JP6297602B2 - ホスゲン化のガス状粗生成物からの、気相中の第一級アミンをホスゲン化することにより調製されたイソシアネートの分離方法 - Google Patents

ホスゲン化のガス状粗生成物からの、気相中の第一級アミンをホスゲン化することにより調製されたイソシアネートの分離方法 Download PDF

Info

Publication number
JP6297602B2
JP6297602B2 JP2015556484A JP2015556484A JP6297602B2 JP 6297602 B2 JP6297602 B2 JP 6297602B2 JP 2015556484 A JP2015556484 A JP 2015556484A JP 2015556484 A JP2015556484 A JP 2015556484A JP 6297602 B2 JP6297602 B2 JP 6297602B2
Authority
JP
Japan
Prior art keywords
liquid
stream
quench
isocyanate
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2015556484A
Other languages
English (en)
Japanese (ja)
Other versions
JP2016506970A (ja
JP2016506970A5 (enExample
Inventor
フリートヘルム、シュテフェンス
バスティアン、マール
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covestro Deutschland AG
Original Assignee
Covestro Deutschland AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Covestro Deutschland AG filed Critical Covestro Deutschland AG
Publication of JP2016506970A publication Critical patent/JP2016506970A/ja
Publication of JP2016506970A5 publication Critical patent/JP2016506970A5/ja
Application granted granted Critical
Publication of JP6297602B2 publication Critical patent/JP6297602B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2015556484A 2013-02-08 2014-02-05 ホスゲン化のガス状粗生成物からの、気相中の第一級アミンをホスゲン化することにより調製されたイソシアネートの分離方法 Expired - Fee Related JP6297602B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13154596 2013-02-08
EP13154596.4 2013-02-08
PCT/EP2014/052260 WO2014122180A1 (de) 2013-02-08 2014-02-05 Verfahren zur abtrennung eines durch phosgenierung eines primären amins in der gasphase hergestellten isocyanats aus dem gasförmigen rohprodukt der phosgenierung

Publications (3)

Publication Number Publication Date
JP2016506970A JP2016506970A (ja) 2016-03-07
JP2016506970A5 JP2016506970A5 (enExample) 2017-03-09
JP6297602B2 true JP6297602B2 (ja) 2018-03-20

Family

ID=47750442

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2015556484A Expired - Fee Related JP6297602B2 (ja) 2013-02-08 2014-02-05 ホスゲン化のガス状粗生成物からの、気相中の第一級アミンをホスゲン化することにより調製されたイソシアネートの分離方法

Country Status (8)

Country Link
US (1) US9932299B2 (enExample)
EP (1) EP2953928B1 (enExample)
JP (1) JP6297602B2 (enExample)
KR (1) KR20150114523A (enExample)
CN (1) CN105121403B (enExample)
HU (1) HUE034207T2 (enExample)
SA (1) SA515360864B1 (enExample)
WO (1) WO2014122180A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3122719B1 (de) 2014-03-27 2018-05-16 Covestro Deutschland AG Verfahren zum betreiben einer gasphasenphosgenierungsanlage
JP6621759B2 (ja) 2014-03-27 2019-12-18 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ 気相ホスゲン化プラントの運転方法
US10919845B2 (en) 2017-04-03 2021-02-16 Covestro Deutschland Ag Cleaning device for gas flows from isocyanate production
CN110914236B (zh) * 2017-06-08 2023-01-31 科思创德国股份有限公司 制备异氰酸酯的方法
EP3634947B1 (de) 2017-06-08 2022-09-07 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von isocyanaten in der gasphase
JP2024543700A (ja) * 2021-12-17 2024-11-21 モジア（シャンハイ）バイオテック・カンパニー・リミテッド 気相無溶媒方法によってイソシアネートを調製する方法
CN115155467B (zh) * 2022-08-09 2023-10-10 宁夏瑞泰科技股份有限公司 采用液相光气化合成六亚甲基二异氰酸酯的系统及方法

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4101590A (en) * 1976-08-23 1978-07-18 Maruzen Oil Co., Ltd. Process for separation and purification of vinylphenol
DE2756928A1 (de) * 1977-12-21 1979-07-05 Bayer Ag Verfahren zur kontinuierlichen herstellung von monoisocyanaten
DE3714439A1 (de) 1987-04-30 1988-11-10 Bayer Ag Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten
DE4217019A1 (de) 1992-05-22 1993-11-25 Bayer Ag Verfahren zur Herstellung von aromatischen Diisocyanaten
DE19523385A1 (de) 1995-06-23 1997-01-09 Bayer Ag Verfahren zur Herstellung von Triisocyanaten
US6120640A (en) 1996-12-19 2000-09-19 Applied Materials, Inc. Boron carbide parts and coatings in a plasma reactor
DE10158160A1 (de) 2001-11-28 2003-06-12 Basf Ag Herstellung von Isocyanaten in der Gasphase
DE10161384A1 (de) 2001-12-14 2003-06-18 Bayer Ag Verbessertes Verfahren für die Herstellung von (/Poly)-isocyanaten in der Gasphase
EP1371634A1 (en) * 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate
EP1371633A1 (en) 2002-06-14 2003-12-17 Bayer Ag Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
DE10245704A1 (de) 2002-09-30 2004-04-01 Bayer Ag Verfahren zum Quenchen eines gasförmigen Reaktionsgemisches bei der Gasphasenphosgenierung von Diaminen
DE60214195T2 (de) 2002-10-22 2007-10-04 Bayer Materialscience Ag Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung
DE10349504A1 (de) 2003-10-23 2005-05-25 Bayer Technology Services Gmbh Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE10359627A1 (de) 2003-12-18 2005-07-21 Bayer Materialscience Ag Verfahren zur Herstellung von Diisocyanaten
DE102004030164A1 (de) 2004-06-22 2006-01-19 Basf Ag Verfahren zur Herstellung von Isocyanaten
DE102005036870A1 (de) 2005-08-02 2007-02-08 Bayer Materialscience Ag Verfahren zur Gasphasenphosgenierung
DE102005037328A1 (de) 2005-08-04 2007-02-08 Basf Ag Verfahren zur Herstellung von Isocyanaten
DE102005042392A1 (de) * 2005-09-06 2007-03-08 Basf Ag Verfahren zur Herstellung von Isocyanaten
US7504533B2 (en) 2006-04-24 2009-03-17 Bayer Materialscience Llc Process for the production of isocyanates
DE102006058634A1 (de) * 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
DE102006058633A1 (de) 2006-12-13 2008-06-19 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
EP2028178A1 (de) * 2007-08-22 2009-02-25 Bayer MaterialScience AG Herstellung von Isocyanaten mit niedrigen Chlorgehalten
JP5771528B2 (ja) * 2008-11-07 2015-09-02 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ イソシアネートの製造方法
FR2939131B1 (fr) * 2008-12-01 2010-12-17 Rhodia Operations Procede de fabrication d'acide adipique
CN102239143B (zh) * 2008-12-03 2014-02-12 巴斯夫欧洲公司 制备异氰酸酯的方法
DE102008061686A1 (de) 2008-12-11 2010-06-17 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
KR20120013937A (ko) 2009-04-08 2012-02-15 바스프 에스이 이소시아네이트의 제조 방법
DE102009032413A1 (de) 2009-07-09 2011-01-13 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten
KR101869117B1 (ko) * 2010-10-14 2018-06-19 바스프 에스이 이소시아네이트를 제조하는 방법
PL214499B1 (pl) 2010-12-10 2013-08-30 Inst Chemii Przemyslowej Im Prof Ignacego Moscickiego Sposób wydzielania toluilenodiizocyjanianu z mieszaniny poreakcyjnej w procesie fosgenowania toluilenodiaminy w fazie gazowej

Also Published As

Publication number Publication date
EP2953928A1 (de) 2015-12-16
US9932299B2 (en) 2018-04-03
EP2953928B1 (de) 2017-08-09
CN105121403A (zh) 2015-12-02
SA515360864B1 (ar) 2017-10-29
HUE034207T2 (hu) 2018-01-29
US20150368190A1 (en) 2015-12-24
WO2014122180A1 (de) 2014-08-14
JP2016506970A (ja) 2016-03-07
CN105121403B (zh) 2017-12-08
KR20150114523A (ko) 2015-10-12

Similar Documents

Publication Publication Date Title
JP6297602B2 (ja) ホスゲン化のガス状粗生成物からの、気相中の第一級アミンをホスゲン化することにより調製されたイソシアネートの分離方法
TWI471295B (zh) 製備異氰酸酯之方法
CN101302174B (zh) 生产异氰酸酯的方法
JP5129808B2 (ja) ＨＣｌ酸化法の生成ガスから塩素を分離する方法
US10836713B2 (en) Method for producing isocyanates in the gas phase
JP6743068B2 (ja) 化学反応用塩化水素製造方法
CN111630027B (zh) 制备异氰酸酯的方法
KR101685699B1 (ko) 이소시아네이트의 기상 제조 방법
US10858311B2 (en) Method for producing isocyanates
CN107848960B (zh) 用于制备异氰酸酯的方法
KR101829481B1 (ko) 기체 상에서의 이소시아네이트의 제조 방법
CN114423736B (zh) 异氰酸酯的蒸馏方法
KR102898304B1 (ko) 이소시아네이트의 제조 방법
HK1133245A (en) Method for separating chlorine from the product gas from an hci oxidation process
HK1124586A (en) A process for the production of isocyanates

Legal Events

Date Code Title Description
RD03 Notification of appointment of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7423

Effective date: 20161118

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20170203

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20170203

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20170925

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20171003

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20180104

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20180123

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20180221

R150 Certificate of patent or registration of utility model

Ref document number: 6297602

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees