KR20180084276A - 과산화수소 분해용 촉매의 제조 방법 - Google Patents

과산화수소 분해용 촉매의 제조 방법 Download PDF

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KR20180084276A
KR20180084276A KR1020170007129A KR20170007129A KR20180084276A KR 20180084276 A KR20180084276 A KR 20180084276A KR 1020170007129 A KR1020170007129 A KR 1020170007129A KR 20170007129 A KR20170007129 A KR 20170007129A KR 20180084276 A KR20180084276 A KR 20180084276A
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South Korea
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decomposition
hydrogen peroxide
catalyst
mixed solution
manganese oxide
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KR1020170007129A
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KR101948659B1 (ko
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이강봉
남윤식
서명기
김민준
이관영
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한국과학기술연구원
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
    • A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
    • A61L2/18—Liquid substances or solutions comprising solids or dissolved gases
    • A61L2/186—Peroxide solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/32—Manganese, technetium or rhenium
    • B01J23/34—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
    • B01J35/0006—
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0203—Preparation of oxygen from inorganic compounds
    • C01B13/0211—Peroxy compounds
    • C01B13/0214—Hydrogen peroxide

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)

Abstract

세틸트리메틸암모늄 브로마이드(Cetyltrimethyl ammonium bromide: CTAB)가 용해된 제1 용매에 탄소 재료를 혼합한 후 분산시켜 혼합 용액을 형성하는 단계; 해당 혼합 용액에 망간 산화물 전구체를 주입시키고 교반하는 단계; 해당 망간 산화물 전구체가 주입된 해당 혼합 용액에 제2 용매를 주입한 후 교반시켜 탄소 재료 상에 담지된 망간 산화물을 포함하는 예비 과산화수소 분해용 촉매를 제조하는 단계; 이온 교환 공정을 통해 예비 과산화수소 분해용 촉매로부터 CTAB를 제거한 하여 탄소 재료 상에 담지된 다공성 망간 산화물을 포함하는 과산화수소 분해용 촉매를 제조하는 단계; 를 포함하는 과산화수소 분해용 촉매의 제조 방법이 제공된다.
KR1020170007129A 2017-01-16 2017-01-16 과산화수소 분해용 촉매의 제조 방법 KR101948659B1 (ko)

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KR1020170007129A KR101948659B1 (ko) 2017-01-16 2017-01-16 과산화수소 분해용 촉매의 제조 방법

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KR1020170007129A KR101948659B1 (ko) 2017-01-16 2017-01-16 과산화수소 분해용 촉매의 제조 방법

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KR101948659B1 KR101948659B1 (ko) 2019-02-18

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110575848A (zh) * 2019-09-19 2019-12-17 燕山大学 一种用于催化臭氧氧化挥发性有机物的催化剂的制备方法
CN112742378A (zh) * 2021-01-22 2021-05-04 上海大学 锰钾矿型锰氧化物微孔蜂窝铝芯催化剂模块、其制备方法及其催化分解过氧化氢的应用

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002059003A (ja) * 2000-08-18 2002-02-26 Katayama Chem Works Co Ltd 過酸化水素分解触媒およびそれを用いた過酸化水素の分解方法
US6991772B1 (en) 1995-05-31 2006-01-31 The United States Of America As Represented By The Secretary Of The Air Force H2O2 decomposition catalyst
JP2010274169A (ja) * 2009-05-27 2010-12-09 Nisshinbo Holdings Inc 過酸化水素分解用触媒およびその製造方法
JP2012063302A (ja) * 2010-09-17 2012-03-29 Japan Organo Co Ltd 超純水中の全有機炭素含有量の測定システム及び方法
KR20140067308A (ko) * 2012-11-26 2014-06-05 국방과학연구소 암모니아 및 과산화수소 가스 제거제 및 장치

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6991772B1 (en) 1995-05-31 2006-01-31 The United States Of America As Represented By The Secretary Of The Air Force H2O2 decomposition catalyst
JP2002059003A (ja) * 2000-08-18 2002-02-26 Katayama Chem Works Co Ltd 過酸化水素分解触媒およびそれを用いた過酸化水素の分解方法
JP2010274169A (ja) * 2009-05-27 2010-12-09 Nisshinbo Holdings Inc 過酸化水素分解用触媒およびその製造方法
JP2012063302A (ja) * 2010-09-17 2012-03-29 Japan Organo Co Ltd 超純水中の全有機炭素含有量の測定システム及び方法
KR20140067308A (ko) * 2012-11-26 2014-06-05 국방과학연구소 암모니아 및 과산화수소 가스 제거제 및 장치

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
- J. Mater. Chem. A. 2014, 2, pp.3641-3647 *
Do, Si-Hyun, et al. "Hydrogen peroxide decomposition on manganese oxide (pyrolusite): kinetics, intermediates, and mechanism." Chemosphere 75.1 (2009): 8-12.
J. Nanosci. Nanotechnol. 2016, Vol.16, No.9, pp.9153-9159 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110575848A (zh) * 2019-09-19 2019-12-17 燕山大学 一种用于催化臭氧氧化挥发性有机物的催化剂的制备方法
CN110575848B (zh) * 2019-09-19 2020-11-27 燕山大学 一种用于催化臭氧氧化挥发性有机物的催化剂的制备方法
CN112742378A (zh) * 2021-01-22 2021-05-04 上海大学 锰钾矿型锰氧化物微孔蜂窝铝芯催化剂模块、其制备方法及其催化分解过氧化氢的应用

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