 미용비누 조성물을 기름야자나무(Elaeis guineensis Jacq)의 기름야자 과육에서 얻은 과육팜유와 씨로부터 얻은 핵팜유의 혼합중량비율을 4:1~5:1로 혼합한 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 혼합식물유를 가성소다 포화수용액과 반응시킨 반응물에 2중량%의 글리세린을 첨가하여 균질화시킨 비누소지 86중량%에 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비로 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 천연식물약재 100중량부를 30%의 에타놀 수용액으로 추출한 추출액과 그 식물약재 압착잔사를 고온고압 수용액으로 추출한 추출액을 혼합한 2~3포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물에 관한 것이며 그 조성물을 이용한 다기능성 미용비누의 제조방법은 기름야자의 과육팜유와 씨앗에서 짜낸 핵팜유의 혼합중량비를 4:1~5:1로 혼합해서된 혼합팜유와 코코넛유의 배합중량비를 78:6의 혼합식물유를 가성소다 포화수용액과 반응시킨 2중량%의 글리세린을 첨가해서 균질화시킨 비누소지를 얻는 1단계 공정; The present invention relates to a multifunctional soap composition and a method for producing a multifunctional soap using the composition. The multifunctional cosmetic soap composition of the present invention is prepared from the pulp palm oil obtained from the oil palm flesh of the oil palm tree (Elaeis guineensis Jacq). 2% by weight of glycerin in the reaction product obtained by reacting a mixed vegetable oil with a mixed weight ratio of mixed palm oil and coconut oil of 78:6 in which the mixed weight ratio of heuk palm oil obtained from seeds was mixed with a saturated aqueous solution of caustic soda To 86% by weight of the soap body homogenized by adding peanut oil, olive oil, galactose fermentation broth, salicylic acid, aloe fermentation broth and opuntia cactus 1% by weight each, soapnut, allatoin and bamboo salt 0.5% by weight each, and mulberry mistletoe, Eoseongcho, pine The extract obtained by extracting 100 parts by weight of natural plant medicinal materials mixed in a ratio of 2:1.5:0.5:0.5:0.5:0.5 to each weight ratio of ivy, aralia, locust tree and mother with 30% ethanol aqueous solution and the compressed residue of the plant medicinal material at high temperature Multifunctional cosmetic soap composed of 5.5% by weight of mixed extract concentrate of 2 to 3 poises, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine fragrance The composition is related to the composition, and the method of manufacturing a multifunctional beauty soap using the composition is the mixing weight ratio of the mixed palm oil and coconut oil obtained by mixing the mixture weight ratio of the pulp palm oil of the oil palm and the nuclear palm oil squeezed from the seeds at 4:1-5:1. A one-step process of obtaining a homogenized soap base by adding 2% by weight of glycerin by reacting the mixed vegetable oil of 78:6 with a saturated aqueous caustic soda solution;
상기 비누소지 86중량% 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에 발효액 및 손바닥 선인장 각각 1중량%, 소프넛, 알라토인 및 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무 담쟁이, 두릅나무, 주엽나무 및 산모 각각의 중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 알콜 수용액으로 추출한 추출액과 식물약재의 추출잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출액을 농축하여 얻은 2~3포이즈의 혼합추출 농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 미용비누 조성물을 조성하는 2단계 공정;The soap base 86% by weight of peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution, and 1% by weight of opuntia cactus, each 0.5% by weight of soft nut, allatoin and bamboo salt, and mulberry mistletoe, Eoseongcho, pine ivy, aralia, A mixed extract obtained by extracting the extract obtained by extracting the plant medicinal materials mixed so that the weight ratio of each of the medicinal plants and the mother is 2:1.5:0.5:0.5:0.5:0.5 with an aqueous alcohol solution and the extract obtained by extracting the extract residue of the plant medicinal material with high temperature and high pressure water. 2 to compose a multifunctional beauty soap composition comprising 5.5% by weight of mixed extract concentrate of 2 to 3 poise obtained by concentration, 0.3% by weight of lecithin, 0.3% by weight of ascorbic acid, 0.2% by weight of sorbic acid, and 0.2% by weight of jasmine flavor Step process;
상기 다기능성 미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 비누원료를 얻는 3단계 공정;A three-step process of obtaining a colloidal soap raw material by reacting for 1 hour while stirring the multifunctional cosmetic soap composition and maintaining the temperature up to 80 to 85°C;
상기 비누 원료의 수소이온 농도(PH)를 유기산 또는 유기알카리로 PH6~7범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the soap raw material to a pH range of 6 to 7 with an organic acid or an organic alkali; And
수소이온농도를 PH6~7로 조절한 비누원료를 온도 80~85℃로 유지시키면서 감압시킨 상태에서 수분함량 8~10중량%될때까지 건조시킨 후 3~4일간 숙성 안정화시킨후 성형하는 5단계 공정으로 구성되는 다기능성 비누의 제조방법이다.A five-step process of drying the soap raw material whose hydrogen ion concentration is adjusted to PH6~7 while maintaining the temperature at 80~85℃ until the moisture content reaches 8~10% by weight, and then aging and stabilizing for 3~4 days It is a manufacturing method of multifunctional soap consisting of.
상기 본 발명 미용비누 제조방법에 있어서, 다른 실시예로서, 혼합 식물유에 가성소다 대신 유기 알카리인 트리에타놀아민과 반응시켜 다기능성 미용 크림비누를 제조할 수 있으며 이를 구체적으로 설명하면 기름야자의 과육으로부터 얻은 과육팜유와 씨에서 얻은 핵팜유 혼합비를 2:1~3:1로 혼합해서된 혼합팜유와 코코넛유의 혼합중량비를 78:6으로한 식물혼합유를 트리에타놀아민 포화수용액과 반응시킨 반응물에 2중량%의 그리세린을 첨가 균질화시킨 다기능성 크림비누 소지를 얻는 1단계 공정;In the method for producing a cosmetic soap of the present invention, as another embodiment, a multifunctional cosmetic cream soap may be prepared by reacting a mixed vegetable oil with triethanolamine, an organic alkali instead of caustic soda. The mixture ratio of the obtained pulp palm oil and the nuclear palm oil obtained from the seeds is 2:1~3:1, and a mixture of plant oils obtained by mixing the mixed palm oil and coconut oil in a weight ratio of 78:6 is reacted with a saturated aqueous triethanolamine solution. A one-step process of obtaining a multifunctional cream soap base obtained by homogenizing the addition of grycerin by weight;
상기 크림비누소지 86중량%, 낙화생유, 올리브유, 갈락토즈발효액, 살리실산, 알로에발효액 및 손바닥선인장 각각 1중량%, 소프넛, 알란토인, 죽염 각각 0.5중량% 그리고 뽕나무 겨우살이, 어성초, 소나무담쟁이, 두릅나무, 주엽나무 및 산모의 혼합중량비를 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합된 천연식물약재의 추출농축액 5.5중량%, 레시친 0.3중량%, 아스코르빈산 0.3중량%, 소르브산 0.2중량%, 자스민향 0.2중량%로 조성되는 다기능성 크림미용비누 조성물을 조성하는 2단계 공정;86% by weight of the cream soap base, peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution and palm cactus each 1% by weight, softnut, allantoin, bamboo salt 0.5% by weight each, and mulberry mistletoe, Eoseongcho, pine ivy, aralia tree , 5.5% by weight of extract concentrate of natural plant medicinal materials mixed so that the mixed weight ratio of the main leaf tree and mother is 2:1.5:0.5:0.5:0.5:0.5, lecithin 0.3% by weight, ascorbic acid 0.3% by weight, sorbic acid 0.2% %, a two-step process of forming a multifunctional cream cosmetic soap composition comprising 0.2% by weight of jasmine flavor;
상기 다기능성 크림미용비누 조성물을 교반하면서 온도 80~85℃까지 승온하여 유지시킨 상태에서 1시간 반응시켜 교질상의 크림미용비누 원료를 얻는 3단계 공정;A three-step process for obtaining a gelatinous cream cosmetic soap raw material by reacting for 1 hour while stirring the multifunctional cream cosmetic soap composition while maintaining the temperature by raising the temperature to 80 to 85°C;
상기 교질상 크림미용비누 원료의 수소이온 농도(PH)를 유기산, 유기알카리로 PH6~7의 범위로 조절하는 4단계 공정; 및A four-step process of adjusting the hydrogen ion concentration (PH) of the raw material for the gelatinous cream cosmetic soap in the range of PH6 to 7 with an organic acid and an organic alkali; And
PH를 조절한 크림미용비누 원료를 온도 80~85℃로 유지시킨 상태에서 감압처리하여 수분함량 60~65중량%될때까지 열처리한 후 냉각시킨 후 3~4일간 숙성 안정화시키는 5단계 공정으로 구성되는 다기능성 크림미용비누 제조방법이라 할 수 있다.It consists of a 5-step process in which the ingredients of the cream cosmetic soap with adjusted PH are treated under reduced pressure while maintaining the temperature at 80~85℃, heat treated until the moisture content reaches 60~65% by weight, cooled, and stabilized for 3~4 days. It can be said to be a manufacturing method of multifunctional cream and beauty soap.
상기 본 발명 비누소지 원료로 사용하고 있는 기름야자나무(Elaeis guineensis Jacq)의 기름야자의 열매에 24~34%, 열매살에 50~67%, 속씨에 50~55%의 기름이 있으며 기름을 구성하고 있는 지방산은 팔미틴산 40%, 올레인산 45%, 스테아린산 3.6%, 리놀산 8%, 미스트린산 3.6%로 이루어져 있고 기름에는 0.06%카로틴이 있으며 열매의 과육을 과열수증기로 쪄서 지방분해 효소를 비활성화시킴과 동시에 단백질을 응고시키고 압착하여 기름을 얻게 되는데 이를 과육팜유라 하고 열매 속씨를 압착하여 얻어진 기름을 핵팜유라고 하며 과육(열매살)팜유와 핵팜유는 성분에서 큰 차이가 있고 과육팜유는 핵팜유에 비해 비누 사용시 물에서 쉽게 팽윤되거나 물러지지 않으므로 비누를 오래 사용할 수 있으며 반면 핵팜유는 항균 보습효과가 우수하고 과육팜유에 비해 고급유라 할 수 있다.The oil palm fruit of the oil palm tree (Elaeis guineensis Jacq) used as the raw material for the soap of the present invention contains 24 to 34%, 50 to 67% of the fruit flesh, and 50 to 55% of the oil in the inner seed. The fatty acids used are palmitic acid 40%, oleic acid 45%, stearic acid 3.6%, linoleic acid 8%, and mystrinic acid 3.6%, and there is 0.06% carotene in the oil, and the flesh of the fruit is steamed with superheated steam to inactivate the lipolytic enzyme. Protein is solidified and compressed to obtain oil. This is called pulp palm oil, and the oil obtained by pressing the seeds inside the fruit is called hack palm oil. There is a big difference in composition between pulp (fruit) palm oil and hack palm oil. When using soap, it does not easily swell or fade in water, so you can use soap for a long time. On the other hand, hemp palm oil has excellent antibacterial moisturizing effect and is a high-quality oil compared to pulp palm oil.
낙화생유는 성분으로 알카로이드 아미노산이 함유되어 있고 보습효과 아토피성 피부질환 땀띠 여드름 치유에 효과가 있고 항균 기능을 갖는 식물유이며 올리브유는 감람나무의 열매살에 50~70%, 씨에 20%기름을 함유하고 있으며 기름의 7~10%는 팔미틴, 2~4%는 스테아린, 20~84%는 올레인, 4~12%는 리놀레인을 함유하고 있으며 작용으로는 보습효과 가려움증해소 여드름진정, 항암효과가 있는 것으로 알려져 있다.Peanut oil contains alkaloid amino acids as an ingredient, moisturizing effect, and is effective in healing atopic skin diseases, heat spots, acne, and antibacterial. Olive oil contains 50-70% oil in the fruit flesh of olive trees and 20% oil in the seeds. 7~10% of the oil contains palmitine, 2~4% stearin, 20~84% olein, and 4~12% linolein. It has a moisturizing effect, relieves itching, soothes acne, and has anticancer effects. It is known to have.
갈락토즈 발효액은 생연초 추출물로서 부틸렌그리콜, 펜틸렌그리콜, 소디움벤죠이트가 함유되어 있고 작용으로는 항암효과가 있고 죽은깨, 기미, 검버섯제거 효과가 있는 것으로 알려져 있다.Galactose fermentation broth is a raw tobacco extract that contains butylene glycol, pentylene glycol, and sodium benzoate, and is known to have anti-cancer effects as well as dead sesame, spots and age spots.
알란토인은 방울풀의 잎과 씨에는 알리스톨톤, 알란토인(C4H6O3N4), 마그노플로린, 알칼로이드인 아리스톨로킨과 사포닌, 유기산, 탄닌질이 함유되어 있는데 알란토인 성분을 분리 추출한 추출액으로 여드름, 아토피성 알러지 염증에 효과가 있고 향균성이 우수하며 살리신산은 조팜나무 잎에 함유되어 있는 아스코르빈산 살리실산메틸 성분을 함유하고 있으며 이로부터 추출 분리한 쳔연의 살리실산으로 여드름을 진정시키고 피부미용, 습성습진에 효과가 있는 것으로 알려져 있다.Allantoin contains allantoin, allantoin (C 4 H 6 O 3 N 4 ), magnoflorin, alkaloids aristolokin, saponin, organic acids, and tannins in the leaves and seeds of bellflower. The extract obtained by separating allantoin components It is effective against acne and atopic allergic inflammation and has excellent antibacterial properties.Salicylic acid contains methyl salicylate of ascorbic acid contained in the leaves of the palm tree, and salicylic acid extracted and separated from it is used to calm acne and make skin beauty , It is known to be effective against wet eczema.
죽염은 대나무에 소금을 넣어 1500℃ 이상의 고온에서 3회 구운 죽염으로 미네랄성분이 풍부하며 가려움즘, 아토피성 피부염, 건선억제, 항균 및 방부효과가 있다.Bamboo salt is a bamboo salt that is baked three times at a high temperature of 1500℃ or higher by putting salt in bamboo. It is rich in minerals and has itchiness, atopic dermatitis, psoriasis suppression, antibacterial and antiseptic effects.
소퍼넛은 무환자나무의 열매살에 얻은 추출액으로 추출액에는 무환자사포닌(사핀두스 사포닌)이 다량 함유되어 있어 물과 만나면 다량의 거품이 발생하고 천연세제로 사용되며 종래 민간에서도 세척제 그리고 피부와 머리를 감는데 사용해온 것으로 작용으로는 얼굴의 죽은 깨, 몸에서 발산하는 냄새를 없애는데 효과가 있다.Soffernut is an extract obtained from the fruit flesh of a patient-free tree.The extract contains a large amount of patient-free saponin (saffindus saponin), so when it meets water, a large amount of foam is generated and is used as a natural detergent. It has been used to remove dead sesame seeds from the face and odor from the body.
알로에 속 식물은 약 170종이 있고, 잎은 살져있고 변두리에 가시가 있으며, 흰색, 노란색, 붉은색 꽃이 이삭처럼 모여 핀다. 열대지방에 자라는 것은 높이 4m이고, 잎의 길이는 65cm에 달하고, 알로에는 산지에 따라 기원식물이 다르며 케이프(cape)알로에, 나탈(nathal)알로에, 소코트린(socotrine)알로에, 잔지바르(zanzibar)알로에, 구라카오(curacao)알로에, 자파라바드(jaffarabad)알로에가 있고, 우리나라에는 긴 잎 알로에, 얼룩 잎 알로에, 넓은 잎 알로에가 있다. 알로에의(잎즙)에는 알로인 C20 H18 O9(알로에-에모딘-d-아라비노시드) 16~20%, 알로에-에모딘, 나탈로인, 라바르베론(이소에모딘), 수지 12%(알로레시탄놀 C22 H26 O6의 계파산에스테르)가 함유되어 있다. 알로에 잎즙 말린 것은 소화 및 식욕 항진약으로 사용하고 있고 알로에 생즙은 소량의 에타놀을 첨가 항균약으로 상처를 관장하거나, 썩는 염증부위를 씻는데 사용하며, 또한 본 발명에서 사용되는 알로에 생잎을 썰어서 암실에서 온도 4~8℃를 유지시켜 12~15일간 발효시킨 것은, 약해지는 생명활동을 자극하는 생물원 자극소라고 하는 물질이 생성되는데, 그 화학조성은 아직 밝혀지지 않았으나 대체로 지방족디카르본산, 분자량이 큰 방향족유기산으로 보고있으며 생물원자 극소라하는 생성물질을 환자의 면역기능을 향상시키며, 방사선 피해 시, 피부손상을 방지하는데 사용되고 상처, 화상피부와 점막 염증치료에 바르기도 하며 민간요법으로 피부암, 땀띠, 여드름 치유에 사용되고 있고 미용효과로서는 보습효과가 크다.There are about 170 species of plants in the genus Aloe, and the leaves are thin and have thorns at the edges, and white, yellow, and red flowers are gathered like spikelets. It grows in the tropics with a height of 4m and a leaf length of 65cm. Aloe has different origin plants depending on the production area. Cape aloe, nathal aloe, socotrine aloe, zanzibar aloe , Curacao aloe, jaffarabad aloe, and long leaf aloe, spot leaf aloe, and broad leaf aloe in Korea. In aloe (leaf juice), aloin C20 H18 O9 (Aloe-emodine-d-arabinoside) 16-20%, aloe-emodine, natalioin, labaveron (isoemodin), resin 12% ( It contains allolecitanol C22 H26 O6). Dried aloe leaf juice is used as a digestive and appetite suppressant, and fresh aloe juice is used to enema wounds with an antibacterial drug by adding a small amount of ethanol, or to wash rotting inflamed areas. Also, fresh aloe leaves used in the present invention are sliced and used in a dark room. Fermented for 12 to 15 days while maintaining a temperature of 4 to 8°C produces a substance called a biological source stimulator that stimulates weakening life activities, and its chemical composition is not yet known, but mostly aliphatic dicarboxylic acid and molecular weight It is regarded as a large aromatic organic acid, and it is used to improve patient's immune function and prevent skin damage in case of radiation damage. It is also applied to wounds, burns and inflammation of mucous membranes. It is a folk remedy for skin cancer and heat rash. , It is used for acne healing and has a great moisturizing effect as a cosmetic effect.
또한 손바닥선인장 진액은 무질소물로서 프라보노이드 성분이 함유되어 있고 악성피부염, 염증 치유에 효과가 있다.In addition, palm cactus essence is nitrogen-free, contains flavonoids, and is effective in healing malignant dermatitis and inflammation.
그 밖에 뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무 및 산모의 천연 식물약재들은 피부병에 대한 항균성을 가지거나 피부질병을 예방, 치유할 수 있는 천연 식물약재들로서 그 성분과 작용을 알아보면, 뽕나무 겨우살이의 잎이 붙은 가지에서 알칼로이드, 플라보노이드, 사포닌이 확인 되었으며, 또한 올레아놀산(C30 H48 O3), b-아미린(C10 H50 O), 메소이노시톨, 비스찐, 옥시다제, 세릴알콜, 미리스틴산, 아라킨, 고무질(점액), 페닐아민, 프로피오콜린, 아세틸콜린, 수지가 있다.In addition, mulberry mistletoe, pine ivy, Eoseongcho, Aralia, main salt, and mother's natural plant medicines are natural plant medicines that have antibacterial properties against skin diseases or can prevent and heal skin diseases. Alkaloids, flavonoids, and saponins were identified in the leaves of the mulberry mistletoe, and oleanolic acid (C30 H48 O3), b-amirin (C10 H50 O), mesoinositol, bistine, oxidase, seryl alcohol, myristic acid , Arachine, rubbery (mucous), phenylamine, propiocholine, acetylcholine, and resin.
구라파에서 자라는 겨우살이에는 흰 무정형 물질인 비스코톡신, 시린기린, 고무질과 수지가 들어 있으며, 비스코톡신은 3가지 물질 즉, 비스코톡신 A2, A3, B로 순수하게 분리되었으며 이 3 물질은 모두 46개 아미노산으로 이루어졌으나, 배열순서에서 다르다. 비스코톡신 A3은 유황을 가교로 한 연결이 3곳에 있고, 즉 16과 26번 사이 그리고 3과 40번, 4와 32번 사이에 유황연결이 있으며 이 펩티드는 항암활성이 있다. Mistletoe grown in Europe contains white amorphous substances such as biscotoxin, syringin, rubber and resin, and biscotoxins are purely separated into three substances, namely, biscotoxins A2, A3, and B. All three substances are 46 amino acids. It consists of, but is different in the order of arrangement. Biscotoxin A3 has sulfur-linked links at 3 locations, namely, between 16 and 26, and between 3 and 40, and 4 and 32, and this peptide has anticancer activity.
씨에는 응집소인 아그글루티닌이 있는데 미량에서 항암작용을 하며 여기에는 N-모노메틸리진이 0.10~0.25그람분자%, N-디메틸리진이 0.15~0.30그람분자%, N-트리메틸리진이 0.05~0.12그람분자%이 있으며 활성은 뒤의 것이 세다.Seeds contain agglutinin, an agglutinin, which has anticancer activity in trace amounts. N-monomethyl lysine contains 0.10 to 0.25 gram molecule%, N-dimethyllizine is 0.15 to 0.30 gram molecule%, and N-trimethyl lysine is 0.05~ There is 0.12 gram molecule%, and the activity is the second one.
또한 이 천연 식물약재는 11종의 항암활성 단백질이 분리되었으며, 이것들은 0.006~0.05mg/kg에서 암세포의 디핵산 합성을 억제하며, 항암 단백질이 약간이라도 변질되면 항암활성이 없어지며 4종의 단백질 성분은 센 항원성이 있는데, 10ug 아래에서 항체를 생산하고, 비스코톡신 A는 사르코마 180 암을 일으킨 흰 생쥐의 생존기간을 대조에 비하여 98%로 더 늘이였다.In addition, 11 kinds of anticancer active proteins were isolated from this natural plant medicine, and these inhibit the synthesis of dinucleic acid in cancer cells at 0.006~0.05mg/kg. If the anticancer protein is slightly altered, the anticancer activity disappears and 4 kinds of proteins The component has strong antigenicity, producing antibodies under 10 ug, and Biscotoxin A increased the survival time of white mice with Sarcoma 180 cancer to 98% compared to the control.
작용으로는 항균, 항바이러스, 항암 기능이 있다. 소나무 담쟁이의 줄기와 잎은 사포닌(용혈지수 100), 찌아니딘과 말비딘의 3.5-디글루코시드, 말비딘-3-글루코시드, 씨에 알카로이드가 있다. 종양 흡수약, 응종, 벤 상처, 피부 염증, 여드름 억제 효과가 있다.It has antibacterial, antiviral, and anticancer functions. The stems and leaves of pine ivy have saponins (hemolytic index 100), 3.5-diglucosides of zianidin and malvidin, malvidin-3-glucoside, alkaloids in seeds. It is effective in suppressing tumor absorbing drugs, clots, cuts, skin inflammation, and acne.
소나무담쟁이의 줄기와 잎에는 사포닌(용혈지수 100), 찌아니딘, 말비딘 3.5-디 글루코시드, 말비딘-3-글르코시드, 씨에는 알카로이드가 들어 있으며 작용으로는 종양흡수약으로 옹종치료에 사용하며 가려움증, 여드름 치료에 효능이 있고 피부미용에 효과적이다.The stems and leaves of pine ivy contain saponin (hemolysis index 100), tianidine, malvidin 3.5-diglucoside, malvidin-3-glucoside, and alkaloids in seeds. It is used to treat itching and acne, and is effective for skin care.
어성초의 생전초에는 정유가 함유되어 있다. 그 주성분은 메틸노닐케톤, 미르센, 라우린알데히드, 카프린알데히드, 카프르산이고 이 밖에도 기체 크로마토그래피에 의해 28개의 성분이 밝혀졌다.Eoseongcho's raw raw plants contain essential oils. Its main components are methylnonylketone, myrcene, laurinaldehyde, caprinaldehyde, and capric acid. In addition, 28 components were identified by gas chromatography.
이 식물의 비린내와 같은 불쾌한 냄새는 데카노일아세트알데히드와 라우릴알데히드에 의한 것으로, 이 성분은 신선한 어성초에만 들어있으며 100℃ 이상의 고온 처리시는 그의 변화 생성물인 메틸노닐케톤, 미르센, 카프르산이 있다.The unpleasant smell like the fishy smell of this plant is caused by decanoylacetaldehyde and laurylaldehyde, and this component is contained only in fresh fish vinegar. When treated at a high temperature of 100℃ or higher, the product of its change, methylnonylketone, myrcene, and capric acid have.
잎에는 쿠에르찌트린과 물에 용해되는 무기성분 2.7%가 들어있고 그의 주성분은 칼리움염이다. 꽃과 열매 이삭에는 쿠에르찌트린이 없고 이소쿠에르찌트린이 들어있다.The leaves contain quercitrin and 2.7% of an inorganic component soluble in water, and its main component is potassium salt. The ears of flowers and fruits do not contain quercitrin, but contain isoquerzitrin.
작용으로는 대장균, 티푸스균, 파라티푸스균, 적리균, 림균, 포도상균 및 사상균에 대한 항균작용이 있고, 데카노일아세트알데히드는 비병원성 곰팡이는 물론 백선균, 무좀균 등에 대한 항균작용이 있으며, 포도상균, 임균, 항산성세균에도 억균작용이 있고, 포도상균에 대한 항균력은 슬파민보다 훨씬 세다.As an action, it has an antibacterial action against Escherichia coli, typhus, paratyphobacteriaceae, red lychee, lymphis, staphylococcus aureus and filamentous fungi, and decanoylacetaldehyde has antibacterial action against non-pathogenic fungi, as well as tinea and athlete's foot, staphylococcus, gonococci, Anti-acid bacteria also have an antibacterial effect, and the antibacterial activity against staphylococcus is much stronger than that of sulfamin.
전초는 피부염증약, 무좀치루, 아토피, 여드름, 피부질환, 가려움증에 효과가 있다.Outpost is effective against skin inflammation drugs, athlete's foot fistula, atopy, acne, skin diseases, and itching.
두릅나무의 껍질에는 사포닌 배당체인 아랄로시드(타랄린)가 들어있다. 아랄로시드 A는 물 분해하면 올레아놀산과 포도당, 아라비노즈, 2분자의 글루쿠론산이 되고, 아랄로시드 B는 물 분해하면 올레놀산과 포도당, 아라비노즈, 2분자의 글루쿠론산이 되며 아랄로시드 C를 가수분해하면 올레아놀산과 포도당, 아라비노즈, 글루쿠론산, 갈락토즈가 되고 그 밖에 정유 0.05% 푸로토카테킨산, 콜린이 함유되어 있으며, 또한 알카로이드 반응에 양성인 물질도 있다.Araloside (taralline), a saponin glycoside, is contained in the bark of the aralia tree. Arloside A becomes oleanolic acid, glucose, arabinose, and two molecules of glucuronic acid when decomposed in water. Arloside B becomes oleanolic acid, glucose, arabinose, and two molecules of glucuronic acid when decomposed in water. When seed C is hydrolyzed, it becomes oleanolic acid, glucose, arabinose, glucuronic acid, and galactose, and other essential oils contain 0.05% furotocatechinic acid and choline, and some substances are positive for alkaloid reactions.
사포닌은 줄기보다 뿌리껍질에 많으며, 씨에는 약 5%의 기름이 있고 이 기름에는 페트로셀린산, 팔매틴산, 리놀산, 페트로셀리딘산이 있으며, 뿌리에는 스티그마스테린, 탄닌질, 꽃 이삭에는 크산틴, 구아닌, 어린 싹에는 로이진, 아스파라긴산, 글루타민산, 아스파라긴, 알라닌, 티로신, 히스티딘 등이 많다.Saponin is more in the root bark than in the stem, and the seeds contain about 5% of oil, and this oil contains petrocelic acid, palmatinic acid, linoleic acid, and petrosellidic acid, and stigmasterin, tannins in the roots, and xanthine in the ear of flowers. , Guanine, and young shoots are rich in roijin, aspartic acid, glutamic acid, asparagine, alanine, tyrosine, and histidine.
작용으로는 뿌리껍질의 물 또는 알콜 추출물은 흥분작용이 있으며, 메디날에 대한 길항작용과 함께 강심작용이 있다.As an action, the water or alcohol extract of the root bark has an excitatory action, and it has an antagonistic action against the median and a strong heart action.
또한 두릅나무 껍질의 약리작용 성분은 아랄로시드로서, 아랄로시드 조직의 산화환원 과정과 신상선 피질의 글루코코르티코이드 분비기능을 높이며, 유기체의 저항성과 백혈구의 탐식기능도 높히며, 잇발지지 조직층(치주층) 치료에도 좋은 효과가 있으며 그 밖에도 부종, 수종, 피부의 상처를 치유하는 효과가 있다.In addition, the pharmacological component of aralloside is arloside, which enhances the redox process of araloside tissue and the secretion of glucocorticoids in the renal gland cortex, increases the resistance of organisms and phagocytosis of leukocytes, and supports gum tissue layer ( Periodontal layer) has a good effect in treatment, and in addition, it has the effect of healing swelling, swelling, and skin wounds.
주염나무의 어린 잎에는 알칼로이드 함량이 높고, 열매는 조협이라 하여 가을에 따서 말린 것이고, 씨는 조협지라 하여 여문 씨를 증기에 쪄서 말린 것이며, 가시를 따서 말린 것을 조각자라 한다.The young leaves of the Juyeom tree have a high content of alkaloids, and the fruits are called Johyeop and are dried in autumn, the seeds are called Johyeopji, and the seeds are steamed and dried in steam.
주염나무의 어린 줄기와 잎, 열매, 씨에 알칼로이드가 있고 알칼로이드의 대부분은 트리아칸틴이고 아직 밝혀지지 않은 다른 하나의 알칼로이드가 들어 있으며, 알콜에 용해되나 물, 에테르, 벤졸에는 용해되지 않는다.There are alkaloids in the young stems, leaves, fruits and seeds of the main salt tree, and most of the alkaloids are triacantin and contain another alkaloid that has not been identified yet. It is soluble in alcohol but not in water, ether, and benzol.
알칼로이드 함량은 열매에서 0.12%, 꽃에서 0.11%, 잎에서 0.01~1.02%이며 잎에는 아스코르빈산, 목부에는 플라본 화합물인 푸스틴, 피세린, 몰리사카찌딘(로이코안로찌아니딘)이 들어있고, 새로운 카테콜로 알려졌던 글레디트신은 몰리사카찌딘이다.The alkaloid content is 0.12% in fruit, 0.11% in flowers, 0.01 to 1.02% in leaves, and ascorbic acid in leaves, and flavone compounds such as fustine, picerine, and molisaacchidin (leicoanthinidine) are contained in the neck. In addition, the new catechol, known as gleditcin, is molisaccazidine.
열매에는 안트라퀴논 약 2~3%, 탄닌질, 열매 살에는 당분 약 20~30%가 있으며, 씨의 눈젖에는 만노갈락탄이 들어있다.Fruit contains about 2~3% of anthraquinone, tannins, and about 20~30% of sugar in the flesh of the fruit, and mannogalactan is contained in the eyelids of seeds.
씨는 라력, 종창, 종독의 피부질병, 가시는 항염증, 곪긴데, 부스럼, 피부암, 혀암에 효과가 있다고하며, 민간에서는 열매를 피부를 매끈하게 하는 욕탕료 또는 비누 대용으로 쓴 흔적이 남아있다.Seeds are said to be effective against swelling, swelling, skin diseases of swelling, thorns, anti-inflammatory, festering, swelling, skin cancer, and tongue cancer, and in the private sector, traces of the use of fruit as a bath material to smooth the skin or as a substitute for soap remain.
산모는 여러 해살이 풀로서, 뿌리와 줄기에 유리형 및 결합형의 크리소파놀, 에모딘, 옥시 메틸안트라키논인 루미찐, 크리소파네인, 크리소판산, 크리소파놀안트론, 탄닌질, 네포딘과 그 배당체 네포시드가 있다.The mother is a variety of seaweeds, and the roots and stems are free and bound to chrysophanol, emidine, oxymethylanthraquinone, luminicin, chrysophanein, chrysophanoic acid, chrysophanolanthrone, tannins, yes. There are fodin and its glycoside neposide.
전초에는 산성 싱아산 칼리움 1.1%, 마른 잎에 아스코르빈산 750~1200mg이 들어있다. 잎에는 카페산, 몰식자산, 프로토 키테킨산, 클로로겐산, p-크마르산, 페를라산, 쿠에르쩨틴, 델피니딘, 찌아니딘, 루틴, 히페로시드, 철염, 루미찐이 들어있다.The outpost contains 1.1% of acidic potassium cyanide, and 750-1200mg of ascorbic acid in the dried leaves. Leaves contain caffeic acid, molar acid, protocythenic acid, chlorogenic acid, p-xmaric acid, perlaic acid, querzetin, delpinidine, ziidine, lutein, hyperoside, iron salt, and lumitin.
뿌리 달임약은 설사, 적리, 장무력증, 위염에 먹으며 설사약, 오줌내기약, 땀내기약으로도 먹으며 전초는 신석류, 황달, 비타민 결핍증에 사용하고 피멋이약으로 장궁출혈, 열내림약으로 열병과 폐결핵약으로 쓰며, 잎즙은 아픔멋이약으로 류마치스 및 허리 아픔에 사용하고 뱀이나 벌레, 동물에 물렸을 때 해독약으로 사용하고 피부병·피부염증·옴·습진에도 효과가 있다.Root decoction is eaten for diarrhea, red blood, intestinal weakness, gastritis, and is also used as diarrhea, peeing, and sweating. The outpost is used for kidney pomegranate, jaundice, and vitamin deficiency. It is used as a medicine for pulmonary tuberculosis, and leaf juice is used as a pain-moist medicine for rheumatism and back pain, and as an antidote for bites by snakes, insects, and animals, and is effective for skin diseases, skin inflammation, scabies and eczema.
위에서 설명한 천연 식물약재로서 뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무 및 산모는 피부질병의 예방 및 치유기능과 작용이 있는 천연 식물약재들이므로, 한꺼번에 1단계로 알콜 수용액으로 처리하여 추출액을 얻고 그 압착잔사를 2단계로 고압 고온수로 처리한 각 추출액을 혼합하여 혼합추출액을 농축한 혼합추출액을 얻는 방법이다.As the natural plant medicinal materials described above, mulberry mistletoe, pine ivy, Eoseongcho, Aralia, main salt and maternal are natural plant medicinal products that have functions and functions to prevent and heal skin diseases, so the extract is treated with an aqueous alcohol solution in one step at a time. This is a method of obtaining a mixed extract obtained by concentrating the mixed extract by mixing each extract obtained by obtaining the compressed residue in two steps with high pressure hot water.
상기 식물약재들의 혼합추출농축액의 제조방법을 구체적으로 설명하면,When explaining in detail the method for preparing the mixed extract concentrate of the plant medicinal materials,
뽕나무 겨우살이, 소나무 담쟁이, 어성초, 두릅나무, 주염나무, 산모 2.8:1:1:1:1:1의 비율중량으로 혼합한 천연 식물약재 100중량부와 30%의 에타놀 수용액 300중량부를 밀폐용기에 투입, 75~77℃로 유지시킨 상태에서 12~15시간 열처리하여 추출물을 얻고, 이 추출물을 압착하여 에타놀 수용액의 추출액과 1차 식물약재 잔사를 분리하고, 분리된 1차 식물약재 잔사에 잔사 중량의 3배의 물을 첨가, 온도 150~160℃로 유지된 밀폐 고압부에서 4~5시간 열처리하여 추출물을 얻고, 이 추출물을 압착하여 물 추출액과 2차 식물약재 잔사를 분리하고, 분리된 물 추출액을 상기 에타놀 수용액 추출액에 혼합하여 혼합추출액을 얻고, 이 혼합추출액을 온도 80℃로 유지시킨 상태에서 감압 농축하여 에타놀을 완전히 회수하고, 계속 가열하여 농축시키므로서 2~3포이즈의 식물약재 농축추출액을 제조한다.Mulberry mistletoe, pine ivy, Eoseongcho, Aralia, main salt, maternal 2.8:1:1:1:1: 100 parts by weight of natural plant medicinal mixture and 300 parts by weight of 30% ethanol aqueous solution in an airtight container Addition, heat treatment for 12 to 15 hours in a state maintained at 75 to 77°C to obtain an extract, and the extract is compressed to separate the extract of ethanol aqueous solution from the first plant medicine residue, and the weight of the residue on the separated first plant medicine residue 3 times the amount of water is added and heat-treated in a sealed high-pressure part maintained at a temperature of 150 to 160°C for 4 to 5 hours to obtain an extract, and the extract is compressed to separate the water extract from the secondary plant medicine residue, and the separated water extract Was mixed with the ethanol aqueous solution extract to obtain a mixed extract, and the mixed extract was concentrated under reduced pressure while maintaining the temperature at 80°C to completely recover ethanol, and continued heating to concentrate, thereby obtaining a concentrated extract of 2 to 3 poise of plant medicine. To manufacture.
상기 농축된 농축추출액을 얻는 방법에 있어서, 에타놀 수용액의 온도를 77℃ 이상으로 하면 에타놀의 비점 이상의 온도가 되므로, 에타놀의 많은 량이 증발하므로 에타놀의 손실이 커지며 또한, 천연 식물약재들 중에는 알콜에 용해되는 성분과, 물에 용해되는 성분이 있고, 알콜 및 물 양측 모두에 용해되는 성분이 있으며, 고온의 물에 의해 용해되는 성분이 있고, 물과 알콜에 용해되지 않으나 아세트산(식초산) 또는 에텔에만 용해되는 성분도 있다. 그러나 공정의 난이성, 경제성, 유효특성 등 종합적인 여건을 고려할 때, 에타놀 수용액에서 추출하는 공정과 고압 고온의 물에서 추출하는 공정을 분리해서 추출하는 방법이 천연 식물약재로부터 유용한 약리적인 성분을 효율적으로 추출하는 방법이라 할 수 있다.In the method of obtaining the concentrated concentrated extract, if the temperature of the ethanol aqueous solution is set to 77°C or higher, the temperature of the ethanol solution becomes higher than the boiling point of ethanol, so that a large amount of ethanol evaporates, resulting in a large loss of ethanol, and it is soluble in alcohol among natural plant medicines. There is a component that is dissolved in water, a component that is soluble in water, and there is a component that is soluble in both alcohol and water, and there is a component that is soluble by high temperature water, and is not soluble in water and alcohol, but only in acetic acid or ether. Some ingredients dissolve. However, considering the overall conditions such as difficulty, economy, and effective characteristics of the process, the method of separating and extracting the process of extracting from ethanol aqueous solution and the process of extracting from high pressure and high temperature water efficiently extracts useful pharmacological components from natural plant medicines. It can be said to be a method of extraction.
항산화제는 레시친을 사용하며 아스코르빈산을 함께 사용하므로서, 시너지스트 항산화 효과를 얻을 수 있어 지방산을 주성분으로 하는 비누와 산화에 의한 산폐를 방지하므로서, 비누의 변질을 방지할 수 있고, 산폐에 의하여 발생되는 악취를 방지할 수 있으며, 피부에도 지속적으로 사용 시, 항산화 작용으로 피부의 노화진행을 지연시킬 수 있고, 또한 보존제로서 소르빈산(sorbic acid) 또는 그의 염류를 사용하고 이들의 방부제로서의 작용기작은 탈수소 효소계의 작용을 저해하고, 항균작용으로서 기작은 미생물포자의 발아와 성장과정을 억제하므로서, 미생물 생세포의 증식을 방지하게 되고, 미생물 세포 내 효소계 기능을 저해하므로서 정상적인 미생물 생육을 억제하게 된다.As an antioxidant, lecithin is used and ascorbic acid is used together to obtain a synergistic antioxidant effect, so it is possible to prevent deterioration of soap by preventing acid waste due to oxidation and soap containing fatty acids as the main component. It can prevent the odor that occurs, and when it is used continuously on the skin, it can delay the aging process of the skin due to its antioxidant action, and sorbic acid or its salts are used as a preservative, and the mechanism of action as a preservative is dehydrogenation. It inhibits the action of the enzyme system and inhibits the germination and growth process of microbial spores as an antimicrobial mechanism, thereby preventing the proliferation of living microorganism cells, and inhibiting the normal growth of microorganisms by inhibiting the enzyme system function in the microbial cell.
또한 전술한 죽염 등의 용해도가 높은 성분을 함께 첨가하는 경우, 솔베이트(sorbate)의 용해도가 상대적으로 감소하고, water phase의 축적되는 양이 많으므로, 미생물에 대한 항균효과가 상승하며 항산화제와 함께 첨가하면 솔베이트의 항균효과가 상승하게 된다.In addition, when a component having high solubility such as bamboo salt is added together, the solubility of sorbate is relatively decreased and the amount of accumulation in the water phase is large, so that the antibacterial effect against microorganisms increases, and antioxidants and When added together, the antibacterial effect of sorbate increases.
본 발명의 구성을 보다 명확하게 하고 다기능성 미용비누의 효과를 알아보기 위해 실시예를 들기로 한다.Examples will be given in order to clarify the configuration of the present invention and to find out the effect of the multifunctional cosmetic soap.
본 발명 비누소지 86kg, 낙화생유, 올리브유, 갈락토즈 발효액, 살리실산, 알로에발효액 및 손바닥선인장엑기스 각각 1kg, 소프넛, 알란토인 및 죽염 각각 0.5kg, 그리고 뽕나무 겨우살이, 어성초 담장이, 소나무 담장이, 두릅나무, 주엽나무 및 산모 각각의 혼합중량비가 2:1.5:0.5:0.5:0.5:0.5가 되도록 혼합한 식물약재들을 30중량%의 알콜수용액으로 추출한 추출액과 그 추출액을 얻고 난 식물약재 잔사를 고온고압수로 추출한 추출액을 혼합한 혼합추출 농축액 5.5kg, 레시친 0.3kg, 아스코르빈산 0.3kg, 소르브산 0.2kg, 자스민향 0.2kg으로 조성한 다기능성 미용비누 조성물로 본 발명 다기능성 미용비누 제조방법에 따라 다기능성 미용비누를 제조하였다.86 kg of soap base of the present invention, peanut oil, olive oil, galactose fermentation solution, salicylic acid, aloe fermentation solution and palm cactus extract 1 kg each, soft nut, allantoin and bamboo salt 0.5 kg each, and mulberry mistletoe, Eoseongcho fence, pine fence, aralia, main leaf The extract obtained by extracting the mixed plant medicines so that the mixing weight ratio of each of the trees and mothers was 2:1.5:0.5:0.5:0.5:0.5 with 30% by weight of an alcoholic aqueous solution, and the plant medicine residue obtained from the extract was extracted with high temperature and high pressure water. Multi-functional beauty soap composition composed of 5.5 kg of mixed extract concentrate mixed with extract, 0.3 kg of lecithin, 0.3 kg of ascorbic acid, 0.2 kg of sorbic acid, and 0.2 kg of jasmine flavor, according to the multifunctional beauty soap manufacturing method of the present invention. Soap was prepared.
실험예 1Experimental Example 1
본 발명 비누의 사용기간을 알아보기 위해 목욕탕A 및 B를 찾아가 종래 사용하는 비누의 사용하는 기간을 알아본 결과 3일을 사용하면 비누의 3/4이 닳아 버리고 1/4이 남게 되나 사용할 수 없는 상태로 된다고 하였다.To find out the use period of the soap of the present invention, visit Bathhouse A and B to find out the period of use of the conventional soap. After 3 days of use, 3/4 of the soap is worn out and 1/4 remains, but cannot be used. It was said to be in a state.
실시예(1)에서 제조한 비누 100식을 A목욕탕과 B목욕탕에 주면서 사용할 수 있는 기간을 측정해 달라고 부탁하고 일주일 후 찾아가 결과를 알아본 결과 5일까지는 사용할 수 있다고 한다.Giving 100 meals of soap prepared in Example (1) to Bath A and Bath B, asked to measure the period of use, and visited after a week to find out the results.
실험예 2Experimental Example 2
여드름이 심하게 돋은 고등학교 남학생 10명을 대상으로 각자 실시예(1)에서 제조한 10개식의 비누를 제공하고 아침 저녁 2회에 걸쳐 세수 하도록 하고 20일 간격으로 치유 상태를 조사한 결과 다음 표(1)을 얻을 수 있었다.Ten high school boys with severe acne were provided with 10 soaps prepared in Example (1), and were washed twice in the morning and at night, and the healing status was investigated every 20 days. Was able to get.
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