KR102577048B1 - Mist composition for improving hair gloss and moisturizing power - Google Patents

Abstract

The present invention is cyclopentasiloxane, C12-15 alkyl benzoate, phenyl trimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, blood Provides a mist composition for hair care containing sebum-3 caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance, and ethanol.

Description

Mist composition for improving hair gloss and moisturizing power}

The present invention relates to a mist composition for improving hair shine and moisturizing power.

Hair is composed of medula, cortex, and cuticle, and most of the hair is cortex, which is made up of keratin protein. If Cortex's keratin protein is lost, the hair becomes weak along with symptoms such as hair brittleness and hair breakage. To prevent loss of Cortex's keratin protein, it is necessary to protect and improve the hair cuticle.

The hair cuticle is a thin layer on the outermost layer of the hair and takes the form of multiple layers to protect the keratin protein of Cortex. Protecting and improving the hair cuticle can protect the keratin protein in Cortex from external stimuli such as perm, dye, and dryer, and at the same time, maintain smooth and shiny hair.

On the other hand, a hair treatment composition is known that is filled in a container and discharged in the form of a mist using a pump-type dispenser or trigger-type dispenser. When the composition is discharged in the form of a mist, the composition can be applied uniformly over a wide range of hair, and sagging from the hair after application is suppressed, providing excellent feeling of use.

Conventionally, hair treatment compositions discharged in the form of a mist either provide hair-styling performance or conditioning performance depending on the composition design.

Patent Document 1: Republic of Korea Patent 10-2339025

The present invention was devised to solve the above problems, and the purpose of the present invention is to provide a mist composition for hair care with excellent overall preference such as hair texture, shine, moisturizing power, and fragrance.

The object of the present invention is not limited to the problems mentioned above, and other problems not mentioned will be clearly understood by those skilled in the art from the description below.

In order to achieve the above object, the present invention

Cyclopentasiloxane, C12-15 alkyl benzoate, phenyl trimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, PPG-3 Provides a mist composition for hair care containing caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance, and ethanol.

In addition, the present invention

Preparing camellia seed powder, jojoba seed powder, and argan kernel powder by crushing camellia seeds, jojoba seeds, and argan kernels; Preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder at a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring for 2-4 days at a temperature of 28-32°C; and filtering the extract, concentrating it under reduced pressure, centrifuging it to remove foreign substances, and then distilling it under reduced pressure; preparing camellia seed oil, jojoba seed oil, and argan kernel oil, including;

Washing peony, angelica root and Rehmannia glutinosa and pre-treating them at a temperature of 18-22°C and a pressure of 140-160 MPa for 3-7 minutes; Preparing a mixed juice by mixing pretreated peony, angelica root and Rehmannia glutinosa at a weight ratio of 1:1:1 and extracting the juice; Centrifuging the mixed juice to obtain a supernatant containing exosomes; Preparing a lyophilisate by lyophilizing the supernatant containing the exosomes; Forming an aqueous two-phase system using polyethylene glycol/dextran in the freeze-dried product; and obtaining a lower layer liquid in which exosomes in the aqueous two-phase system are concentrated; preparing exosomes derived from Peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa, including;

Washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; And filtering and concentrating the extract under reduced pressure and then freeze-drying; preparing a fermented Schisandra seed extract and a fermented buckwheat seed extract including;

3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 Die Mix 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3 caprylyl ether, 0.3-3 parts by weight of geraniol, and 18-22 parts by weight of ethanol, and incubate at 400°C at a temperature of 38-42°C. Preparing a first mixture by stirring for 3-7 minutes at a rotation speed of 600 rpm;

1-5 parts by weight of peony-derived exosomes, angelica root exosomes, and Rehmannia glutinosa-derived exosomes prepared above, 0.5-4 parts by weight of Schisandra chinensis seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 Parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of flavoring, and 11-15 parts by weight of broccoli water were mixed, and the mixture was heated at a temperature of 48-52°C at a rotation speed of 700-900 rpm. Preparing a second mixture by stirring for 3-7 minutes; and

Mixing the first mixture and the second mixture and stirring for 13-17 minutes at a rotation speed of 400-600 rpm at a temperature of 43-47° C. .

In addition, the fragrance includes 18-22 parts by weight of lemon verbena oil, 18-22 parts by weight of vanilla oil, 8-12 parts by weight of mandarin oil, 2-6 parts by weight of hexyl salicylate, 18-22 parts by weight of dioctyl adipate, It is characterized in that it contains 1-5 parts by weight of propylene glycol, 1-5 parts by weight of butylphenylmethylpropional, and 18-22 parts by weight of ethanol.

The mist composition for hair care according to the present invention has excellent overall preference in terms of hair texture, shine, moisturizing power, and scent.

Hereinafter, various embodiments will be described in more detail. The embodiments described herein may be modified in various ways. Specific embodiments may be described in detail in the detailed description. However, the specific embodiments disclosed are only intended to facilitate understanding of the various embodiments. Accordingly, the technical idea is not limited to the specific embodiments disclosed, and should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.

Terms containing ordinal numbers, such as primary, secondary, first, second, etc., may be used to describe various components, but these components are not limited by the above-mentioned terms. The above-mentioned terms are used only for the purpose of distinguishing one component from another.

In this specification, terms such as 'include' or 'have' are intended to designate the presence of features, numbers, steps, operations, components, parts, or combinations thereof described in the specification, but are not intended to indicate the presence of one or more other features. It should be understood that this does not exclude in advance the possibility of the existence or addition of elements, numbers, steps, operations, components, parts, or combinations thereof. When a component is said to be 'connected' or 'connected' to another component, it is understood that it may be directly connected or connected to the other component, but that other components may exist in between. It should be. On the other hand, when a component is mentioned as being 'directly connected' or 'directly connected' to another component, it should be understood that there are no other components in between.

In addition, when describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the gist of the present invention, the detailed description thereof is abbreviated or omitted.

This invention

Cyclopentasiloxane, C12-15 alkyl benzoate, phenyl trimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, PPG-3 Provides a mist composition for hair care containing caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance, and ethanol.

The mist composition for hair care according to the present invention has excellent overall preference in terms of hair texture, shine, moisturizing power, and scent.

Containing the above camellia seed oil, jojoba seed oil, and argan kernel oil, you can have healthier and more shiny hair.

The combination of panthenol and phytantriol has a heat protection effect on hair.

In addition, the present invention

Preparing camellia seed powder, jojoba seed powder, and argan kernel powder by crushing camellia seeds, jojoba seeds, and argan kernels; Preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder at a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring for 2-4 days at a temperature of 28-32°C; and filtering the extract, concentrating it under reduced pressure, centrifuging it to remove foreign substances, and then distilling it under reduced pressure; preparing camellia seed oil, jojoba seed oil, and argan kernel oil, including;

Washing peony, angelica root and Rehmannia glutinosa and pre-treating them at a temperature of 18-22°C and a pressure of 140-160 MPa for 3-7 minutes; Preparing a mixed juice by mixing pretreated peony, angelica root and Rehmannia glutinosa at a weight ratio of 1:1:1 and extracting the juice; Centrifuging the mixed juice to obtain a supernatant containing exosomes; Preparing a lyophilisate by lyophilizing the supernatant containing the exosomes; Forming an aqueous two-phase system using polyethylene glycol/dextran in the freeze-dried product; and obtaining a lower layer liquid in which exosomes in the aqueous two-phase system are concentrated; preparing exosomes derived from Peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa, including;

Washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; And filtering and concentrating the extract under reduced pressure and then freeze-drying; preparing a fermented Schisandra seed extract and a fermented buckwheat seed extract including;

3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 Die Mix 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3 caprylyl ether, 0.3-3 parts by weight of geraniol, and 18-22 parts by weight of ethanol, and incubate at 400°C at a temperature of 38-42°C. Preparing a first mixture by stirring for 3-7 minutes at a rotation speed of 600 rpm;

1-5 parts by weight of peony-derived exosomes, angelica root exosomes, and Rehmannia glutinosa-derived exosomes prepared above, 0.5-4 parts by weight of Schisandra chinensis seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 Parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of flavoring, and 11-15 parts by weight of broccoli water were mixed, and the mixture was heated at a temperature of 48-52°C at a rotation speed of 700-900 rpm. Preparing a second mixture by stirring for 3-7 minutes; and

Mixing the first mixture and the second mixture and stirring for 13-17 minutes at a rotation speed of 400-600 rpm at a temperature of 43-47° C. .

Hereinafter, the manufacturing method of the mist composition for hair care according to the present invention will be described in detail in each step.

First, the method for producing a mist composition for hair care according to the present invention includes the step of preparing camellia seed oil, jojoba seed oil, and argan kernel oil. The step of producing the camellia seed oil, jojoba seed oil, and argan kernel oil includes grinding camellia seeds, jojoba seeds, and argan kernels to prepare camellia seed powder, jojoba seed powder, and argan kernel powder; Preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder at a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring for 2-4 days at a temperature of 28-32°C; And filtering the extract, concentrating it under reduced pressure, centrifuging it to remove foreign substances, and distilling it under reduced pressure.

The camellia seed oil is excellent in preventing rancidity while supplying unsaturated fatty acids, and also supplies a large amount of active ingredients such as oleic acid and oleic acid triglyceride to improve skin barrier function and prevent moisture loss. It is known to relieve fine wrinkles, have excellent antibacterial properties, improve skin elasticity, and provide antioxidant effects.

The jojoba seed oil has a less oily feel than other vegetable oils and has the structure of wax ester, a component of sebum, improving the effect of removing sebum and reducing the amount of dead skin cells and sebum secretion, and improving skin gloss and elasticity. It is also known to improve the moisturizing effect by forming a moisture film on the skin and helping prevent moisture loss.

The argan kernel oil contains abundant vitamin E, which breathes vitality and vitality into tired skin and makes the skin texture soft and supple. It is rich in omega 6, which makes up the cell membrane, and is known to have excellent skin moisturizing and regenerative effects. .

In the present invention, camellia seed oil, jojoba seed oil, and argan kernel oil are applied to a mist composition for hair care. Accordingly, it improves the texture and shine of the hair, prevents the destruction of the scalp moisturizing factor, and provides moisture and nutrition to the dry scalp, making the scalp healthy.

Next, the method for producing a mist composition for hair care according to the present invention includes the step of producing exosomes derived from peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa. The step of preparing the peony-derived exosomes, Angelica quasi-derived exosomes, and Rehmannia glutinosa-derived exosomes involves washing the peony, Angelica root, and Rehmannia glutinosa and pretreating them at a temperature of 18-22°C and a pressure of 140-160 MPa for 3-7 minutes. step; Preparing a mixed juice by mixing pretreated peony, angelica root and Rehmannia glutinosa at a weight ratio of 1:1:1 and extracting the juice; Centrifuging the mixed juice to obtain a supernatant containing exosomes; Preparing a lyophilisate by lyophilizing the supernatant containing the exosomes; Forming an aqueous two-phase system using polyethylene glycol/dextran in the freeze-dried product; and obtaining a lower layer solution in which exosomes in the aqueous two-phase system are concentrated.

Exosomes refer to small membrane-structured vesicles secreted from various cells and are defined as a type of extracellular vesicles (EVs). All cells exchange information with other cells or the external environment and secrete extracellular vesicles for this purpose. Exosomes have a size of about 50 to 200 nm and contain biologically active substances such as proteins, lipids, and nucleic acids. Exosomes exist in various cells such as mammals, bacteria, and plants, and can be used for diagnosis and treatment because they reflect the state of the cells from which they originate. Exosomes are double phospholipid membrane structures that easily penetrate cells and perform various physiological and pathological functions such as immune response and signal transduction.

Peony is the root of the cultivar Hambak and San peony, which are perennial herbs belonging to the Ranunculaceae family. It has astringent and antipyretic effects and is effective in relieving pain, and is widely applied to bruises and abdominal pain caused by them.

Angelica gigas Nakai is the root of Angelica gigas Nakai, a perennial aromatic herb belonging to the Apiaceae family. Its components include essential oil and pyranocoumarins such as decursinol, decursin, nadakenetin, umbelliferone, beta-sitosterol and other water-soluble non-volatile substances. It contains crystalline substances and is widely used for physical weakness, headaches, abdominal pain, and constipation.

Rehmannia glutinosa is the root of fresh Rehmannia glutinosa Libschitz var. purpurea Makino or Rehmannia glutinosa Liboschitz var. purpurea Makino, and is used to treat conditions such as dry stomach due to lack of essence in the body, bleeding symptoms due to dry stomach, dry mouth, etc. It is known to rule.

In the present invention, exosomes prepared from peony, Angelica root, and Rehmannia glutinosa are used to apply them to a mist composition for hair care. Accordingly, it improves the texture and shine of the hair, prevents the destruction of the scalp moisturizing factor, and provides moisture and nutrition to the dry scalp, making the scalp healthy.

Next, the method for producing a mist composition for hair care according to the present invention includes the step of preparing fermented Schisandra chinensis seed extract and fermented buckwheat seed extract. The step of preparing the fermented Schisandra seed extract and the fermented buckwheat seed extract includes washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; And a step of filtering and concentrating the extract under reduced pressure and then freeze-drying it.

Schisandra chinensis is known to be effective in improving blood circulation by purifying the blood and reducing the formation of blood clots. It is known that more than 85% of the lignan content of Schisandra chinensis is contained in Schisandra seeds, and that only by using Schisandra seeds can you enjoy proper anti-cancer and antioxidant effects.

Buckwheat seeds germinate well even in dry land, have a short growing period of 60 to 100 days, and are particularly strong at adapting to poor environments. It grows in cool and moderately rainy areas, with mild conditions in the early stages of growth, not high temperatures and little rain during the flowering and maturation stages. However, because the growing season is short and the adaptability to climate is strong, it can be cultivated anywhere except central soil up to 70 degrees north latitude, so its cultivation range is very wide.

In the present invention, extracts are prepared after fermentation using Schisandra chinensis seeds and buckwheat seeds, and the extracts are applied to a mist composition for hair care. Accordingly, it improves the texture and shine of the hair, prevents the destruction of the scalp moisturizing factor, and provides moisture and nutrition to the dry scalp, making the scalp healthy.

Next, the method for producing the mist composition for hair care according to the present invention is 3-7 parts by weight of glycerin, 1-5 parts by weight of the camellia seed oil, jojoba seed oil and argan kernel oil prepared above, and 0.3-3 parts by weight of panthenol. parts, 0.3-3 parts by weight of phytantriol, 1-5 parts by weight of PEG-12 dimethicone, 1-5 parts by weight of PEG-3 caprylyl ether, 0.3-3 parts by weight of geraniol, and 18 parts by weight of ethanol. -22 parts by weight are mixed and stirred for 3-7 minutes at a temperature of 38-42°C and a rotation speed of 400-600 rpm to prepare a first mixture.

In the above step, the first mixture is prepared by mixing glycerin, camellia seed oil, jojoba seed oil, and argan kernel oil using ethanol.

More preferably, the mixture is stirred at a temperature of 39-41°C and a rotation speed of 450-550 rpm for 4-6 minutes.

Next, the method for producing the mist composition for hair care according to the present invention is 1-5 parts by weight of peony-derived exosomes, angelica root exosomes, and Rehmannia glutinosa-derived exosomes prepared above, Schisandra chinensis seed fermented extract, and buckwheat prepared above. 0.5-4 parts by weight of seed fermentation extract, 3-7 parts by weight of cyclopentasiloxane, 1-5 parts by weight of C12-15 alkyl benzoate, 1-5 parts by weight of phenyltrimethicone, 1-5 parts by weight of citric acid, Mix 0.3-3 parts by weight of benzyl benzoate, 0.3-3 parts by weight of benzyl salicylate, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of fragrance, and 11-15 parts by weight of broccoli water. , and preparing a second mixture by stirring for 3-7 minutes at a temperature of 48-52°C and a rotation speed of 700-900 rpm.

In the above step, a second mixture is prepared by mixing exosomes, fermentation extract, cyclopentasiloxane, etc. using broccoli water.

Broccoli not only contains a large amount of antioxidant beta-carotene, rutin, ascorbic acid, selenium, quercetin, and glutathione, but also contains nutrients such as calcium, vitamin C, and folic acid, which are used for skin care.

More preferably, the mixture is stirred at a temperature of 49-51°C and a rotation speed of 750-850 rpm for 4-6 minutes.

The fragrance is 18-22 parts by weight of lemon verbena oil, 18-22 parts by weight of vanilla oil, 8-12 parts by weight of mandarin oil, 2-6 parts by weight of hexyl salicylate, 18-22 parts by weight of dioctyl adipate, and propylene glycol. It preferably contains 1-5 parts by weight, 1-5 parts by weight of butylphenylmethylpropional, and 18-22 parts by weight of ethanol, 19-21 parts by weight of lemon verbena oil, 19-21 parts by weight of vanilla oil, and 9-9 parts by weight of mandarin oil. Contains 11 parts by weight, 3-5 parts by weight of hexyl salicylate, 19-21 parts by weight of dioctyl adipate, 2-4 parts by weight of propylene glycol, 2-4 parts by weight of butylphenylmethylpropional, and 19-21 parts by weight of ethanol. It is more desirable to do so.

Lemon verbena is a perennial shrub plant of the Verbena family. In China, it is called Yeongmong Verbena, and other names include deodorizing tree and perfume tree. In modern times, lemon verbena is used as an ornamental plant, functional herbal tea, and as a raw material for soap due to its refreshing scent similar to lemon.

Vanilla (Vanilla Planifolia) is an orchid plant native to tropical America and Mexico, and the fruit part is usually called vanilla bean. In the present invention, vanilla bean is used to include processed black vanilla beans with a unique scent obtained through a processing process of steaming and drying vanilla beans (vanilla beans) several times.

Mandarin, also called mandarin orange, contains vitamin P, ascorbic acid, carotenoid, limonoid flavonoid, coumarin, and naringenin family components. Among them, the naringenin family is a component found in the peel of mandarin. It is an ingredient with excellent antioxidant properties and plays an important role in preventing the proliferation of microorganisms that occur when it comes in contact with oxygen.

In the present invention, lemon verbena oil, vanilla bean oil, mandarin oil, and hexyl salicylate can be used as natural ingredients to provide a luxurious scent.

The hexyl salicylate is a colorless liquid with a green, floral, and spicy scent, and is often used to create the characteristic floral scent of floral combination fragrances.

The dioctyl adipate, propylene glycol, butylphenylmethylpropional, and ethanol are used as solvents to stabilize and easily disperse the fragrance.

Next, the method for producing a mist composition for hair care according to the present invention involves mixing the first mixture and the second mixture and stirring for 13-17 minutes at a rotation speed of 400-600 rpm at a temperature of 43-47 ° C. Includes steps.

More preferably, the mixture is stirred at a temperature of 44-46°C and a rotation speed of 450-550 rpm for 14-16 minutes.

Hereinafter, the present invention will be explained in more detail by the following examples.

However, the following examples only illustrate the content of the present invention and the scope of the invention is not limited by the examples and experimental examples.

<Preparation Example 1> Production of camellia seed oil, jojoba seed oil, and argan kernel oil

Camellia seeds, jojoba seeds, and argan kernels were crushed to prepare camellia seed powder, jojoba seed powder, and argan kernel powder. A mixed powder was prepared by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1. An extract was prepared by mixing 10 g of the mixed powder and 60 g of hexane and stirring for 3 days at a temperature of 30°C. The process of filtering, concentrating under reduced pressure, and centrifuging to remove foreign substances was repeated. By repeating the final reduced-pressure distillation, the residual solvent, hexane, was removed to less than 0.1 ppm, thereby producing camellia seed oil, jojoba seed oil, and argan kernel oil.

<Preparation Example 2> Preparation of exosomes derived from peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa

Peonies, Angelica gigas, and Rehmannia glutinosa were washed, placed in an ultra-high pressure machine, and pretreated for 5 minutes at a temperature of 20°C and a pressure of 150 MPa. Pretreated peony, Angelica gigas, and Rehmannia glutinosa were squeezed using a juicer to prepare a mixed juice. The mixed juice was centrifuged at 10,000xg for 10 minutes, and the supernatant was obtained. The supernatant was freeze-dried at a temperature of -50°C for 8 hours to prepare a lyophilisate. An aqueous two-phase system was formed using an aqueous solution of 3.3% by weight of polyethylene glycol with a weight average molecular weight of 10,000-35,000 and dextran with a weight average molecular weight of 400,000-500,000 at a concentration of 1.7% by weight in the freeze-dried product. The lower layer containing concentrated exosomes in the aqueous two-phase system was obtained to prepare exosomes derived from peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa.

<Preparation Example 3> Preparation of fermented Schisandra chinensis seed extract and buckwheat seed fermented extract

Schisandra seeds and buckwheat seeds were washed three times with boiled water and ground to prepare Schisandra chinensis seed powder and buckwheat seed powder. A mixture was prepared by mixing 20 parts by weight of Schisandra chinensis seed powder, 20 parts by weight of buckwheat seed powder, and 60 parts by weight of water, and 1 part by weight of Saccharomyces cerevisiae as a yeast was added to the mixture, followed by 40 parts by weight. Fermentation was carried out for 36 hours at a temperature of ℃. 300 g of butylene glycol was mixed with the fermented mixture and stirred for 5 days at a temperature of 30° C. to prepare an extract. The extract was filtered, concentrated under reduced pressure, and then freeze-dried to prepare Schisandra chinensis seed fermented extract and buckwheat seed fermented extract.

<Preparation Example 4> Preparation of fragrance

20 parts by weight of lemon verbena oil, 20 parts by weight of vanilla oil, 10 parts by weight of mandarin oil, 4 parts by weight of hexyl salicylate, 20 parts by weight of dioctyl adipate, 3 parts by weight of propylene glycol, 3 parts by weight of butylphenylmethylpropional, and A fragrance was prepared by mixing 20 parts by weight of ethanol.

<Example 1> Preparation of mist composition for hair care-1

5 parts by weight of glycerin, 3 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared in Preparation Example 1, 1 part by weight of panthenol, 1 part by weight of phytantriol, 3 parts by weight of PEG-12 dimethicone , 3 parts by weight of PPG-3caprylyl ether, 1 part by weight of geraniol, and 20 parts by weight of ethanol were mixed and stirred for 5 minutes at a rotation speed of 500 rpm at a temperature of 40°C to prepare a first mixture. .

Cyclopentasiloxane 5 parts by weight, C12-15 alkyl benzoate 3 parts by weight, phenyl trimethicone 3 parts by weight, citric acid 3 parts by weight, benzyl benzoate 1 part by weight, benzyl salicylate 1 part by weight, limonene 1 parts by weight, 1 part by weight of linalool, 3 parts by weight of the fragrance prepared in Preparation Example 4, and 18 parts by weight of ethanol were mixed and stirred for 5 minutes at a rotation speed of 800 rpm at a temperature of 50° C. to prepare a second mixture. .

The first mixture and the second mixture were mixed and stirred for 15 minutes at a temperature of 45°C and a rotation speed of 500 rpm to prepare a mist composition for hair care.

<Example 2> Preparation of perfume composition-2

5 parts by weight of glycerin, 3 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared in Preparation Example 1, 1 part by weight of panthenol, 1 part by weight of phytantriol, 3 parts by weight of PEG-12 dimethicone , 3 parts by weight of PPG-3caprylyl ether, 1 part by weight of geraniol, and 20 parts by weight of ethanol were mixed and stirred for 5 minutes at a rotation speed of 500 rpm at a temperature of 40°C to prepare a first mixture. .

3 parts by weight of peony-derived exosomes, angelica root exosomes, and Rehmannia glutinosa-derived exosomes prepared in Preparation Example 2, 2 parts by weight of Schisandra chinensis seed fermented extract and buckwheat seed fermented extract prepared in Preparation Example 3, 5 cyclopentasiloxane Parts by weight, C12-15 alkylbenzoate 3 parts by weight, phenyl trimethicone 3 parts by weight, citric acid 3 parts by weight, benzyl benzoate 1 part by weight, benzyl salicylate 1 part by weight, limonene 1 part by weight, linalool A second mixture was prepared by mixing 1 part by weight, 3 parts by weight of the flavor prepared in Preparation Example 4, and 13 parts by weight of broccoli water, and stirring for 5 minutes at a rotation speed of 800 rpm at a temperature of 50°C.

The first mixture and the second mixture were mixed and stirred for 15 minutes at a temperature of 45°C and a rotation speed of 500 rpm to prepare a mist composition for hair care.

<Experimental Example 1> Analysis of feeling of use and preference

In order to evaluate the hair conditioning effect after use of the hair care mist compositions of Examples 1 and 2, hairtress panel evaluation was performed in the following manner.

A hairtress weighing 5.3-5.5 g and length 20 cm was washed five times using 1 g of a 15% solution of sodium laureth sulfate, an anionic surfactant, and then dried. After spraying each composition three times on a dry hair brush, a hair usability test was conducted on 20 women and men aged 20-40 years, and the results were evaluated based on the evaluation items below to evaluate the usability of each product. It is shown in Table 1 below.

(9 points: very good, 7 points: good, 5 points: average, 3 points: bad, 1 point: very bad)

Hair feel (combing) shine Moisturizing power Comprehensive preference Example 1 8.0 8.2 8.2 8.1 Example 2 8.4 8.5 8.5 8.5

As shown in Table 1, it was confirmed that the mist composition for hair care according to the present invention had excellent palatability and excellent hair texture, shine, and moisturizing power.

Claims (2)

Preparing camellia seed powder, jojoba seed powder, and argan kernel powder by crushing camellia seeds, jojoba seeds, and argan kernels; Preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder at a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring for 2-4 days at a temperature of 28-32°C; and filtering the extract, concentrating it under reduced pressure, centrifuging it to remove foreign substances, and then distilling it under reduced pressure; preparing camellia seed oil, jojoba seed oil, and argan kernel oil, including;
Washing peony, Angelica and Rehmannia glutinosa and pre-treating them at a temperature of 18-22°C and a pressure of 140-160 MPa for 3-7 minutes; Preparing a mixed juice by mixing pretreated peony, angelica root and Rehmannia glutinosa at a weight ratio of 1:1:1 and extracting the juice; Centrifuging the mixed juice to obtain a supernatant containing exosomes; Preparing a lyophilisate by lyophilizing the supernatant containing the exosomes; Forming an aqueous two-phase system using polyethylene glycol/dextran in the freeze-dried product; and obtaining a lower layer liquid in which exosomes in the aqueous two-phase system are concentrated; preparing exosomes derived from Peony, exosomes derived from Angelica gigas, and exosomes derived from Rehmannia glutinosa, including;
Washing Schisandra chinensis seeds and buckwheat seeds with boiled water and pulverizing them to prepare Schisandra chinensis seed powder and buckwheat seed powder; Prepare a mixture by mixing 18-22 parts by weight of Schisandra chinensis seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water, and add 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture. and then fermenting at a temperature of 38-42°C for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring for 4-6 days at a temperature of 28-32°C; And filtering and concentrating the extract under reduced pressure and then freeze-drying; preparing a fermented Schisandra seed extract and a fermented buckwheat seed extract including;
Lemon verbena oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 8-12 parts by weight, hexyl salicylate 2-6 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1-5 Preparing a fragrance by mixing 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol;
3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 Die Mix 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3 caprylyl ether, 0.3-3 parts by weight of geraniol, and 18-22 parts by weight of ethanol, and incubate at 400°C at a temperature of 38-42°C. Preparing a first mixture by stirring for 3-7 minutes at a rotation speed of 600 rpm;
1-5 parts by weight of peony-derived exosomes, angelica root exosomes, and Rehmannia glutinosa-derived exosomes prepared above, 0.5-4 parts by weight of Schisandra chinensis seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 Parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of the flavor prepared above, and 11-15 parts by weight of broccoli water were mixed, and the mixture was heated at 700-900 rpm at a temperature of 48-52°C. Preparing a second mixture by stirring for 3-7 minutes at a rotation speed of; and
Mixing the first mixture and the second mixture, and stirring for 13-17 minutes at a temperature of 43-47°C and a rotation speed of 400-600 rpm. delete