KR102324554B1 - Jelly Toothpaste and Manufacturing Method of thereof - Google Patents

Abstract

The present invention relates to a jelly toothpaste and a method for preparing the same, comprising: an outer layer; and kernels provided inside the outer layer; Including, wherein the outer layer is 15-20 parts by weight of gelatin, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract based on 100 parts by weight of purified water Parts by weight, xylitol 40 to 45 parts by weight, propolis extract 5 to 10 parts by weight, pectin 10 to 15 parts by weight, L-menthol 5 to 10 parts by weight, glycerin 1 to 3 parts by weight, and astaxanthin 10 to 15 parts by weight It is a technical feature to include, and by having grains inside the outer layer, there is an advantage of excellent cleaning power during brushing, and there is an advantage of protecting the gums.

Description

Jelly toothpaste and manufacturing method thereof

The present invention relates to a jelly toothpaste and a method for manufacturing the same, and more particularly, to a jelly toothpaste that has excellent cleaning power during brushing and can protect the gums, and a method for manufacturing the same.

Toothpaste is a drug compound that is used by putting it on a toothbrush for the purpose of cleaning and polishing the teeth, and it is in the form of powder, cream, liquid, etc. It is made to help in the prevention or treatment of disinfection, calculus dissolving, odor reduction, and tooth decay or pyorrhea. As a component, the base can be mentioned first. Calcium carbonate, calcium phosphate, calcium sulfate, magnesium carbonate, magnesium chloride and the like are used for this. These are helpful for mechanical cleaning of teeth. If the size, hardness, and shape of the particles are not suitable, there is a risk of damaging the surface of the teeth. It should not be sensitive, and the hardness should be about 3 degrees Mohs hardness.

In addition to this base, cleaning agents, flavoring agents, coloring agents, sterilizing agents, tartar dissolving agents, neutralizing agents, etc. are mixed little by little. In addition to the cream type, binders and stabilizers are added.

In other words, paste toothpaste is widely used as a toothpaste used for cleaning the oral cavity and teeth. Often there will be no In addition, the toothpaste remaining inside the tube cannot be completely used in the process of use, and the tube into which the toothpaste is injected is disposable and must be discarded every time, so there is a problem of severe waste and environmental pollution.

In order to solve this problem, a liquid toothpaste that can be used relatively sparingly and the container can be reused has been proposed. However, such a liquid toothpaste is not used in reality due to the problem that the liquid toothpaste composition easily flows down during use, which is very inconvenient and wasteful.

Republic of Korea Patent Publication No. 10-1272225 (2013.06.11.) discloses a jelly toothpaste and a manufacturing method thereof.

Since the jelly toothpaste breaks without sagging, it has an advantage that it can be cut more comfortably when applied to a toothbrush, but has a disadvantage in that it has insufficient cleaning power.

KR 10-1272225 B1 2013.06.11.

An object of the present invention is to provide a jelly toothpaste excellent in cleaning power when brushing, and a method for preparing the same.

Another object of the present invention is to provide a jelly toothpaste that can protect the gums when brushing, and a method for preparing the same.

In order to achieve the above object, the present invention provides the following means.

The present invention, the outer layer; and kernels provided inside the outer layer; Including, wherein the outer layer is 15-20 parts by weight of gelatin, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract based on 100 parts by weight of purified water Parts by weight, xylitol 40 to 45 parts by weight, propolis extract 5 to 10 parts by weight, pectin 10 to 15 parts by weight, L-menthol 5 to 10 parts by weight, glycerin 1 to 3 parts by weight, and astaxanthin 10 to 15 parts by weight The hydroxyapatite has an average particle diameter of 1 to 500 nm, and the kernels provided in the outer layer are 15 to 20 parts by weight of gelatin, 5 to 10 parts by weight of hydroxyapatite, 1 to lemon juice based on 100 parts by weight of purified water. 5 parts by weight, 1 to 5 parts by weight of calcium carbonate, 3 to 7 parts by weight of grape seed extract, and 30 to 35 parts by weight of xylitol, it provides a jelly toothpaste.

The outer layer further comprises 0.1 to 1 parts by weight of stevia aged in 100 parts by weight of purified water, wherein the aged stevia is 0.1 to 1 parts by weight of Bacillus natto and 1 to 5 parts by weight of purified bioceramic stone to 100 parts by weight of stevia. Aging for 20-30 days at 10-15°C, the bioceramic stone purified water is added to 100 parts by weight of water and 1-5 parts by weight of the bioceramic stone and left for 10-14 hours, and the bioceramic stone is 40 to pearlite A mixture containing 50% by weight, 25 to 35% by weight of sericite and 20 to 30% by weight of loess is put into water, kneaded and aged, and then calcined at a temperature of 1,300 to 1,400° C. for 1 to 2 hours.

The kernels additionally include 0.1 to 1 part by weight of baekhwago extract and fermented product in 100 parts by weight of purified water, wherein the fermented baekhwago extract is 600 to 700 parts by weight of complex brine added to 100 parts by weight of baekhwago and at 90 to 95° C. for 4 to 6 hours After extraction, 5 to 10 parts by weight of synthetic synthetic bacteria are added to 100 parts by weight of the baekhwago extract and fermented at 35 to 40° C. for 46 to 48 hours. The complex brine is water 95% by weight, magnetic salt 3% by weight, bamboo salt 1% by weight and 1% by weight of green tea salt, and the magnetic salt is deposited by heating and concentrating seawater at 160 to 180° C. for 4 to 5 days in a cauldron, and the bamboo salt is sun-dried salt in a bamboo barrel with one side blocked, and the entrance is made of loess. After sealing, it is heated at 1,000~1,200℃ for 10~12 hours, and the green seaweed salt is put into 100 parts by weight of sea salt solution and 20~30 parts by weight of green seaweed and heated at 110~120℃ for 10~12 hours. The salinity is 25 to 30% by weight, and the composite synthetic bacteria comprises 40 to 50% by weight of Honggukgyun, 20 to 30% by weight of Bacillus subtilis, 10 to 20% by weight of yeast, and 5 to 15% by weight of yeast.

In addition, the present invention, manufacturing the outer layer (step 1); preparing kernels (step 2): and providing the kernels inside the outer layer (step 3); including, but in step 1, the outer layer is prepared by stirring gelatin and fruit juice at 100° C. in a weight ratio of 1:1 to make a gelatin solution (S 1); 15-20 parts by weight of the gelatin solution, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Part, xylitol 40-45 parts by weight, propolis extract 5-10 parts by weight, pectin 10-15 parts by weight, L-menthol 5-10 parts by weight, glycerin 1-3 parts by weight and astaxanthin 10-15 parts by weight vacuum Mixing for 20-30 minutes in the state (S 2); and cooling the mixture at 15-20° C. for 20-25 minutes (S 3); Including, in S 1, the fruit juice contains 60% by weight of kiwi juice and 40% by weight of mango juice, and in S 2, the grape seed extract is 20-30 parts by weight of grape seeds with respect to 100 parts by weight of water in a water bath, and internal mixing is maintained at 40 ~ 45 ℃ and extracted by heating in hot water for 10 ~ 12 hours, and the propolis extract is added with 10 ~ 20 parts by weight of propolis based on 100 parts by weight of 70% (v/v) ethanol and 65 through a reflux extraction tube. It provides a method for producing a jelly toothpaste, in which extraction is performed under reflux at ~70°C for 6 to 8 hours.

In step 2, the kernels are prepared by mixing gelatin and vegetable juice at 100° C. in a weight ratio of 1:1 to make a gelatin solution (A 1); 15-20 parts by weight of the gelatin solution, 5-10 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 3-7 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Mixing parts and 30 to 35 parts by weight of xylitol in a vacuum for 20 to 30 minutes (A 2); and injecting the mixture into a silicone mold and molding at 10 to 12° C. for 3 to 4 hours (A 3); Including, wherein the vegetable juice of A 1 contains 60% by weight of carrot juice and 40% by weight of tomato juice, and in step 3, the kernels are put in a molding mold and the outer layer is poured, and then 3 at 10-12°C. Mold for ~4 hours.

The jelly toothpaste according to the present invention has an advantage in that it has excellent cleaning power when brushing teeth by having grains inside the outer layer.

In addition, the jelly toothpaste according to the present invention has the advantage of protecting the gums when brushing teeth.

Hereinafter, the present invention will be described in detail.

First, a jelly toothpaste according to the present invention will be described.

The jelly toothpaste of the present invention,

outer layer; and

kernels provided inside the outer layer;

includes

The outer layer is 15-20 parts by weight of gelatin, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract, xylitol based on 100 parts by weight of purified water 40 to 45 parts by weight, 5 to 10 parts by weight of propolis extract, 10 to 15 parts by weight of pectin, 5 to 10 parts by weight of L-menthol, 1 to 3 parts by weight of glycerin, and 10 to 15 parts by weight of astaxanthin.

When less than 15 parts by weight of gelatin is included with respect to 100 parts by weight of the purified water, there is a problem in that it is difficult to obtain a jelly formulation, and when it contains more than 20 parts by weight, there is a problem that the toothpaste becomes hard.

When less than 25 parts by weight of hydroxyapatite is included with respect to 100 parts by weight of the purified water, there is a problem in that the cleaning power is deteriorated, and when it is included in more than 30 parts by weight, there is a problem of damaging the gums.

The hydroxide apatite preferably has an average particle diameter of 1 to 500 nm. If the average particle diameter is less than 1 nm, aggregation of the particles is severe and the viscosity is greatly increased, making it impossible to use as a toothpaste. There is this.

When less than 1 part by weight of lemon juice is included with respect to 100 parts by weight of the purified water, there is a problem of poor palatability, and when more than 5 parts by weight is included, there is a problem in that the lemon flavor is too strong.

When less than 1 part by weight of calcium carbonate is included with respect to 100 parts by weight of the purified water, there is a problem in that the toothpaste does not show abrasiveness, so the plaque cleaning power is insufficient, and when it contains more than 5 parts by weight, there is a problem of damaging the gums.

When less than 5 parts by weight of grape seed extract is included with respect to 100 parts by weight of the purified water, there is a problem in that the cleaning power is lowered, and when it is included in more than 10 parts by weight, there is a problem of interfering with iron absorption.

The grape seed (Grape seed) is rich in polyphenols and exhibits antioxidant and cholesterol-suppressing effects, is excellent for anti-aging, and contains catechins to have detoxification and sterilization and anti-cancer effects, and to enhance skin elasticity, Prevents aging.

If less than 40 parts by weight of xylitol is included with respect to 100 parts by weight of the purified water, there is a problem in that the caries prevention effect is lowered, and when it contains more than 45 parts by weight, digestive disorders may occur.

The xylitol is a sugar alcohol having a refreshing feeling and is widely used as a caries prevention material that inhibits the growth of Streptococcus mutans, a plaque-forming bacterium, to reduce lactic acid production and inhibit the formation of insoluble glucan. Because xylitol is a pentose alcohol, it is not used by oral bacteria and does not cause tooth decay. Unlike other sweeteners, only xylitol has this effect.

When less than 5 parts by weight of the propolis extract is included with respect to 100 parts by weight of the purified water, there is a problem in that the cleaning power is lowered, and when it is included in more than 10 parts by weight, inflammation in the mouth may occur.

The propolis is collected from the sap of trees, the bark of fruit trees, and the stamens of flowers by bees, and is a substance used for self-defense of bees or repair of the hive, mainly resin, beeswax, essential oil, pollen, various organic substances and minerals. It is composed of substances and has antibacterial, antifungal, antiviral, antitumor, and wound healing properties as well as antioxidant action. Various organic and mineral substances in propolis contain a large amount of flavonoids, and these flavonoids show strong antibacterial effects. The flavonoids of propolis are all aglycones, which is different from flavonoids of other plants, and this advantage is involved in the antibacterial action of propolis. In addition, since propolis does not have an antibacterial action against intestinal bacteria, it has no adverse effect on the intestinal flora useful to the human body, that is, bifidobacteria or lactic acid bacteria, even when administered orally. Therefore, propolis is a very safe natural antibacterial substance that is not toxic no matter how much it is ingested.

When less than 10 parts by weight of pectin is included with respect to 100 parts by weight of the purified water, there is a problem in that it is difficult to obtain a jelly formulation, and when more than 15 parts by weight is included, there is a problem that the toothpaste becomes hard.

When less than 5 parts by weight of L-menthol is included with respect to 100 parts by weight of the purified water, there is a problem that it does not sufficiently serve as a flavoring agent, and when it contains more than 10 parts by weight, there is a problem of stimulating the stomach.

When less than 1 part by weight of glycerin is included with respect to 100 parts by weight of the purified water, there is a problem that it does not sufficiently act as a wetting agent, and when it contains more than 3 parts by weight, there is a problem of stimulating the stomach.

When astaxanthin is included in less than 10 parts by weight with respect to 100 parts by weight of the purified water, there is a problem in that it does not sufficiently act as an antioxidant, and when it is included in more than 15 parts by weight, there is a problem that the skin turns yellow.

The outer layer may additionally include 0.1 to 1 parts by weight of aged stevia in 100 parts by weight of purified water.

The outer layer has the advantage of improving the palatability by including stevia aged in purified water.

To the aged stevia, 0.1 to 1 parts by weight of Bacillus natto and 1 to 5 parts by weight of purified bioceramic stone water are added to 100 parts by weight of stevia and aged at 10 to 15° C. for 20 to 30 days.

The bioceramic stone purified water is prepared by adding 1 to 5 parts by weight of the bioceramic stone to 100 parts by weight of water and leaving it to stand for 10 to 14 hours.

The bioceramic stone is a mixture containing 40 to 50% by weight of pearlite, 25 to 35% by weight of sericite, and 20 to 30% by weight of loess in water, kneaded and aged, and then 1 to at a temperature of 1,300 to 1,400 ° C. Firing for 2 hours.

The bacilli present in natto straw bacteria (Bacillus natto) is attached to the approximately 10 million at a straw bundle, and the size of the bacteria has a length 2.33 microns, a width of 1 micron and has a property to form spores for the preservation of the species .

The present invention is characterized in that the cleaning power is improved by providing the grains inside the outer layer.

It is preferable that 45-50 parts by weight of the kernels provided in the outer layer are included with respect to 100 parts by weight of the outer layer.

If the amount of grains provided inside the outer layer is less than 45 parts by weight with respect to 100 parts by weight of the outer layer, the cleaning power may decrease, and if it exceeds 50 parts by weight, there is a problem in that the feel is inferior.

The kernels provided inside the outer layer are 15-20 parts by weight of gelatin, 5-10 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 3 parts by weight of grape seed extract, based on 100 parts by weight of purified water. 7 parts by weight and 30 to 35 parts by weight of xylitol.

The kernel may additionally contain 0.1 to 1 part by weight of fermented white baekhwago extract in 100 parts by weight of purified water.

The kernel has the advantage of being able to protect the gums when brushing by including the fermented baekhwago extract in purified water.

The baekhwago contains a large amount of protein, various amino acids, vitamin B, vitamin D, minerals, etc., and helps prevent skin aging through antioxidant action that removes free radicals that promote skin aging, atopic dermatitis and acne It contains lentinen, an anti-cancer and anti-tumor polysaccharide substance, which improves skin diseases such as inflammation, eczema, and melasma, and helps to increase immunity, suppress the proliferation of cancer cells, and prevent high blood cancer. In addition, vitamins B1, B2, It contains a large amount of ergosterine of vitamin D, which strengthens bones and promotes absorption of calcium and phosphorus.

The fermented baekhwago extract is added 600-700 parts by weight of complex brine to 100 parts by weight of baekhwago, extracted at 90-95° C. for 4-6 hours, and 5-10 parts by weight of complex synthetic bacteria is added to 100 parts by weight of baekhwago extract and 35- Fermented at 40°C for 46-48 hours.

The complex salt water includes 95% by weight of water, 3% by weight of magnetic salt, 1% by weight of bamboo salt, and 1% by weight of seaweed salt.

The magnetic salt is deposited by heating and concentrating seawater in a cauldron at 160-180°C for 4-5 days,

The bamboo salt is heated at 1,000 to 1,200 ° C for 10 to 12 hours after putting sea salt in a bamboo barrel blocked on one side and sealing the entrance with ocher,

The green seaweed salt is added to 100 parts by weight of sea salt, 20 to 30 parts by weight of green seaweed, and heated at 110 to 120° C. for 10 to 12 hours, and the salinity of the sea salt is preferably 25 to 30% by weight.

The composite synthetic bacteria comprises 40-50% by weight of Honggukgyun, 20-30% by weight of Bacillus subtilis, 10-20% by weight of yeast, and 5-15% by weight of yeast.

The complex synthetic bacteria is a concept of mixing Hong Guk-gyun, Bacillus subtilis, Hyogo and Koji-gyun, and by mixing in this way, the production of complex active enzymes is possible.

The Hong Guk-gyun is a red filamentous fungus belonging to the genus Ascomycetes Monascus, and produces dark red pigment and monacolin K as various beneficial metabolites in the process of fermenting grains such as rice. This fungus has been used for a long time as a natural food coloring agent or processed product, as well as a material for promoting digestion and improving blood flow in various regions of East Asia, including China. Mebinoline, a secondary metabolite produced by Hong Guk-gyun, strongly inhibits HMG-CoA (3-hydroxy-methyl-3-glutaryl-coenzyme) reductase, a cholesterol biosynthetic enzyme, thereby reducing blood lipid concentration and inhibiting cholesterol synthesis. It has various functions such as antifungal, suppression of blood sugar rise, blood pressure control, anti-obesity, and anti-cancer. In addition, Hong Guk-gyun produces red pigments (rubropuntain, monascorubin), yellow pigments (monascin, ankaflavin), purple pigments (rubropunctamine, monascorubramine), etc., and these pigments have antibacterial and anticancer effects.

The Hong Guk-gyun is Monascus pilosus ( Monascus pilosus ), Monascus rubber ( Monascus ruber ), Monascus purpureus ), Monascus kaoliang ( Monascus kaoliang ), Monascus barykery ( Monascus barykery ) and Monascus barykery ) Any one selected from the group consisting of Monascus anka may be used.

The Bacillus subtilis ( B. subtilis ), Bacillus lichneformis ( B. lichneformis ), Bacillus megaterium ( B. megaterium ), Bacillus amyloliquefaciens ( B. amyloliquefaciens ), Bacillus natto ( B . natto), Bacillus la Alliance system (B.antharcis), Bacillus alkylene tooth (B.lentus), Bacillus mirror's buffer (B.pumilus), Bacillus rendering if N-Sys (B.thuringiensis), Bacillus al bay (B.alvei ), Bacillus azo topic Sans (B.azotofixans), Bacillus maese lance (B.macerans), Bacillus Poly miksa (B.polymyxa), Bacillus papil Rie (B.popilliae), Bacillus core posts lance (B.coagulans), Bacillus Stearothermophilus ( B. stearothermophilus ), Bacillus pasteurii ( B.pasteurii ), Bacillus paricus ( B.sphaericus ) and Bacillus pastidiosus ( B.fastidiosus ) Any one selected from the group consisting of may be used.

Wherein the yeast is made to my process Lucy (Saccharomyces rouxii), three Levy cyano as Saccharomyces My process as Saccharomyces (Saccharomyces cereviciae), my process Ob pole miss in Saccharomyces (Saccharomyces oviformis) and My process stay Neri (Saccharomyces steineri) in Saccharomyces Any one selected from the group may be used.

The yeast may use any one selected from the group consisting of Aspergillus oryzae (Aspergillus oryzae) and Aspergillus sojae (Aspergillus sojae).

The jelly toothpaste according to the present invention has an advantage in that it has excellent cleaning power when brushing teeth by having grains inside the outer layer.

In addition, the jelly toothpaste according to the present invention has the advantage of protecting the gums when brushing teeth.

Next, a method for manufacturing a jelly toothpaste according to the present invention will be described.

The manufacturing method of the jelly toothpaste according to the present invention,

preparing an outer layer (step 1);

preparing kernels (step 2): and

providing the kernels inside the outer layer (step 3);

includes

In step 1, the outer layer,

Stirring gelatin and fruit juice at 100° C. in a weight ratio of 1:1 to make a gelatin solution (S 1);

15-20 parts by weight of the gelatin solution, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Part, xylitol 40-45 parts by weight, propolis extract 5-10 parts by weight, pectin 10-15 parts by weight, L-menthol 5-10 parts by weight, glycerin 1-3 parts by weight and astaxanthin 10-15 parts by weight vacuum Mixing for 20-30 minutes in the state (S 2); and

cooling the mixture at 15-20° C. for 20-25 minutes (S 3);

includes

In S 1, the fruit juice includes 60% by weight of kiwi juice and 40% by weight of mango juice.

In S 2, the grape seed extract is preferably extracted by putting 20 to 30 parts by weight of grape seeds in a water bath with respect to 100 parts by weight of water, maintaining the internal mixing ratio at 40 to 45° C., and heating for 10 to 12 hours.

The propolis extract is preferably added to 10-20 parts by weight of propolis with respect to 100 parts by weight of 70% (v/v) ethanol and refluxed extraction at 65-70° C. for 6-8 hours through a reflux extraction tube.

In step 2, the kernels,

Stirring gelatin and vegetable juice at 100° C. in a weight ratio of 1:1 to prepare a gelatin solution (A 1);

15-20 parts by weight of the gelatin solution, 5-10 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 3-7 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Mixing parts and 30 to 35 parts by weight of xylitol in a vacuum for 20 to 30 minutes (A 2); and

Putting the mixture into a silicone mold and molding at 10 to 12° C. for 3 to 4 hours (A 3);

includes

The vegetable juice of A 1 includes 60% by weight of carrot juice and 40% by weight of tomato juice.

Step 3 is a step of molding at 10 to 12° C. for 3 to 4 hours after putting the kernels in a mold and pouring the outer layer.

In step 1, 0.1 to 1 part by weight of stevia aged in 100 parts by weight of purified water may be additionally included in the preparation of the outer layer.

To the aged stevia, 0.1 to 1 parts by weight of Bacillus natto and 1 to 5 parts by weight of purified bioceramic stone water are added to 100 parts by weight of stevia and aged at 10 to 15° C. for 20 to 30 days.

The bioceramic stone purified water is prepared by adding 1 to 5 parts by weight of the bioceramic stone to 100 parts by weight of water and leaving it to stand for 10 to 14 hours.

The bioceramic stone is a mixture containing 40 to 50% by weight of pearlite, 25 to 35% by weight of sericite, and 20 to 30% by weight of loess in water, kneaded and aged, and then 1 to at a temperature of 1,300 to 1,400 ° C. Firing for 2 hours.

In step 2, 0.1 to 1 part by weight of fermented baekhwago extract may be additionally included in 100 parts by weight of purified water when preparing the kernels.

The fermented baekhwago extract is added 600-700 parts by weight of complex brine to 100 parts by weight of baekhwago, extracted at 90-95° C. for 4-6 hours, and 5-10 parts by weight of complex synthetic bacteria is added to 100 parts by weight of baekhwago extract and 35- Fermented at 40°C for 46-48 hours.

The complex salt water includes 95% by weight of water, 3% by weight of magnetic salt, 1% by weight of bamboo salt, and 1% by weight of seaweed salt.

The magnetic salt is deposited by heating and concentrating seawater in a cauldron at 160-180°C for 4-5 days,

The bamboo salt is heated at 1,000 to 1,200 ° C for 10 to 12 hours after putting sea salt in a bamboo barrel blocked on one side and sealing the entrance with ocher,

The green seaweed salt is added to 100 parts by weight of sea salt, 20 to 30 parts by weight of green seaweed, and heated at 110 to 120° C. for 10 to 12 hours, and the salinity of the sea salt is preferably 25 to 30% by weight.

The composite synthetic bacteria comprises 40 to 50% by weight of Honggukgyun, 20 to 30% by weight of Bacillus subtilis, 10 to 20% by weight of yeast, and 5 to 15% by weight of yeast.

Hereinafter, the configuration and effects of the present invention will be described in more detail through examples. These examples are only for illustrating the present invention, and the scope of the present invention is not limited by these examples.

Gelatin and fruit juice at 100° C. were stirred at a weight ratio of 1:1 to prepare a gelatin solution. The fruit juice was mixed with 60% by weight of kiwi juice and 40% by weight of mango juice. Based on 100 parts by weight of purified water at 80° C., 20 parts by weight of the gelatin solution, 30 parts by weight of hydroxide apatite, 5 parts by weight of lemon juice, 5 parts by weight of calcium carbonate, 10 parts by weight of grape seed extract, 45 parts by weight of xylitol, 10 parts by weight of propolis extract Parts, 15 parts by weight of pectin, 10 parts by weight of L-menthol, 3 parts by weight of glycerin and 15 parts by weight of astaxanthin were mixed in a vacuum for 20 minutes to prepare a mixture. As the hydroxide apatite, those having an average particle diameter of 1 to 500 nm were used. The grape seed extract was extracted by putting 20 parts by weight of grape seeds in a water bath with respect to 100 parts by weight of water and heating the water for 10 hours while maintaining the internal mixing ratio at 40°C. The propolis extract was extracted with 20 parts by weight of propolis based on 100 parts by weight of 70% (v/v) ethanol and refluxed at 70° C. for 8 hours through a reflux extraction tube. The mixture was cooled at 15° C. for 20 minutes to prepare an outer layer.

Gelatin and vegetable juice at 100° C. were stirred at a weight ratio of 1:1 to prepare a gelatin solution. The vegetable juice was mixed with 60% by weight of carrot juice and 40% by weight of tomato juice. Based on 100 parts by weight of purified water at 80° C., 20 parts by weight of the gelatin solution, 10 parts by weight of hydroxide apatite, 5 parts by weight of lemon juice, 5 parts by weight of calcium carbonate, 7 parts by weight of grape seed extract and 35 parts by weight of xylitol in a vacuum state for 20 minutes mixed to make a mixture. The mixture was put into a silicone mold and molded at 10° C. for 3 hours to prepare kernels.

50 parts by weight of the kernels were put in a mold, 100 parts by weight of the outer layer was poured, and then molded at 10° C. for 3 hours to prepare a jelly toothpaste.

In Example 1, except that 1 part by weight of aged stevia was additionally included in 100 parts by weight of purified water when preparing the outer layer and 1 part by weight of fermented baekhwago extract was additionally included in 100 parts by weight of purified water when preparing the kernels. Jelly toothpaste was prepared.

The aged stevia was aged at 15° C. for 30 days by adding 1 part by weight of Bacillus natto bacteria and 5 parts by weight of purified bioceramic stone water to 100 parts by weight of stevia. The bioceramic stone purified water was prepared by adding 5 parts by weight of the bioceramic stone to 100 parts by weight of water and leaving it to stand for 14 hours. The bioceramic stone was prepared by mixing a mixture containing pearlite 50% by weight, sericite 30% by weight and loess 20% by weight in water, kneading it, and then calcining it at a temperature of 1,400° C. for 2 hours.

The fermented baekhwago extract was prepared by adding 700 parts by weight of complex salt to 100 parts by weight of baekhwago, extracting at 95°C for 6 hours, adding 10 parts by weight of complex synthetic bacteria to 100 parts by weight of baekhwago extract, and fermenting at 35°C for 48 hours. . The complex brine was mixed with 95% by weight of water, 3% by weight of magnetic salt, 1% by weight of bamboo salt, and 1% by weight of seaweed salt. The magnetic salt was deposited by heating and concentrating seawater at 180° C. for 5 days in a cauldron. The bamboo salt was prepared by putting sea salt in a bamboo barrel with one side blocked, sealing the entrance with ocher, and heating it at 1,200° C. for 10 hours. The green tea salt was prepared by adding 20 parts by weight of green tea to 100 parts by weight of sea salt solution and heating at 110° C. for 10 hours. The salinity of the sea salt solution was 25% by weight.

The composite synthetic bacteria were mixed with 50% by weight of Honggukgyun, 30% by weight of Bacillus subtilis, 15% by weight of yeast, and 5% by weight of yeast. The Hong Guk-gyun used Monascus pilosus, the Bacillus subtilis was used for the Bacillus subtilis , and the yeast Saccharomyces rouxii was used, and the yeast was used. Aspergillus oryzae ( Aspergillus oryzae ) was used.

[Comparative Example 1]

Silicon dioxide (ABSIL 73K) 11.25% by weight, silicon dioxide (MFIL 43K) 6.5% by weight, methyl paraoxybenzoate 0.15% by weight, sodium carboxymethylcellulose 0.7% by weight, polyethylene glycol 1.5% by weight, stevioside 0.1% by weight, xylitol powder 0.1% by weight, ascorbic acid 0.01% by weight, erythritol 0.25% by weight, chitosan 0.01% by weight, sodium monofluorophosphate 0.05% by weight, tocopheryl acetate 0.01% by weight, sorbitol solution 55% by weight, glycerin 5% by weight, purified water 13.6% by weight % into the sample machine. Purified water was administered after stopping at about 80°C. The ingredients put into the sample machine were mixed in a vacuum to form a paste. A toothpaste formulation was created by mixing the powder and liquid ingredients to a certain extent. Then, 2.8% by weight of gelatin was dissolved in hot water to make a liquid, and then put into a toothpaste made into a paste before hardening at room temperature and mixed in a vacuum. Then, 1% by weight of sodium lauryl sulfate was dissolved in 0.97% by weight of ethanol, and mixed again with the liquid phase in a vacuum. After mixing to some extent, 1% by weight of a strawberry flavoring agent was added and mixed to prepare a jelly toothpaste.

[Experimental Example 1]

For the jelly toothpaste prepared in Examples 1 and 2 and Comparative Example 1, formulation, convenience, preference, cleaning power, gum protection degree, and foam amount were tested, and the results are shown in Table 1. The formulation was evaluated by visually observing the shape of the final product. Convenience was evaluated by visually observing whether toothpaste was cut or sagged when applied. Cleaning power, degree of gum protection, and preference were evaluated by surveying 50 children aged 8 to 13 years old. The amount of foam was evaluated by visually observing the amount of foam produced when brushing teeth.

Example 1 Example 2 Comparative Example 1 formulation jelly jelly jelly when applied to the toothbrush broken broken broken taste preference 46 people 48 people 46 people scent preference 48 people 48 people 48 people tactile preference 45 people 45 people 45 people detergency 40 people 45 people 30 people Gum protection 38 people 43 people 25 people amount of foam less less less

According to Table 1, it can be seen that the jelly toothpastes of Examples 1 and 2 are superior to the jelly toothpaste of Comparative Example 1 in cleaning power and gum protection degree.

Claims (5)

outer layer; and
kernels provided inside the outer layer;
including,
The outer layer is 15-20 parts by weight of gelatin, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract, xylitol based on 100 parts by weight of purified water 40 to 45 parts by weight, 5 to 10 parts by weight of propolis extract, 10 to 15 parts by weight of pectin, 5 to 10 parts by weight of L-menthol, 1 to 3 parts by weight of glycerin and 10 to 15 parts by weight of astaxanthin,
The hydroxide apatite has an average particle diameter of 1-500 nm,
The kernels provided inside the outer layer are 15-20 parts by weight of gelatin, 5-10 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 3 parts by weight of grape seed extract, based on 100 parts by weight of purified water. 7 parts by weight and 30 to 35 parts by weight of xylitol,
jelly toothpaste.
The method of claim 1,
The outer layer further comprises 0.1 to 1 part by weight of stevia aged in 100 parts by weight of purified water,
The aged stevia is added 0.1 to 1 parts by weight of Bacillus natto and 1 to 5 parts by weight of purified bioceramic stone water to 100 parts by weight of stevia and aged at 10 to 15° C. for 20 to 30 days,
The bioceramic stone purified water is added to 100 parts by weight of water and 1 to 5 parts by weight of the bioceramic stone and left for 10 to 14 hours,
The bioceramic stone is a mixture containing 40 to 50% by weight of pearlite, 25 to 35% by weight of sericite, and 20 to 30% by weight of loess in water, kneaded and aged, and then 1 to at a temperature of 1,300 to 1,400 ° C. calcined for 2 hours,
jelly toothpaste.
The method of claim 1,
The kernels additionally include 0.1 to 1 part by weight of fermented white baekhwago extract in 100 parts by weight of purified water,
The fermented baekhwago extract is added 600-700 parts by weight of complex brine to 100 parts by weight of baekhwago, extracted at 90-95° C. for 4-6 hours, and 5-10 parts by weight of complex synthetic bacteria is added to 100 parts by weight of baekhwago extract and 35- Fermented at 40°C for 46-48 hours,
The complex brine contains 95% by weight of water, 3% by weight of magnetic salt, 1% by weight of bamboo salt, and 1% by weight of seaweed salt,
The magnetic salt is deposited by heating and concentrating seawater in a cauldron at 160-180°C for 4-5 days,
The bamboo salt is heated at 1,000 to 1,200 ° C for 10 to 12 hours after putting sea salt in a bamboo barrel blocked on one side and sealing the entrance with ocher,
The green seaweed salt is added to 100 parts by weight of sea salt solution and 20 to 30 parts by weight of green seaweed is heated at 110 to 120° C. for 10 to 12 hours, and the salinity of the sea salt water is 25 to 30 weight percent,
The complex synthetic bacteria comprises 40 to 50% by weight of Hong Guk bacteria, 20 to 30% by weight of Bacillus subtilis, 10 to 20% by weight of yeast, and 5 to 15% by weight of yeast,
jelly toothpaste.
preparing an outer layer (step 1);
preparing kernels (step 2): and
providing the kernels inside the outer layer (step 3);
including,
In step 1, the outer layer,
Stirring gelatin and fruit juice at 100° C. in a weight ratio of 1:1 to make a gelatin solution (S 1);
15-20 parts by weight of the gelatin solution, 25-30 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 5-10 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Part, xylitol 40-45 parts by weight, propolis extract 5-10 parts by weight, pectin 10-15 parts by weight, L-menthol 5-10 parts by weight, glycerin 1-3 parts by weight and astaxanthin 10-15 parts by weight vacuum Mixing for 20-30 minutes in the state (S 2); and
cooling the mixture at 15-20° C. for 20-25 minutes (S 3);
includes,
In S 1, the fruit juice contains 60% by weight of kiwi juice and 40% by weight of mango juice,
In S 2, the grape seed extract is extracted by putting 20 to 30 parts by weight of grape seeds in a water bath with respect to 100 parts by weight of water, maintaining the internal temperature at 40 to 45° C., and heating for 10 to 12 hours,
The propolis extract is extracted under reflux for 6-8 hours at 65-70°C with a reflux extraction tube into 10-20 parts by weight of propolis based on 100 parts by weight of 70% (v/v) ethanol,
Method for manufacturing jelly toothpaste.
5. The method of claim 4,
In step 2, the kernels,
Stirring gelatin and vegetable juice at 100° C. in a weight ratio of 1:1 to prepare a gelatin solution (A 1);
15-20 parts by weight of the gelatin solution, 5-10 parts by weight of hydroxide apatite, 1-5 parts by weight of lemon juice, 1-5 parts by weight of calcium carbonate, 3-7 parts by weight of grape seed extract with respect to 100 parts by weight of purified water at 80-85°C Mixing parts and 30 to 35 parts by weight of xylitol in a vacuum for 20 to 30 minutes (A 2); and
Putting the mixture into a silicone mold and molding at 10 to 12° C. for 3 to 4 hours (A 3);
including,
The vegetable juice of A 1 contains 60% by weight of carrot juice and 40% by weight of tomato juice,
The step 3 is to put the kernels in a mold, pour the outer layer, and then mold at 10 to 12 ℃ for 3 to 4 hours,
Method for manufacturing jelly toothpaste.