KR102166517B1 - Composition for expressing the fragrance of kerria - Google Patents

Abstract

The present invention relates to a composition for reproducing the scent of yellow plum, and specifically, to a composition for reproducing the scent of yellow plum, which reproduces the unique scent of yellow plum without damaging the natural yellow plum, and improves user preference.
The composition for reproducing the smell of yellow plum according to the present invention can reproduce the unique scent of yellow plum by adjusting the composition based on the components of the yellow plum analyzed by the head space method, and at the same time provide excellent palatability to users. have.

Description

Composition for expressing the fragrance of kerria {Composition for expressing the fragrance of kerria}

The present invention relates to a composition for reproducing the scent of yellow plum blossoms, and specifically, to a composition for reproducing the scent of yellow plums in which the original scent of yellow plums is reproduced as it is and improved palatability without damaging the natural yellow plums.

Plum belongs to the cherry tree family and refers to the flowers of plum trees or plum trees. Plum blossoms bloom before the leaves, but with the blooming, they give off a clear scent. Plum blossoms have a unique and subtle scent that cannot be easily forgotten once smelled, and many attempts have been made to reproduce the scent of plum.

Yellow plum is a type of plum, growing lush in humid places, weak in shade, and about 2m high. The leaves of the yellow plum are alternate, long egg-shaped, and have double teeth at the edge. Yellow plum blossoms bloom from April to May in yellow and like leaves.

Gapsa Duck Forest in Gyeryongsan National Park, Chungcheongnam-do, is famous as the largest yellow plum community in Korea, and its flower shape resembles plum blossoms and is characterized by an elegant and elegant scent.

Existing fragrance components include a solvent extraction method in which an organic solvent is used to form Absolute, and a steam distillation method in which the fragrance component is made into essential oil. However, in most of the above methods, metabolites of plants or components of plant tissues are extracted together with the fragrance component by heating and organic solvent treatment in the extraction process, and some fragrance components are destroyed in the heating process and are transformed into other components. In addition, since the processing process is complicated and takes a lot of time, there may be many differences from the original fragrance of flowers.

Recently, in order to compensate for the above shortcomings, a head space method and a solid phase micro extraction (SPME) method have been developed. These methods, unlike conventional extraction methods, do not use a solvent and do not require a pretreatment process, so that they can quickly and conveniently analyze the fragrance component, and are evaluated as techniques for reproducing the original fragrance of flowers.

However, when the scent components analyzed through the above methods are combined as they are, the scent intensity of the composition may be too high, or an allergic component may be contained excessively, and the palatability may not be preferred by users. have.

An object of the present invention is to solve the above problems, and to provide a composition for reproducing the smell of yellow plum, which reproduces the unique scent of yellow plum without damaging the natural yellow plum, and improves the user's palatability.

The technical problems of the present invention are not limited to the technical problems mentioned above, and other technical problems that are not mentioned will be clearly understood by those skilled in the art from the following description.

The composition for reproducing the smell of yellow plum according to an embodiment of the present invention is a group consisting of phenoxanol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate. It characterized in that it comprises at least one selected from.

Preferably, the composition for reproducing the scent of yellow plum blossom, phenoxanol 10 to 30% by weight; 15 to 35% by weight of alpha-hexyl cinamic aldehyde; And 5 to 26% by weight of methyl dihydro jasmonate.

Preferably, the scent reproducing composition of the yellow plum is, butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, di-limonene (D-limonene) ), phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarine and benzyl alcohol It may further include one or more selected.

In addition, preferably, the composition for reproducing the fragrance of the yellow plum blossom is 0.1 to 1.5% by weight of butyl butyrate; And cis-3-hexenyl acetate may include 0.1 to 1.5% by weight.

In addition, the scent reproducing composition of the yellow plum, 3- (4-tetra-butylphenyl) butanal (3- (4-tert-butylphenyl) butanal) and bergamot oil (bergamot oil) at least one selected from the group consisting of It may contain more.

In addition, preferably, the composition for reproducing the scent of yellow plum blossom may include 10 to 30% by weight of 3-(4-tetra-butylphenyl)butanal and 0.1 to 10% by weight of bergamot oil.

In one embodiment of the present invention, it is possible to provide a composition for external application for skin comprising a composition for reproducing the fragrance of yellow plum blossom.

In addition, in an embodiment of the present invention, it is possible to provide a cosmetic composition comprising a composition for reproducing the fragrance of yellow plum blossom.

In one embodiment of the present invention, it is possible to provide a personal care product comprising a composition for reproducing the fragrance of yellow plum blossom.

In addition, in an embodiment of the present invention, it is possible to provide a home care product comprising a composition for reproducing the fragrance of yellow plum blossom.

The composition for reproducing scent of yellow plum according to the present invention has the effect of reproducing the unique scent of yellow plum without damaging the natural yellow plum.

In addition, the composition for reproducing the smell of yellow plum according to the present invention is based on the components of the yellow plum analyzed by the head space method, and by adjusting the composition, it reproduces the unique smell of yellow plum and provides excellent palatability to the user at the same time. I can.

Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by an expert skilled in the art to which the present invention belongs. In general, the nomenclature used in this specification is well known and commonly used in the art. In addition, in describing an embodiment of the present invention, if it is determined that a detailed description of a related known configuration or function obstructs an understanding of the embodiment of the present invention, a detailed description thereof will be omitted. In addition, embodiments of the present invention will be described below, but the technical idea of the present invention is not limited thereto or is not limited thereto, and may be modified and variously implemented by those skilled in the art.

Hereinafter, the present invention will be described in detail.

The present invention relates to a composition for reproducing scent of yellow plum, wherein the composition for reproducing scent of yellow plum includes phenoxanol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate. jasmonate) may include one or more selected from the group consisting of.

As described above, for yellow plum blossoms, when the fragrance components analyzed through the head space method are combined, the intensity of the fragrance may be too high or an allergy-causing component may be excessively contained, and the palatability is low. There is a problem that it may not be preferred by users.

In consideration of these problems, the inventors of the present invention are known as allergen components among the scent components of yellow plum analyzed through the head space method, and the intensity of the scent is too high and the amount of ?t is high, benzyl benzoate. ), it was replaced with methyl dihydro jasmonate, which is not an allergen component and has a soft similar scent.

In addition, butyl butyrate and cis-3-hexenyl acetate, among the scent components of yellow plum analyzed by the head space method, also have very high scent strength, so when applied as they are Since it is not natural and has an artificial feeling, most of the above two components were replaced with alpha-hexyl cinamic aldehyde and phenoxanol, which have a similar fragrance but give a mild nuance, respectively.

As such, the composition for reproducing the scent of yellow plum according to the present invention is not simply a combination of the scent components analyzed through the head space method, but as new alternative components, phenoxanol, alpha-hexyl cinnamic aldehyde and methyl dihydroza By including at least one type of smonate, there is a characteristic that reproduces the smell of yellow plum blossoms.

The composition for reproducing the smell of yellow plum according to an embodiment of the present invention may contain 10 to 30% by weight of phenoxanol, preferably 12 to 28% by weight, and more preferably 15 to 25 It may include weight %, and most preferably 18 to 22 weight %.

The composition for reproducing the smell of yellow plum according to an embodiment of the present invention may contain 15 to 35% by weight of alpha-hexyl cinnamic aldehyde, preferably 18 to 32% by weight, and more preferably It may contain 20 to 30% by weight, and most preferably, may contain 23 to 27% by weight.

The composition for reproducing the smell of yellow plum according to an embodiment of the present invention may include 5 to 26% by weight of methyl dihydro jasmonate, preferably 7 to 24% by weight, more preferably It may contain 10 to 20% by weight, most preferably may contain 13 to 18% by weight.

When the contents of phenoxanol, alpha-hexyl cinamic aldehyde, and methyl dihydro jasmonate are within the above ranges, reproducibility of fragrance is excellent and intensity of fragrance is appropriate, so palatability can be improved.

The scent reproducing composition of yellow plum according to an embodiment of the present invention may further include a scent component of yellow plum analyzed by a head space method. If the fragrance component of the yellow plum analyzed by the head space method is additionally included, the similarity of the fragrance of the yellow plum can be improved.

The scent components of the yellow plum analyzed by the headspace method were butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, and di-limonene (D- limonene), phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarine, and benzyl alcohol do.

The scent reproducing composition of the yellow plum according to the present invention, along with phenoxanol, alpha-hexyl cinamic aldehyde and methyl dihydro jasmonate, butyl butyrate, cis-, which are scent components analyzed by a head space method. By further including at least one selected from the group consisting of 3-hexenyl acetate, benzyl benzoate, di-limonene, phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarin and benzyl alcohol, the smell of yellow plum Similarity can be improved.

Specifically, the odor reproduction composition of yellow plum according to the present invention includes butyl butyrate and cis-3-of odor components analyzed by the head space method along with phenoxanol, alpha-hexyl cinnamic aldehyde and methyl dihydro jasmonate. It may further include hexenyl acetate, di-limonene, benzaldehyde and coumarin.

Among the scent components of yellow plum analyzed by the head space method, the main components that create the intrinsic odor of yellow plum are butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, di-limonene, benzaldehyde and coumarin. At this time, since benzyl benzoate is an allergen component, the intensity of the fragrance is too high, and the content is high, in an embodiment of the present invention, the entire amount of benzyl benzoate was replaced with methyl dihydro jasmonate. In other words, the composition for reproducing the scent of yellow plum according to an embodiment of the present invention includes butyl butyrate, cis-3-hexenyl acetate, di-limonene, and benzaldehyde, which are the main components that create the intrinsic odor of yellow plum except for benzyl benzoate. And by further including coumarin, to improve the smell similarity of yellow plum blossom, and minimize the artificial feeling.

The scent reproducing composition of yellow plum according to the present invention, as a scent component of yellow plum analyzed by the headspace method, may contain 0.1 to 1.5% by weight of butyl butyrate, preferably 0.2 to 1.3% by weight, and , More preferably, it may contain 0.3 to 1.2% by weight, most preferably may contain 0.5 to 1% by weight.

The composition for reproducing the smell of yellow plum according to the present invention may contain 0.1 to 1.5% by weight of cis-3-hexenyl acetate, and preferably 0.2 to 1.3% by weight, as a fragrance component of yellow plum analyzed by the headspace method. It may include, more preferably 0.3 to 1.2% by weight, and most preferably 0.5 to 1% by weight.

Specifically, as described above, butyl butyrate and cis-3-hexenyl acetate have very high scent strength, and when applied as such, they have a similar scent, but a mild nuance These ingredients have replaced most of each with alpha-hexyl cinnamic aldehyde and phenoxanol that give (nuance). However, when butyl butyrate and cis-3-hexenyl acetate are completely replaced with different components, a problem of inferior flavor similarity may occur. Therefore, butyl butyrate and cis-3-hexenyl acetate may be added in small amounts to reinforce the similarity. At this time, when butyl butyrate and cis-3-hexenyl acetate are added in an amount of 1.5% by weight or more, since the artificial feeling is strong and not natural, it is preferable to add it in an amount of 1.5% by weight or less. When butyl butyrate and cis-3-hexenyl acetate are included in trace amounts of 0.1 to 1.5% by weight, respectively, the smell similarity of yellow plum is improved and palatability may be slightly improved.

The scent reproducing composition of yellow plum according to the present invention, as the scent component of yellow plum analyzed by the headspace method, may contain 0.1 to 10% by weight of di-limonene, and preferably 0.5 to 8% by weight. And, more preferably 1 to 7% by weight may be included, and most preferably 3 to 6% by weight may be included.

The scent reproducing composition of yellow plum according to the present invention, as a scent component of yellow plum analyzed by the headspace method, may contain 0.1 to 1% by weight of benzaldehyde, preferably 0.1 to 0.8% by weight, and , More preferably 0.1 to 0.6% by weight may be included, and most preferably 0.1 to 0.5% by weight.

The scent reproducing composition of yellow plum according to the present invention, as the scent component of yellow plum analyzed by the headspace method, may contain 0.1 to 1% by weight of coumarin, preferably 0.1 to 0.8% by weight, More preferably 0.1 to 0.6% by weight may be included, and most preferably 0.1 to 0.5% by weight may be included.

The composition for reproducing the smell of yellow plum according to the present invention is at least one selected from the group consisting of 3-(4-tetra-butylphenyl)butanal (3-(4-tert-butylphenyl)butanal) and bergamot oil. It may further include. The scent reproducing composition of yellow plum blossoms, by further containing 3-(4-tetra-butylphenyl)butanal, can give a natural and rich feeling as a whole, and by further containing bergamot oil, palatability is improved, and the characteristic scent of yellow plums You can implement a fresh feeling without harming the.

Specifically, the composition for reproducing the smell of yellow plum according to the present invention may contain 10 to 30% by weight of 3-(4-tetra-butylphenyl)butanal, preferably 12 to 28% by weight, and , More preferably, it may contain 15 to 25% by weight, and most preferably may contain 18 to 22% by weight. By including 3-(4-tetra-butylphenyl)butanal within the above range, the composition for reproducing the smell of yellow plum blossom can realize a natural and rich feeling as a whole.

In addition, specifically, the composition for reproducing the smell of yellow plum according to the present invention may contain 0.1 to 10% by weight of bergamot oil, preferably 0.5 to 8% by weight, and more preferably 1 to 6 It may contain weight %, and most preferably, it may contain 2 to 5 weight %. By including bergamot oil within the above range, the composition for reproducing the scent of yellow plum can realize a fresh feeling without harming the peculiar scent of yellow plum, thereby greatly improving palatability.

As a result of performing a sensory evaluation on the scent similarity and palatability of the yellow plum blossoms for the composition for reproducing the scent of yellow plum according to the present invention, the similarity and palatability were the highest when the composition and content were satisfied. The sensory evaluation will be described in detail below.

The composition for reproducing yellow plum scent according to the present invention may be included in a composition for external application for skin, a personal care product, a cosmetic composition, and a home care product. In this case, the blending amount may be appropriately selected and blended in order to achieve a desired effect according to a technique conventional in the art.

Specifically, the composition for external application for skin refers to an agent that acts on the external application of the skin among external preparations, and it means a skin external preparation having a differentiated scent unique to yellow plum by containing the composition for reproducing the scent of yellow plum according to the present invention as an active ingredient. Specifically, skin external preparations may be prepared and used as pharmaceuticals or quasi-drugs in the form of creams, gels, patches, sprays, ointments, warnings, lotions, liniment, pasta products, or cataplasma products for skin external use, but are limited thereto. It is not.

For example, when the composition for reproducing yellow plum scent according to the present invention is prepared as an ointment for external use for skin, it may be included in an amount of 0.01 to 5% by weight, preferably 0.05 to 3% by weight, more preferably 0.05 to 2% by weight. , Most preferably 0.1 to 0.5% by weight may be included.

Personal care products include cosmetics applied to the body including human and animal skin, hair, scalp, and nails, hair care products, toiletries, cosmeceuticals, beauty supplements, insect repellents, personal hygiene and cleansing products. Including, but not limited thereto, may be applied to all personal care compositions into which fragrances are added.

For example, the personal care products are deodorant, antiperspirant, spray, shaving agent, skin, lotion, moisturizer, toner, bath agent, cleansing agent, shampoo, conditioner, conditioner, mousse, styling gel, perfume, hair Spray, hair dye, hair colorant, hair bleach, remover, nail cream, dead skin softener, sunscreen, insect repellent, anti-aging agent, lipstick, foundation, face powder, eyeliner, eye shadow, mascara, soap, hand liquid, for personal care Non-woven fabric supplies, makeup remover, facial cleansing agent, cold cream, face mask, cologne, lotion, hair cuticle coat, shower gel, body wash, scrubbing cleanser, nail conditioner, lip balm, lip gloss, acne skin preparation, mouthwash, massage oil , Toothpaste, ointment base, local wound healing agent, mist, hair removal agent, personal care lubricant, and nail coloring aids, but are not limited thereto.

The yellow plum scent reproducing composition according to the present invention may be included in 3 to 30% by weight, preferably 5 to 20% by weight, more preferably 5 to 15% by weight, most preferably when prepared as a personal care product perfume. It may be included in 10 to 15% by weight.

The composition for reproducing the fragrance of yellow plum according to the present invention may be included in the cosmetic composition.

Cosmetic composition is not only basic products such as cream, serum, essence, skin, lotion, body oil, body lotion, etc., but also lipstick, foundation, lip balm, blusher, shading, highlighter, sun stick, lipstick, makeup base, foundation, pact, concealer And makeup products such as skin covers.

For example, when the yellow plum scent reproducing composition according to the present invention is prepared as a cream, which is a cosmetic composition, it may be included in 0.01 to 5% by weight, preferably 0.05 to 3% by weight, more preferably 0.05 to 2% by weight, Most preferably 0.1 to 0.5% by weight may be included.

In addition, for example, when the composition for reproducing the scent of yellow plum according to the present invention is prepared as an essence as a cosmetic composition, it may be included in an amount of 0.01 to 5% by weight, preferably 0.05 to 3% by weight, more preferably 0.05 to 2% by weight. %, most preferably 0.1 to 0.5% by weight.

Home care products include products used domestically to clean surfaces or maintain hygiene, such as in kitchens and bathrooms (e.g. hard surface cleaners, manual and automatic dish care, toilet cleaners and disinfectants, dish detergents), textile care. And products for use in laundry products such as washing (for example, detergents, fabric softeners, pre-treatment stain removers), and fragrances that are used to remove odors by emitting fragrance compounds or, in some cases, as a perfume substitute. , It is not limited thereto, and may be applied to any home care composition into which a fragrance is added.

For example, home care products include laundry detergents, laundry detergent additives, laundry bars, fabric softeners, dish detergents, wood polishes, bathtub and tile cleaners, toilet bowl cleaners, hard surface cleaners, window cleaners, anti-fog agents, drain cleaners, and carpet cleaners. , A prewash spotter, a rust stain cleaner, a scale remover, a deodorant and an air freshener, but are not limited thereto.

The present invention will be described in more detail through the following examples. These examples are for illustrative purposes only, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not construed as being limited by these examples.

Example 1: Preparation of a composition to reproduce the smell of yellow plum

(1) Analysis of scent components of yellow plum blossoms through the head space method

The present invention analyzed the smell of yellow plum using the head space method in order to analyze the scent component of yellow plum without damaging the natural yellow plum. Specifically, sulfur plum was put in a sealed container, solid fine extract fiber (SPME Fiber (75㎛ Carboxen/PDMS)) was injected, and the scented yellow plum was adsorbed for 1 hour, and then held in Agilent 7890A GC device for 60 seconds. The analysis was carried out. As a result, as shown in Table 1 below, the fragrance component of yellow plum flower was derived.

No. ingredient CAS.NO. Content (% by weight) One Butyl butyrate 109-21-7 20.5 2 Cis-3-hexenyl acetate 36181-71-8 25 3 Benzyl benzoate 120-51-4 15.67 4 D-limonene 5989-27-5 5.4 5 Phenyl ethyl alcohol 60-12-8 5 6 2-ethyl-1-hexanol 104-76-7 5 7 Benzaldehyde 100-52-7 0.2 8 Coumarin 91-64-5 0.2 9 Benzyl alcohol 100-51-6 0.8 10 Etc - 22.23 Total content 100

(2) Based on the analysis results, determine the composition of the composition for reproducing the smell of yellow plum

It was prepared based on the scent component of yellow plum analyzed using the head space method, but a composition for reproducing the scent of yellow plum was prepared using dipropylene glycol (DPG) as a solvent as other components.

The prepared yellow plum scent reproduction composition and the natural scent of yellow plum were subjected to sensory evaluation by 10 professional sensory panelists.As a result, the main odor components of the yellow plum were butyl butarate, cis-3-hexenyl acetate, and benzyl benzoate. , Di-limonene, benzaldehyde and coumarin were found to be a total of six components.

On the other hand, benzyl benzoate, which is an allergen component, has a high scent intensity, and has a high content, is replaced with methyl dihydro jasmonate, and butyl butyrate and cis-3-hexenyl acetate have strong scent strength, and if used as it is It was judged that it would have an unnatural and artificial feeling, so it was decided to replace it with alpha-hexyl cinnamic aldehyde and phenoxanol, each having a similar scent but mild nuance.

(3) Preparation of the composition for reproducing the smell of yellow plum according to the present invention

Based on the above analysis, a composition for reproducing the smell of yellow plum according to the present invention of Example 1 was prepared. The constituent components and contents are shown in Table 2 below.

No. ingredient CAS.NO. Content (% by weight) One Butyl butyrate 109-21-7 0 2 Cis-3-hexenyl acetate 36181-71-8 0 3 D-limonene 5989-27-5 5.4 4 Benzaldehyde 100-52-7 0.2 5 Coumarin 91-64-5 0.2 6 Phenoxanol 55066-48-3 20.5 7 Alpha-hexyl cinamic aldehyde 101-86-0 25 8 Methyl dihydro jasmonate 24851-98-7 15.67 9 Dipropylene glycol - 33.03 Total content 100

Experimental Example 1: Sensory evaluation of the composition for reproducing the smell of yellow plum prepared in Example 1

Sensory evaluation was performed on the composition for reproducing the smell of yellow plum of Example 1 prepared under the conditions of Table 2. Specifically, the sensory evaluation was conducted on 20 men and women aged 20 to 39 years old, each taking the smell of the living yellow plum flower and the composition of Example 1, and responding to the questionnaire, so that the actual relationship with the yellow plum flower Similarity and palatability were investigated. Specifically, in the questionnaire about the similarity question 1 (how similar is the scent of the composition according to the examples with yellow plum blossoms?), 1 if not at all similar, 2 if not very similar, 3 if moderate, 4 if somewhat similar, If it is very similar, it was indicated as 5, and for question 2 (how much do you like the fragrance of the composition according to the example?) about palatability, 1 if it is not good, 2 if it is not very good, 3 if it is moderate, 4 if it is slightly good, and very If it is good, it was written as 5. The results are shown in Table 3 below.

Evaluation agent Question 1 (similarity) Question 2 (Preference) One 3 2 2 4 5 3 3 2 4 3 3 5 2 3 6 2 2 7 3 2 8 3 2 9 4 2 10 4 3 11 3 3 12 3 3 13 4 3 14 3 4 15 2 2 16 3 2 17 4 3 18 2 3 19 3 2 20 4 2 Average 3.1 2.65

Referring to Table 3, the composition for reproducing the scent of yellow plum according to Example 1 has a similarity of normal and slightly lower palatability compared to the scent of yellow plum.

Examples 2 to 4: Preparation of a composition to reproduce the smell of yellow plum

Although it is the main scent component of yellow plum in Example 1, the intensity of the scent is very high, and when applied as it is, it is judged that it is not natural and has an artificial feeling. In order to improve the scent reproducing composition of the yellow plum according to Examples 2 to 4 was prepared by adding a small amount. At this time, in order to minimize the artificial feeling, the content of each component was adjusted not to exceed 1.5% by weight. Specific constituents and contents of the composition for reproducing the smell of yellow plum according to Examples 2 to 4 are shown in Table 4 below.

No. ingredient Example 2 Example 3 Example 4 Content (% by weight) Content (% by weight) Content (% by weight) One Butyl butyrate 0.5 One 1.5 2 Cis-3-hexenyl acetate 0.5 One 1.5 3 D-limonene 5.4 5.4 5.4 4 Benzaldehyde 0.2 0.2 0.2 5 Coumarin 0.2 0.2 0.2 6 Phenoxanol 20.5 20.5 20.5 7 Alpha-hexyl cinamic aldehyde 25 25 25 8 Methyl dihydro jasmonate 15.67 15.67 15.67 9 Dipropylene glycol 32.03 31.03 30.03 Total content 100 100 100

Experimental Example 2: Sensory evaluation of the composition for reproducing the smell of yellow plum prepared in Examples 2 to 4

Sensory evaluation for similarity and palatability was performed for the composition for reproducing the smell of yellow plum of Examples 2 to 4 prepared under the conditions of Table 4 above. At this time, the sensory evaluation conditions were the same as in Experimental Example 1, and a 10-minute break was given between each questionnaire to avoid paralysis of the sense of smell. The evaluation results are shown in Table 5 below.

Evaluation agent Question 1 (similarity) Question 2 (Preference) Example 2 Example 3 Example 4 Example 2 Example 3 Example 4 One 5 4 4 4 3 3 2 4 4 3 3 3 3 3 5 5 3 3 4 4 4 5 3 4 3 3 2 5 4 5 3 3 4 3 6 5 4 3 4 3 3 7 4 5 3 2 4 2 8 5 5 2 3 4 3 9 3 3 2 2 3 2 10 4 5 3 5 3 4 11 3 4 4 2 2 2 12 4 5 2 5 3 2 13 5 3 3 4 2 2 14 3 3 3 3 2 4 15 5 3 4 4 3 4 16 3 4 4 2 3 4 17 5 4 3 4 4 3 18 5 5 3 3 5 3 19 3 4 4 5 3 2 20 5 5 4 4 5 3 Average 4.25 4.15 3.2 3.4 3.3 2.9

Referring to Table 5, in the case of Example 4 containing 1.5 wt% or more of butyl butyrate and cis-3-hexenyl acetate, the similarity was slightly improved compared to Example 1, but palatability was decreased, and butyl butyrate When cis-3-hexenyl acetate was included in the range of 0.1 to 1% by weight, similarity was greatly improved, and palatability was also slightly improved.

Examples 5 to 7: Preparation of a composition to reproduce the smell of yellow plum

In order to further improve the palatability of Examples 2 and 3, which showed excellent similarity and improved palatability in Experimental Example 2, bergamot oil (CAS.NO 8007-75-8, which gives a fresh feeling without inhibiting the characteristic scent of yellow plum blossom) 68648-33-9, 85049-52-1), and 3-(4-tetra-butylphenyl)butanal (CAS.NO. 80-54-6), which gives a natural and rich feeling overall, were further added. A composition for reproducing the smell of yellow plum according to 5 to 7 was prepared. At this time, the content of cis-3-hexenyl acetate and butyl butyrate was adjusted to 0.8% by weight, which is an intermediate level of Examples 2 and 3, and the content of 3-(4-tetra-butylphenyl)butanal was 20% by weight. And prepared by varying the content of bergamot oil from 1 to 10% by weight. Specific constituents and contents of the composition for reproducing the smell of yellow plum according to Examples 5 to 7 are shown in Table 6 below.

No. ingredient Example 5 Example 6 Example 7 Content (% by weight) Content (% by weight) Content (% by weight) One Butyl butyrate 0.8 0.8 0.8 2 Cis-3-hexenyl acetate 0.8 0.8 0.8 3 D-limonene 5.4 5.4 5.4 4 Benzaldehyde 0.2 0.2 0.2 5 Coumarin 0.2 0.2 0.2 6 Phenoxanol 20.5 20.5 20.5 7 Alpha-hexyl cinamic aldehyde 25 25 25 8 Methyl dihydro jasmonate 15.67 15.67 15.67 9 3-(4-tetra-butylphenyl)butanal 20 20 20 10 Bergamot oil 2 5 10 11 Dipropylene glycol 9.43 6.43 1.43 Total content 100 100 100

Experimental Example 3: Sensory evaluation of the composition for reproducing the smell of yellow plum prepared in Examples 5 to 7

Sensory evaluation of palatability was performed for the composition for reproducing the smell of yellow plum of Examples 5 to 7 prepared under the conditions of Table 6 above. At this time, the sensory evaluation conditions were the same as in Experimental Example 1, and a 10-minute break was given between each questionnaire to avoid paralysis of the sense of smell. The evaluation results are shown in Table 7 below.

Evaluation agent Question 2 (Preference) Example 5 Example 6 Example 7 One 4 4 3 2 4 3 4 3 5 5 3 4 5 5 3 5 5 4 2 6 5 3 4 7 4 4 2 8 4 5 2 9 4 3 3 10 5 4 5 11 4 4 3 12 5 5 3 13 4 5 3 14 5 4 4 15 4 3 2 16 4 5 3 17 4 4 2 18 3 5 3 19 5 4 3 20 4 5 3 Average 4.35 4.2 3

Referring to Table 7 above, in the case of Example 7 containing 10% by weight or more of bergamot oil, the palatability is at a normal level, but Examples 5 and 6 containing bergamot oil in the range of 1 to 5% by weight have excellent palatability. I could confirm.

Example 8: Perfume Preparation

A perfume was prepared by blending the composition for reproducing the smell of yellow plum according to Examples 5 and 6. Specifically, a perfume according to the present invention was prepared by mixing 15% by weight of each of the yellow plum scent reproduction compositions according to Examples 5 and 6, and 80% by weight of alcohol and 5% by weight of purified water, respectively. Through this, it was possible to manufacture a perfume that is most similar to the scent of yellow plum and has excellent palatability.

Example 9: Essence Preparation

The essence was prepared by blending the composition for reproducing the smell of yellow plum according to Example 5 above. Specifically, each component was added in the amount shown in Table 8, and an appropriate amount of preservative and purified water was added thereto to prepare an essence. Through this, it was possible to prepare an essence having a smell of yellow plum blossom.

No. ingredient Content (% by weight) One glycerin 5 2 1,3-butylene glycol 2 3 Polyethylene glycol 2 4 Carbomer One 5 Sodium hyaluronate 0.1 6 Polyacrylamide 2 7 Hydroxyethylcellulose 0.2 8 ethanol 3 9 Antioxidant 0.3 10 Triethanolamine 0.1 11 EDTA 0.1 12 Yellow Plum Fragrance Reproduction Composition according to Example 5 0.1

Example 10: Preparation of nourishing cream

A nourishing cream was prepared by blending the composition for reproducing yellow plum scent according to Example 5 above. Specifically, each component was added in the amount shown in Table 9, and an appropriate amount of preservative and purified water was added thereto to prepare a cream. Through this, it was possible to prepare a nourishing cream having a smell of yellow plum blossom.

No. ingredient Content (% by weight) One 1,3-butylene glycol 3 2 glycerin 3 3 Hydrogenated Lecithin One 4 Trioctanoine 2 5 Stearic Acid 1.5 6 Polysorbate 60 1.5 7 Sorbitansquioleate 2 8 Dimethicone 3 9 Antioxidant 0.3 10 Xanthan gum 0.2 11 Triethanolamine 0.1 12 EDTA 0.1 13 Yellow Plum Fragrance Reproduction Composition according to Example 5 0.2

Example 11: Preparation of ointment

An ointment was prepared by blending the composition for reproducing yellow plum scent according to Example 5 above. Specifically, each component was added in the amount described in Table 10, and an appropriate amount of preservative, colorant and purified water was added thereto to prepare an ointment. Through this, it was possible to prepare an ointment having a smell of yellow plum blossom.

No. ingredient Content (% by weight) One glycerin 8 2 1,3-butylene glycol 4 3 Floating paraffin 15 4 Beta glucan 7 5 Carbomer 0.1 6 Caprylic/Capric Triglyceride 3 7 Squalane One 8 Cetylaryl glucoside 1.5 9 Sorbitan Stearate 0.4 10 Cetearyl alcohol One 11 Yellow Plum Fragrance Reproduction Composition according to Example 5 0.3

As described above, a specific part of the content of the present invention has been described in detail. For those of ordinary skill in the art, this specific technology is only a preferred embodiment, and the scope of the present invention is not limited thereby It will be obvious. Accordingly, it will be said that the substantial scope of the present invention is defined by the appended claims and their equivalents.

Claims (10)

10 to 30% by weight of phenoxanol;
15 to 35% by weight of alpha-hexyl cinnamic aldehyde; And
Including 5 to 26% by weight of methyl dihydro jasmonate,
Butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, D-limonene, phenyl ethyl alcohol, 2 -Ethyl-1-hexanol (2-ethyl-1-hexanol), benzaldehyde (benzaldehyde), coumarin (coumarine) and benzyl alcohol (benzyl alcohol) characterized in that it further comprises at least one selected from the group consisting of , A composition that reproduces the fragrance of yellow plum blossoms. delete delete The method of claim 1,
The composition for reproducing the smell of yellow plum blossoms,
0.1 to 1.5% by weight of butyl butyrate; And
Cis-3-hexenyl acetate, characterized in that containing 0.1 to 1.5% by weight, reproducing the fragrance of yellow plum. The method of claim 1,
The composition for reproducing the smell of yellow plum blossoms,
3-(4-tetra-butylphenyl)butanal (3-(4-tert-butylphenyl)butanal) and bergamot oil, characterized in that it further comprises at least one selected from the group consisting of, sulfur plum Fragrance reproduction composition. The method of claim 5,
The composition for reproducing the smell of yellow plum blossoms,
3-(4-tetra-butylphenyl)butanal 10 to 30% by weight and 0.1 to 10% by weight of bergamot oil, characterized in that it comprises a fragrance reproduction composition of yellow plum. A composition for external application for skin comprising the composition for reproducing the smell of yellow plum according to any one of claims 1 and 4 to 6. A cosmetic composition comprising the composition for reproducing the fragrance of yellow plum according to any one of claims 1 and 4 to 6. A personal care product comprising the composition for reproducing the smell of yellow plum according to any one of claims 1, 4 to 6. A home care product comprising the composition for reproducing the smell of yellow plum according to any one of claims 1 and 4 to 6.