KR102528583B1 - Mist composition for hair care - Google Patents

Abstract

Cyclopentasiloxane, C12-15 alkylbenzoate, phenyltrimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, blood Provided is a mist composition for hair care containing sebum-3 caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance and ethanol.

Description

Mist composition for hair care {Mist composition for hair care}

The present invention relates to a mist composition for hair care.

Hair is composed of medulla, cortex, and cuticle, and most of the hair is cortex composed of keratin protein. When the keratin protein of Cortex is lost, the hair becomes weak along with symptoms such as brittle hair and hair breakage.

The hair cuticle is a thin layer on the outermost layer of the hair that is stacked in layers to protect the keratin protein of the cortex. When the hair cuticle is protected and improved, the keratin protein in the cortex can be protected from external stimuli such as perm, dye, and dryer, and at the same time, it can be managed as smooth and shiny hair.

On the other hand, there is known a hair treatment composition that is filled in a container and discharged in the form of a mist by a pump dispenser or a trigger dispenser. When the composition is discharged in the form of a mist, the composition can be uniformly applied to the hair over a wide area, and the drooping from the hair after application is suppressed, so the feeling of use is excellent.

Conventionally, in the hair treatment composition discharged in the form of a mist, hairdressing performance or conditioning performance is provided depending on the composition design.

Patent Document 1: Korean Registered Patent No. 10-2339025

The present invention was made to solve the above problems, and an object of the present invention is to provide a mist composition for hair care with excellent overall preference in terms of hair texture, gloss, moisturizing power, and fragrance.

The object of the present invention is not limited to the tasks mentioned above, and other tasks not mentioned will be clearly understood by those skilled in the art from the following description.

In order to achieve the above object, the present invention

Cyclopentasiloxane, C12-15 alkylbenzoate, phenyltrimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, PPG-3 A mist composition for hair care containing caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance and ethanol is provided.

In addition, the present invention

preparing camellia seed powder, jojoba seed powder, and argan kernel powder by grinding camellia seeds, jojoba seeds, and argan kernel; preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring at a temperature of 28-32 ° C for 2-4 days; Preparing camellia seed oil, jojoba seed oil, and argan kernel oil comprising; filtering and concentrating the extract under reduced pressure, centrifuging to remove foreign substances, and distilling under reduced pressure;

Washing peony, Angelica gigas and Rehmannia glutinosa and pre-treating them at a temperature of 18-22° C. and a pressure of 140-160 MPa for 3-7 minutes; Mixing the pretreated peony, Angelica gigas and Rehmannia glutinosa in a weight ratio of 1:1:1 and extracting the mixture to prepare a mixed juice; Obtaining a supernatant containing exosomes by centrifuging the mixed juice; preparing a lyophilisate by freeze-drying the supernatant containing the exosomes; forming an aqueous two-phase system using polyethylene glycol/dextran in the lyophilisate; and obtaining a lower layer in which exosomes are concentrated in the aqueous two-phase system;

Preparing Schizandra seed powder and buckwheat seed powder by washing Schizandra seeds and buckwheat seeds with boiled water and grinding them; 18-22 parts by weight of Schisandra seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water were mixed to prepare a mixture, and 1 part by weight of Saccharomyces cerevisiae as a yeast was added to the mixture. After fermentation at a temperature of 38-42 ° C. for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 4-6 days; Preparing a fermented Schisandra seed extract and buckwheat seed extract containing; and freeze-drying the extract after filtering and concentrating under reduced pressure;

3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 die 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3caprylyl ether, 0.3-3 parts by weight of geraniol and 18-22 parts by weight of ethanol were mixed, and the preparing a first mixture by stirring for 3-7 minutes at a rotational speed of 600 rpm;

1-5 parts by weight of peony-derived exosomes prepared above, Angelica-derived exosomes and Rehmannia-derived exosomes, 0.5-4 parts by weight of Schisandra seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of fragrance, and 11-15 parts by weight of broccoli water were mixed, and at a rotational speed of 700-900 rpm at a temperature of 48-52 ° C. stirring for 3-7 minutes to prepare a second mixture; and

Mixing the first mixture and the second mixture and stirring for 13-17 minutes at a rotational speed of 400-600 rpm at a temperature of 43-47 ° C. .

In addition, the fragrance includes 18-22 parts by weight of lemon verbena oil, 18-22 parts by weight of vanilla oil, 8-12 parts by weight of mandarin oil, 2-6 parts by weight of hexyl salicylate, 18-22 parts by weight of dioctyl adipate, It is characterized in that it comprises 1-5 parts by weight of propylene glycol, 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol.

The mist composition for hair care according to the present invention is excellent in overall preference for hair feel, gloss, moisturizing power, fragrance, and the like.

Hereinafter, various embodiments are described in more detail. The embodiments described in this specification may be modified in various ways. Certain embodiments may be described in detail in the Detailed Description. However, the specific embodiments disclosed are only intended to facilitate understanding of various embodiments. Therefore, the technical idea is not limited by the specific embodiments disclosed, and it should be understood to include all equivalents or substitutes included in the spirit and technical scope of the invention.

Terms including ordinal numbers such as primary, secondary, first, and second may be used to describe various elements, but these elements are not limited by the above-mentioned terms. The terminology described above is only used for the purpose of distinguishing one component from another.

In this specification, terms such as 'comprise' or 'having' are intended to designate that there is a feature, number, step, operation, component, part, or combination thereof described in the specification, but one or more other features It should be understood that the presence or addition of numbers, steps, operations, components, parts, or combinations thereof is not precluded. It is understood that when a component is referred to as being 'connected' or 'connected' to another component, it may be directly connected or connected to the other component, but other components may exist in the middle. It should be. On the other hand, when a component is referred to as being 'directly connected' or 'directly connected' to another component, it should be understood that no other component exists in the middle.

In addition, in describing the present invention, if it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be abbreviated or omitted.

the present invention

Cyclopentasiloxane, C12-15 alkylbenzoate, phenyltrimethicone, glycerin, camellia seed oil, jojoba seed oil, argan kernel oil, panthenol, phytantriol, PEG-12 dimethicone, PPG-3 A mist composition for hair care containing caprylyl ether, citric acid, benzyl benzoate, benzyl salicylate, limonene, geraniol, linalool, fragrance and ethanol is provided.

The mist composition for hair care according to the present invention is excellent in overall preference for hair feel, gloss, moisturizing power, fragrance, and the like.

With the above camellia seed oil, jojoba seed oil, and argan kernel oil, you can have healthier and more shiny hair.

The combination of panthenol and phytantriol has a hair heat protection effect.

In addition, the present invention

preparing camellia seed powder, jojoba seed powder, and argan kernel powder by grinding camellia seeds, jojoba seeds, and argan kernel; preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring at a temperature of 28-32 ° C for 2-4 days; Preparing camellia seed oil, jojoba seed oil, and argan kernel oil comprising; filtering and concentrating the extract under reduced pressure, centrifuging to remove foreign substances, and distilling under reduced pressure;

Washing peony, Angelica gigas and Rehmannia glutinosa and pre-treating them at a temperature of 18-22° C. and a pressure of 140-160 MPa for 3-7 minutes; Mixing the pretreated peony, Angelica gigas and Rehmannia glutinosa in a weight ratio of 1:1:1 and extracting the mixture to prepare a mixed juice; Obtaining a supernatant containing exosomes by centrifuging the mixed juice; preparing a lyophilisate by freeze-drying the supernatant containing the exosomes; forming an aqueous two-phase system using polyethylene glycol/dextran in the lyophilisate; and obtaining a lower layer in which exosomes are concentrated in the aqueous two-phase system;

Preparing Schizandra seed powder and buckwheat seed powder by washing Schizandra seeds and buckwheat seeds with boiled water and grinding them; 18-22 parts by weight of Schisandra seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water were mixed to prepare a mixture, and 1 part by weight of Saccharomyces cerevisiae as a yeast was added to the mixture. After fermentation at a temperature of 38-42 ° C. for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 4-6 days; Preparing a fermented Schisandra seed extract and buckwheat seed extract containing; and freeze-drying the extract after filtering and concentrating under reduced pressure;

3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 die 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3caprylyl ether, 0.3-3 parts by weight of geraniol and 18-22 parts by weight of ethanol were mixed, and the preparing a first mixture by stirring for 3-7 minutes at a rotational speed of 600 rpm;

1-5 parts by weight of peony-derived exosomes prepared above, Angelica-derived exosomes and Rehmannia-derived exosomes, 0.5-4 parts by weight of Schisandra seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of fragrance, and 11-15 parts by weight of broccoli water were mixed, and at a rotational speed of 700-900 rpm at a temperature of 48-52 ° C. stirring for 3-7 minutes to prepare a second mixture; and

Mixing the first mixture and the second mixture and stirring for 13-17 minutes at a rotational speed of 400-600 rpm at a temperature of 43-47 ° C. .

Hereinafter, the manufacturing method of the mist composition for hair care according to the present invention will be described in detail for each step.

First, the method for producing a mist composition for hair care according to the present invention includes preparing camellia seed oil, jojoba seed oil, and argan kernel oil. The step of preparing the camellia seed oil, jojoba seed oil, and argan kernel oil includes preparing camellia seed powder, jojoba seed powder, and argan kernel powder by grinding camellia seed, jojoba seed, and argan kernel; preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring at a temperature of 28-32 ° C for 2-4 days; And filtering the extract, concentrating under reduced pressure, centrifuging to remove foreign substances, and then distilling under reduced pressure.

The camellia seed oil has an excellent effect of preventing rancidity while supplying unsaturated fatty acids, etc., and also supplies a large amount of active ingredients such as oleic acid and oleic acid triglyceride to improve the skin barrier function and prevent moisture loss. It is known to alleviate fine wrinkles, and realize excellent antibacterial properties, skin elasticity enhancement, and antioxidant effects.

The jojoba seed oil has a structure of wax ester, which is a component of sebum, and has a structure of wax ester, which is a component of sebum, and has a less oily feeling than other vegetable oils. It is known to act to improve the moisturizing effect that helps prevent moisture loss by forming a moisture film on the skin.

The argan kernel oil contains abundant vitamin E, which infuses vitality and vitality into tired skin, makes the skin texture flexible and soft, and is rich in omega 6 constituting cell membranes, so it is known to have excellent skin moisturizing and regenerating effects. .

In the present invention, camellia seed oil, jojoba seed oil and argan kernel oil are applied to the mist composition for hair care. Accordingly, it can improve the texture and gloss of the hair, prevent the destruction of the scalp moisturizing factor, and provide moisture and nutrition to the dry scalp to make the scalp healthy.

Next, the method for preparing the mist composition for hair care according to the present invention includes preparing peony-derived exosomes, angelica-derived exosomes, and Rehmannia Root-derived exosomes. The step of preparing peony-derived exosomes, Angelica-derived exosomes, and Rehmannia Root-derived exosomes is pre-treated for 3-7 minutes at a temperature of 18-22 ° C and a pressure of 140-160 MPa by washing the peony, Angelica and Rehmannia Root step; Mixing the pretreated peony, Angelica gigas and Rehmannia glutinosa in a weight ratio of 1:1:1 and extracting the mixture to prepare a mixed juice; Obtaining a supernatant containing exosomes by centrifuging the mixed juice; preparing a lyophilisate by freeze-drying the supernatant containing the exosomes; forming an aqueous two-phase system using polyethylene glycol/dextran in the lyophilisate; and obtaining a lower layer in which exosomes are concentrated in the aqueous two-phase system.

Exosome refers to a small membrane-structured vesicle secreted from various cells, and is defined as a type of extracellular vesicles (EVs). All cells exchange information with other cells or the external environment and secrete extracellular endoplasmic reticulum for this purpose. Exosomes have a size of about 50 to 200 nm and contain physiologically active substances such as proteins, lipids, and nucleic acids. Exosomes exist in various cells such as mammals, bacteria, and plants, and can be used for diagnosis and treatment because they reflect the state of the originating cells. Exosomes are a double-phospholipid membrane structure that is easily penetrated into cells and performs various physiological and pathological functions such as immune response and signal transduction.

Peony is a perennial plant belonging to the Buttercup family, a cultivated plant species, and the root of mountain peony.

Angelica gigas Nakai is the root of a perennial aromatic herb belonging to the Apiaceae family. Its components are essential oils and pyranocoumarin-based decurcinol, decursine, nadakenetin, umbelliferon, beta-sitosterol and other water-soluble nonvolatiles. It contains crystal substances, etc., and is widely applied to physical weakness, headache, abdominal pain, and constipation.

Rehmannia glutinosa is the root of Saengjihwang (Rehmannia glutinosa Libschitz var. purpurea Makino) or Rehmannia glutinosa Liboschitz var. purpurea Makino. It is known to govern

In the present invention, exosomes prepared from Peony, Angelica, and Rehmannia are applied to a mist composition for hair care. Accordingly, it can improve the texture and gloss of the hair, prevent the destruction of the scalp moisturizing factor, and provide moisture and nutrition to the dry scalp to make the scalp healthy.

Next, the method for producing a mist composition for hair care according to the present invention includes preparing a fermented extract of Schisandra seed and a fermented extract of buckwheat seed. The step of preparing the fermentation extract of Schizandra seed and fermented buckwheat seed extract is to prepare Schisandra seed and buckwheat seed powder and buckwheat seed powder by washing and grinding Schisandra seed and buckwheat seed with boiled water; 18-22 parts by weight of Schisandra seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water were mixed to prepare a mixture, and 1 part by weight of Saccharomyces cerevisiae as a yeast was added to the mixture. After fermentation at a temperature of 38-42 ° C. for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 4-6 days; and lyophilizing the extract after filtering and concentrating under reduced pressure.

Schisandra chinensis is known to have the effect of improving blood circulation by purifying the blood and reducing the formation of blood clots. It is known that more than 85% of the lignan content of Schisandra chinensis is contained in Schisandra seeds, so that proper effects such as anti-cancer and antioxidant effects can be enjoyed only when Schisandra seeds are used.

Buckwheat seeds sprout well even in dry land, have a short growth period of 60 to 100 days, and have a particularly strong ability to adapt to poor environments. It grows in a cool and moderately rainy area. It is mild in the early stage of growth, and it is not hot and there is little rain in the flowering period. However, because of its short growing season and strong adaptability to the climate, it can be cultivated anywhere except central soil up to 70 degrees north latitude, and its cultivation range is very wide.

In the present invention, extracts are prepared after fermentation using Schisandra seeds and buckwheat seeds, and applied to a mist composition for hair care. Accordingly, it can improve the texture and gloss of the hair, prevent the destruction of the scalp moisturizing factor, and provide moisture and nutrition to the dry scalp to make the scalp healthy.

Next, the method for preparing the mist composition for hair care according to the present invention includes 3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, and 0.3-3 parts by weight of panthenol. phytantriol 0.3-3 parts by weight, PEG-12 dimethicone 1-5 parts by weight, PPG-3 caprylyl ether 1-5 parts by weight, geraniol 0.3-3 parts by weight and ethanol 18 Mixing -22 parts by weight and stirring for 3-7 minutes at a rotational speed of 400-600 rpm at a temperature of 38-42 ° C to prepare a first mixture.

In the above step, a first mixture is prepared, and glycerin, camellia seed oil, jojoba seed oil, and argan kernel oil are mixed with ethanol.

More preferably, the mixture is stirred for 4-6 minutes at a rotational speed of 450-550 rpm at a temperature of 39-41°C.

Next, the method for producing a mist composition for hair care according to the present invention includes 1-5 parts by weight of peony-derived exosomes, angelica-derived exosomes, and Rehmannia Root-derived exosomes prepared above, the fermented extract of Schisandra seed prepared above, and buckwheat Seed fermentation extract 0.5-4 parts by weight, cyclopentasiloxane 3-7 parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyltrimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, 0.3-3 parts by weight of benzyl benzoate, 0.3-3 parts by weight of benzyl salicylate, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of fragrance and 11-15 parts by weight of broccoli water were mixed. , preparing a second mixture by stirring for 3-7 minutes at a rotational speed of 700-900 rpm at a temperature of 48-52 ° C.

In the above step, a second mixture is prepared, and exosomes, fermented extracts, and cyclopentasiloxane are mixed with broccoli water.

Broccoli contains a large amount of beta-carotene, rutin, ascorbic acid, selenium, quercetin, and glutathione, which have antioxidant effects, as well as nutrients such as calcium, vitamin C, and folic acid, so it is used for skin care.

More preferably, the mixture is stirred for 4-6 minutes at a rotational speed of 750-850 rpm at a temperature of 49-51°C.

The fragrance is lemon verbena oil 18-22 parts by weight, vanilla oil 18-22 parts by weight, mandarin oil 8-12 parts by weight, hexyl salicylate 2-6 parts by weight, dioctyl adipate 18-22 parts by weight, propylene glycol 1-5 parts by weight, preferably containing 1-5 parts by weight of butylphenylmethylpropional and 18-22 parts by weight of ethanol, 19-21 parts by weight of lemonverbena oil, 19-21 parts by weight of vanilla oil, 9-21 parts by weight of mandarin oil 11 parts by weight, 3-5 parts by weight of hexyl salicylate, 19-21 parts by weight of dioctyl adipate, 2-4 parts by weight of propylene glycol, 2-4 parts by weight of butylphenylmethylpropional and 19-21 parts by weight of ethanol It is more preferable to

Lemon Verbena is a perennial shrub plant of the Verbena family, and is called Youngmong Verbena in China, and other names include deodorant and perfume trees. In modern times, lemon verbena is used as an ornamental plant, functional herbal tea, and raw material for soaps because it has a refreshing scent similar to that of lemon.

Vanilla (Vanilla Planifolia) is an orchid plant native to Mexico, tropical America, and the fruit part is commonly called vanilla bean. In the present invention, vanilla bean is used as a meaning including vanilla processing beans having a unique aroma of black color obtained by steaming and drying vanilla fruits (vanilla beans) several times.

Mandarin, also known as mandarin orange, contains vitamin P, ascorbic acid, carotenoids, limonoid flavonoids, gumarin, and naringenin-type components. Among them, the component of the naringenin system is a component in the peel of mandarin.

In the present invention, lemon verbena oil, vanilla bean oil, mandarin oil and hexyl salicylate can be applied to exhibit a luxurious fragrance as natural raw materials.

The hexyl salicylate is a colorless liquid with a green, floral, and spicy scent, and is often used to make a characteristic floral scent of a floral combination spice.

The dioctyl adipate, propylene glycol, butylphenylmethylpropional, and ethanol are applied as solvents to stabilize and easily disperse the fragrance.

Next, the method for producing a mist composition for hair care according to the present invention is to mix the first mixture and the second mixture and stir for 13-17 minutes at a rotational speed of 400-600 rpm at a temperature of 43-47 ° C. Include steps.

More preferably, the mixture is stirred for 14-16 minutes at a rotational speed of 450-550 rpm at a temperature of 44-46°C.

Hereinafter, the present invention will be described in more detail by the following examples.

However, the following examples are merely illustrative of the content of the present invention, but the scope of the invention is not limited by the examples and experimental examples.

<Preparation Example 1> Preparation of camellia seed oil, jojoba seed oil and argan kernel oil

Camellia seeds, jojoba seeds, and argan kernels were pulverized to prepare camellia seed powder, jojoba seed powder, and argan kernel powder. A mixed powder was prepared by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1. An extract was prepared by mixing 10 g of the mixed powder and 60 g of hexane and stirring at a temperature of 30° C. for 3 days. After filtering and concentrating under reduced pressure, the process of centrifuging to remove foreign substances was repeated. By repeating the last vacuum distillation, residual solvent, hexane, was removed to less than 0.1 ppm, and through this, camellia seed oil, jojoba seed oil, and argan kernel oil were prepared.

<Preparation Example 2> Preparation of peony-derived exosomes, angelica-derived exosomes, and Rehmannia Root-derived exosomes

Peony, angelica, and Rehmannia were washed and put into an ultra-high pressure machine and pretreated at a temperature of 20°C and a pressure of 150 MPa for 5 minutes. The pre-treated peony, Angelica gigas and Rehmannia were squeezed using a juicer to prepare a mixed juice. After centrifuging the mixed juice at 10,000xg for 10 minutes, the supernatant was obtained. The supernatant was freeze-dried at -50 °C for 8 hours to prepare a lyophilisate. An aqueous two-phase system was formed using an aqueous solution containing 3.3% by weight of polyethylene glycol having a weight average molecular weight of 10,000 to 35,000 and 1.7% by weight of dextran having a weight average molecular weight of 400,000 to 500,000 to the lyophilisate. A lower layer in which exosomes were concentrated in the aqueous two-phase system was obtained to prepare peony-derived exosomes, angelica-derived exosomes, and Rehmannia Root-derived exosomes.

<Preparation Example 3> Preparation of Schizandra seed fermented extract and buckwheat seed fermented extract

Schisandra seeds and buckwheat seeds were washed three times with boiled water and pulverized to prepare Schisandra seed powder and buckwheat seed powder. A mixture was prepared by mixing 20 parts by weight of Schisandra seed powder, 20 parts by weight of buckwheat seed powder, and 60 parts by weight of water, and after adding 1 part by weight of Saccharomyces cerevisiae as a yeast to the mixture, 40 parts by weight It was fermented for 36 hours at a temperature of ° C. An extract was prepared by mixing 300 g of butylene glycol with the fermented mixture and stirring at a temperature of 30° C. for 5 days. The extract was filtered and concentrated under reduced pressure, and then freeze-dried to prepare fermented Schisandra seed extract and buckwheat seed fermented extract.

<Preparation Example 4> Preparation of perfume

20 parts by weight of lemonverbena oil, 20 parts by weight of vanilla oil, 10 parts by weight of mandarin oil, 4 parts by weight of hexyl salicylate, 20 parts by weight of dioctyl adipate, 3 parts by weight of propylene glycol, 3 parts by weight of butylphenylmethylpropional, and A perfume was prepared by mixing 20 parts by weight of ethanol.

<Example 1> Preparation of mist composition for hair care-1

5 parts by weight of glycerin, 3 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared in Preparation Example 1, 1 part by weight of panthenol, 1 part by weight of phytantriol, 3 parts by weight of PEG-12 dimethicone , 3 parts by weight of PPG-3 caprylyl ether, 1 part by weight of geraniol, and 20 parts by weight of ethanol were mixed, and stirred at a rotation speed of 500 rpm at a temperature of 40 ° C. for 5 minutes to prepare a first mixture. .

5 parts by weight of cyclopentasiloxane, 3 parts by weight of C12-15 alkylbenzoate, 3 parts by weight of phenyltrimethicone, 3 parts by weight of citric acid, 1 part by weight of benzyl benzoate, 1 part by weight of benzyl salicylate, 1 part by weight of limonene A second mixture was prepared by mixing 1 part by weight of Linalool, 3 parts by weight of the perfume prepared in Preparation Example 4, and 18 parts by weight of ethanol, and stirring at a temperature of 50 ° C. for 5 minutes at a rotational speed of 800 rpm. .

The first mixture and the second mixture were mixed and stirred at a rotational speed of 500 rpm at a temperature of 45° C. for 15 minutes to prepare a mist composition for hair care.

<Example 2> Preparation of perfume composition-2

5 parts by weight of glycerin, 3 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared in Preparation Example 1, 1 part by weight of panthenol, 1 part by weight of phytantriol, 3 parts by weight of PEG-12 dimethicone , 3 parts by weight of PPG-3 caprylyl ether, 1 part by weight of geraniol, and 20 parts by weight of ethanol were mixed, and stirred at a rotation speed of 500 rpm at a temperature of 40 ° C. for 5 minutes to prepare a first mixture. .

Peony-derived exosomes prepared in Preparation Example 2, Angelica-derived exosomes and Rehmannia-derived exosomes 3 parts by weight, Schizandra seed fermented extract and buckwheat seed fermented extract prepared in Preparation Example 3 2 parts by weight, Cyclopentasiloxane 5 parts by weight, 3 parts by weight of C12-15 alkylbenzoate, 3 parts by weight of phenyl trimethicone, 3 parts by weight of citric acid, 1 part by weight of benzyl benzoate, 1 part by weight of benzyl salicylate, 1 part by weight of limonene, linalool 1 part by weight, 3 parts by weight of the fragrance prepared in Preparation Example 4 and 13 parts by weight of broccoli water were mixed, and stirred for 5 minutes at a rotational speed of 800 rpm at a temperature of 50 ° C. to prepare a second mixture.

The first mixture and the second mixture were mixed and stirred at a rotational speed of 500 rpm at a temperature of 45° C. for 15 minutes to prepare a mist composition for hair care.

<Experimental Example 1> Analysis of feeling of use and preference

In order to evaluate the hair conditioning effect after use of the hair care mist compositions of Examples 1 and 2, the hairtress panel evaluation was conducted in the following manner.

A hairtress weighing 5.3-5.5 g and having a length of 20 cm was washed 5 times with 1 g of a 15% solution of sodium laureth sulfate, an anionic surfactant, and then dried. After spraying each composition on a dry hairtress three times, a hair usability test was conducted on 20 women and men aged 20-40 years, and the results of the evaluation of the usability of each product according to the following evaluation items It is shown in Table 1 below.

(9 points: very good, 7 points: good, 5 points: average, 3 points: poor, 1 point: very bad)

Hair texture (combing) shine moisturizing power comprehensive signage Example 1 8.0 8.2 8.2 8.1 Example 2 8.4 8.5 8.5 8.5

As shown in Table 1, it was confirmed that the mist composition for hair care according to the present invention had excellent palatability and excellent hair texture, gloss, and moisturizing power.

Claims (2)

preparing camellia seed powder, jojoba seed powder, and argan kernel powder by grinding camellia seeds, jojoba seeds, and argan kernel; preparing a mixed powder by mixing the camellia seed powder, jojoba seed powder, and argan kernel powder in a weight ratio of 1:1:1; Preparing an extract by mixing the mixed powder and hexane and stirring at a temperature of 28-32 ° C for 2-4 days; Preparing camellia seed oil, jojoba seed oil, and argan kernel oil comprising; filtering and concentrating the extract under reduced pressure, centrifuging to remove foreign substances, and distilling under reduced pressure;
Washing peony, Angelica gigas and Rehmannia glutinosa and pre-treating them at a temperature of 18-22° C. and a pressure of 140-160 MPa for 3-7 minutes; Mixing the pretreated peony, Angelica gigas and Rehmannia glutinosa in a weight ratio of 1:1:1 and extracting the mixture to prepare a mixed juice; Obtaining a supernatant containing exosomes by centrifuging the mixed juice; preparing a lyophilisate by freeze-drying the supernatant containing the exosomes; forming an aqueous two-phase system using polyethylene glycol/dextran in the lyophilisate; and obtaining a lower layer in which exosomes are concentrated in the aqueous two-phase system;
Preparing Schizandra seed powder and buckwheat seed powder by washing Schizandra seeds and buckwheat seeds with boiled water and grinding them; 18-22 parts by weight of Schisandra seed powder, 18-22 parts by weight of buckwheat seed powder, and 58-62 parts by weight of water were mixed to prepare a mixture, and 1 part by weight of Saccharomyces cerevisiae as a yeast was added to the mixture. After fermentation at a temperature of 38-42 ° C. for 34-38 hours; Preparing an extract by mixing the fermented mixture and butylene glycol and stirring at a temperature of 28-32 ° C. for 4-6 days; Preparing a fermented Schisandra seed extract and buckwheat seed extract containing; and freeze-drying the extract after filtering and concentrating under reduced pressure;
3-7 parts by weight of glycerin, 1-5 parts by weight of camellia seed oil, jojoba seed oil and argan kernel oil prepared above, 0.3-3 parts by weight of panthenol, 0.3-3 parts by weight of phytantriol, PEG-12 die 1-5 parts by weight of methicone, 1-5 parts by weight of PPG-3caprylyl ether, 0.3-3 parts by weight of geraniol and 18-22 parts by weight of ethanol were mixed, and the preparing a first mixture by stirring for 3-7 minutes at a rotational speed of 600 rpm;
1-5 parts by weight of peony-derived exosomes prepared above, Angelica-derived exosomes and Rehmannia-derived exosomes, 0.5-4 parts by weight of Schisandra seed fermented extract and buckwheat seed fermented extract prepared above, cyclopentasiloxane 3-7 parts by weight, C12-15 alkylbenzoate 1-5 parts by weight, phenyl trimethicone 1-5 parts by weight, citric acid 1-5 parts by weight, benzyl benzoate 0.3-3 parts by weight, benzyl salicylate 0.3-3 parts by weight parts by weight, 0.3-3 parts by weight of limonene, 0.3-3 parts by weight of linalool, 1-5 parts by weight of fragrance, and 11-15 parts by weight of broccoli water were mixed, and at a rotational speed of 700-900 rpm at a temperature of 48-52 ° C. stirring for 3-7 minutes to prepare a second mixture; and
Mixing the first mixture and the second mixture, and stirring for 13-17 minutes at a rotational speed of 400-600 rpm at a temperature of 43-47 ° C. Method for producing a mist composition for hair care comprising. delete