KR20150114523A - 기체상에서 1차 아민의 포스겐화에 의해 제조된 이소시아네이트를 포스겐화 기체의 조생성물로부터 분리하는 방법 - Google Patents

기체상에서 1차 아민의 포스겐화에 의해 제조된 이소시아네이트를 포스겐화 기체의 조생성물로부터 분리하는 방법 Download PDF

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Publication number
KR20150114523A
KR20150114523A KR1020157023401A KR20157023401A KR20150114523A KR 20150114523 A KR20150114523 A KR 20150114523A KR 1020157023401 A KR1020157023401 A KR 1020157023401A KR 20157023401 A KR20157023401 A KR 20157023401A KR 20150114523 A KR20150114523 A KR 20150114523A
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KR
South Korea
Prior art keywords
liquid
stream
isocyanate
quenching
quenching liquid
Prior art date
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Abandoned
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KR1020157023401A
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English (en)
Korean (ko)
Inventor
프리트헬름 스테펜스
바스티안 마흐르
Original Assignee
바이엘 머티리얼사이언스 아게
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Publication date
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Publication of KR20150114523A publication Critical patent/KR20150114523A/ko
Abandoned legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C265/00—Derivatives of isocyanic acid
    • C07C265/14—Derivatives of isocyanic acid containing at least two isocyanate groups bound to the same carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020157023401A 2013-02-08 2014-02-05 기체상에서 1차 아민의 포스겐화에 의해 제조된 이소시아네이트를 포스겐화 기체의 조생성물로부터 분리하는 방법 Abandoned KR20150114523A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13154596 2013-02-08
EP13154596.4 2013-02-08
PCT/EP2014/052260 WO2014122180A1 (de) 2013-02-08 2014-02-05 Verfahren zur abtrennung eines durch phosgenierung eines primären amins in der gasphase hergestellten isocyanats aus dem gasförmigen rohprodukt der phosgenierung

Publications (1)

Publication Number Publication Date
KR20150114523A true KR20150114523A (ko) 2015-10-12

Family

ID=47750442

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020157023401A Abandoned KR20150114523A (ko) 2013-02-08 2014-02-05 기체상에서 1차 아민의 포스겐화에 의해 제조된 이소시아네이트를 포스겐화 기체의 조생성물로부터 분리하는 방법

Country Status (8)

Country Link
US (1) US9932299B2 (enExample)
EP (1) EP2953928B1 (enExample)
JP (1) JP6297602B2 (enExample)
KR (1) KR20150114523A (enExample)
CN (1) CN105121403B (enExample)
HU (1) HUE034207T2 (enExample)
SA (1) SA515360864B1 (enExample)
WO (1) WO2014122180A1 (enExample)

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* Cited by examiner, † Cited by third party
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EP3122719B1 (de) 2014-03-27 2018-05-16 Covestro Deutschland AG Verfahren zum betreiben einer gasphasenphosgenierungsanlage
JP6621759B2 (ja) 2014-03-27 2019-12-18 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ 気相ホスゲン化プラントの運転方法
US10919845B2 (en) 2017-04-03 2021-02-16 Covestro Deutschland Ag Cleaning device for gas flows from isocyanate production
CN110914236B (zh) * 2017-06-08 2023-01-31 科思创德国股份有限公司 制备异氰酸酯的方法
EP3634947B1 (de) 2017-06-08 2022-09-07 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von isocyanaten in der gasphase
JP2024543700A (ja) * 2021-12-17 2024-11-21 モジア（シャンハイ）バイオテック・カンパニー・リミテッド 気相無溶媒方法によってイソシアネートを調製する方法
CN115155467B (zh) * 2022-08-09 2023-10-10 宁夏瑞泰科技股份有限公司 采用液相光气化合成六亚甲基二异氰酸酯的系统及方法

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US4101590A (en) * 1976-08-23 1978-07-18 Maruzen Oil Co., Ltd. Process for separation and purification of vinylphenol
DE2756928A1 (de) * 1977-12-21 1979-07-05 Bayer Ag Verfahren zur kontinuierlichen herstellung von monoisocyanaten
DE3714439A1 (de) 1987-04-30 1988-11-10 Bayer Ag Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten
DE4217019A1 (de) 1992-05-22 1993-11-25 Bayer Ag Verfahren zur Herstellung von aromatischen Diisocyanaten
DE19523385A1 (de) 1995-06-23 1997-01-09 Bayer Ag Verfahren zur Herstellung von Triisocyanaten
US6120640A (en) 1996-12-19 2000-09-19 Applied Materials, Inc. Boron carbide parts and coatings in a plasma reactor
DE10158160A1 (de) 2001-11-28 2003-06-12 Basf Ag Herstellung von Isocyanaten in der Gasphase
DE10161384A1 (de) 2001-12-14 2003-06-18 Bayer Ag Verbessertes Verfahren für die Herstellung von (/Poly)-isocyanaten in der Gasphase
EP1371634A1 (en) * 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate
EP1371633A1 (en) 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
DE10245704A1 (de) 2002-09-30 2004-04-01 Bayer Ag Verfahren zum Quenchen eines gasförmigen Reaktionsgemisches bei der Gasphasenphosgenierung von Diaminen
DE60214195T2 (de) 2002-10-22 2007-10-04 Bayer Materialscience Ag Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung
DE10349504A1 (de) 2003-10-23 2005-05-25 Bayer Technology Services Gmbh Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE10359627A1 (de) 2003-12-18 2005-07-21 Bayer Materialscience Ag Verfahren zur Herstellung von Diisocyanaten
DE102004030164A1 (de) 2004-06-22 2006-01-19 Basf Ag Verfahren zur Herstellung von Isocyanaten
DE102005036870A1 (de) 2005-08-02 2007-02-08 Bayer Materialscience Ag Verfahren zur Gasphasenphosgenierung
DE102005037328A1 (de) 2005-08-04 2007-02-08 Basf Ag Verfahren zur Herstellung von Isocyanaten
DE102005042392A1 (de) * 2005-09-06 2007-03-08 Basf Ag Verfahren zur Herstellung von Isocyanaten
US7504533B2 (en) 2006-04-24 2009-03-17 Bayer Materialscience Llc Process for the production of isocyanates
DE102006058634A1 (de) * 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE102006058633A1 (de) 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
EP2028178A1 (de) * 2007-08-22 2009-02-25 Bayer MaterialScience AG Herstellung von Isocyanaten mit niedrigen Chlorgehalten
JP5771528B2 (ja) * 2008-11-07 2015-09-02 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ イソシアネートの製造方法
FR2939131B1 (fr) * 2008-12-01 2010-12-17 Rhodia Operations Procede de fabrication d'acide adipique
CN102239143B (zh) * 2008-12-03 2014-02-12 巴斯夫欧洲公司 制备异氰酸酯的方法
DE102008061686A1 (de) 2008-12-11 2010-06-17 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
KR20120013937A (ko) 2009-04-08 2012-02-15 바스프 에스이 이소시아네이트의 제조 방법
DE102009032413A1 (de) 2009-07-09 2011-01-13 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
KR101869117B1 (ko) * 2010-10-14 2018-06-19 바스프 에스이 이소시아네이트를 제조하는 방법
PL214499B1 (pl) 2010-12-10 2013-08-30 Inst Chemii Przemyslowej Im Prof Ignacego Moscickiego Sposób wydzielania toluilenodiizocyjanianu z mieszaniny poreakcyjnej w procesie fosgenowania toluilenodiaminy w fazie gazowej

Also Published As

Publication number Publication date
EP2953928A1 (de) 2015-12-16
US9932299B2 (en) 2018-04-03
EP2953928B1 (de) 2017-08-09
CN105121403A (zh) 2015-12-02
SA515360864B1 (ar) 2017-10-29
HUE034207T2 (hu) 2018-01-29
US20150368190A1 (en) 2015-12-24
JP6297602B2 (ja) 2018-03-20
WO2014122180A1 (de) 2014-08-14
JP2016506970A (ja) 2016-03-07
CN105121403B (zh) 2017-12-08

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