KR102359834B1 - 중합 방법 - Google Patents

중합 방법 Download PDF

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KR102359834B1
KR102359834B1 KR1020187037029A KR20187037029A KR102359834B1 KR 102359834 B1 KR102359834 B1 KR 102359834B1 KR 1020187037029 A KR1020187037029 A KR 1020187037029A KR 20187037029 A KR20187037029 A KR 20187037029A KR 102359834 B1 KR102359834 B1 KR 102359834B1
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reaction mixture
coolant
polymerization
section
loop
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KR20190026673A (ko
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에릭 도미니끄 데르
장-마르끄 갈레브스키
앙또니 시모엔
아르노 술라쥬
크리스띤 스코룹카
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이네오스 유럽 아게
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F10/04Monomers containing three or four carbon atoms
    • C08F10/08Butenes
    • C08F10/10Isobutene
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/242Tubular reactors in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/2425Tubular reactors in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/248Reactors comprising multiple separated flow channels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/248Reactors comprising multiple separated flow channels
    • B01J19/249Plate-type reactors
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F110/00Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F110/04Monomers containing three or four carbon atoms
    • C08F110/08Butenes
    • C08F110/10Isobutene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/001Multistage polymerisation processes characterised by a change in reactor conditions without deactivating the intermediate polymer
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/04Monomers containing three or four carbon atoms
    • C08F210/08Butenes
    • C08F210/10Isobutene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F4/00Polymerisation catalysts
    • C08F4/005Friedel-Crafts catalysts in general
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside
    • B01J2219/2401Reactors comprising multiple separate flow channels
    • B01J2219/245Plate-type reactors
    • B01J2219/2451Geometry of the reactor
    • B01J2219/2453Plates arranged in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside
    • B01J2219/2401Reactors comprising multiple separate flow channels
    • B01J2219/245Plate-type reactors
    • B01J2219/2451Geometry of the reactor
    • B01J2219/2456Geometry of the plates
    • B01J2219/2458Flat plates, i.e. plates which are not corrugated or otherwise structured, e.g. plates with cylindrical shape
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside
    • B01J2219/2401Reactors comprising multiple separate flow channels
    • B01J2219/245Plate-type reactors
    • B01J2219/2461Heat exchange aspects
    • B01J2219/2462Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polymerisation Methods In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
KR1020187037029A 2016-07-06 2017-06-23 중합 방법 Active KR102359834B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP16178240.4 2016-07-06
EP16178240 2016-07-06
PCT/EP2017/065492 WO2018007165A1 (en) 2016-07-06 2017-06-23 Polymerisation process

Publications (2)

Publication Number Publication Date
KR20190026673A KR20190026673A (ko) 2019-03-13
KR102359834B1 true KR102359834B1 (ko) 2022-02-07

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US (1) US11053331B2 (https=)
EP (1) EP3481547B1 (https=)
JP (1) JP7082579B2 (https=)
KR (1) KR102359834B1 (https=)
CN (1) CN109414675B (https=)
AR (1) AR108957A1 (https=)
BR (1) BR112019000022B1 (https=)
ES (1) ES2949523T3 (https=)
HU (1) HUE062160T2 (https=)
PL (1) PL3481547T3 (https=)
RU (1) RU2744598C2 (https=)
WO (1) WO2018007165A1 (https=)

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Publication number Priority date Publication date Assignee Title
JP7635122B2 (ja) * 2018-11-13 2025-02-25 ビーエーエスエフ ソシエタス・ヨーロピア プソイドイオノン及びヒドロキシプソイドイオノンを製造するための装置及び方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6252016B1 (en) 1997-12-19 2001-06-26 Rohm And Haas Company Continuous polymerization in a non-cylindrical channel with temperature control
US20020048541A1 (en) * 2000-08-17 2002-04-25 Linde Aktiengesellschaft Reactor for performing a strongly heat-conditioned catalytic reaction
US20140235801A1 (en) * 2011-10-26 2014-08-21 Tpc Group Llc Polyisobutylene Prepared at High Velocity and Circulation Rate

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SU1397457A1 (ru) * 1986-06-25 1988-06-15 Предприятие П/Я В-8415 Способ регулировани процесса растворной полимеризации изопрена
DE19520078A1 (de) * 1995-06-07 1996-12-12 Basf Ag Verfahren zur Herstellung von niedermolekularem, hochreaktivem Polyisobuten
EP0891381B2 (en) * 1996-04-01 2006-05-24 The Dow Chemical Company Olefin solution polymerization
DE19654806C2 (de) * 1996-12-31 2001-06-13 Axiva Gmbh Optimierung des Kühlwassersystems einer Polyolefinanlage
US6168765B1 (en) * 1998-09-08 2001-01-02 Uop Llc Process and apparatus for interbed injection in plate reactor arrangement
AU7123700A (en) 1999-09-16 2001-04-17 Texas Petrochemicals Lp Process for preparing polyolefin products
US6884858B2 (en) * 1999-10-19 2005-04-26 Texas Petrochemicals Lp Process for preparing polyolefin products
ATE415425T1 (de) 2004-08-13 2008-12-15 Kuraray Co Verfahren zur kontinuierlichen herstellung von (meth)acrylsäureesterpolymer oder copolymer
EP2017000B1 (en) 2007-07-11 2012-09-05 Corning Incorporated Process intensified microfluidic devices
US8043417B2 (en) * 2008-06-30 2011-10-25 Uop Llc Column installed condenser
EP2348057A1 (en) * 2010-01-21 2011-07-27 INEOS Manufacturing Belgium NV Novel polymers
JP6316308B2 (ja) 2012-12-10 2018-04-25 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 官能化されたポリイソブテンの製造法および該化合物の誘導体
CN103641939A (zh) * 2013-11-27 2014-03-19 河北科技大学 一种聚异丁烯的制备系统和制备方法
CN103641930B (zh) 2013-11-27 2016-09-07 威海市桢昊生物技术有限公司 一种利用酶法从菠萝皮、渣中提取果胶的方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6252016B1 (en) 1997-12-19 2001-06-26 Rohm And Haas Company Continuous polymerization in a non-cylindrical channel with temperature control
US20020048541A1 (en) * 2000-08-17 2002-04-25 Linde Aktiengesellschaft Reactor for performing a strongly heat-conditioned catalytic reaction
US20140235801A1 (en) * 2011-10-26 2014-08-21 Tpc Group Llc Polyisobutylene Prepared at High Velocity and Circulation Rate

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Publication number Publication date
JP7082579B2 (ja) 2022-06-08
WO2018007165A1 (en) 2018-01-11
JP2019519656A (ja) 2019-07-11
BR112019000022B1 (pt) 2023-04-25
US20190309103A1 (en) 2019-10-10
PL3481547T3 (pl) 2023-09-11
EP3481547C0 (en) 2023-06-07
EP3481547B1 (en) 2023-06-07
US11053331B2 (en) 2021-07-06
HUE062160T2 (hu) 2023-10-28
BR112019000022A2 (pt) 2019-04-02
CN109414675B (zh) 2021-11-16
CN109414675A (zh) 2019-03-01
RU2744598C2 (ru) 2021-03-11
AR108957A1 (es) 2018-10-10
ES2949523T3 (es) 2023-09-29
CA3029774A1 (en) 2018-01-11
RU2019102520A3 (https=) 2020-08-06
KR20190026673A (ko) 2019-03-13
RU2019102520A (ru) 2020-08-06
EP3481547A1 (en) 2019-05-15

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