KR20200090439A - Composition for expressing the fragrance of kerria - Google Patents

Abstract

The present invention relates to a composition for expressing fragrance of kerria, and specifically, to a composition for expressing fragrance of kerria, which expresses a unique fragrance of kerria without damaging kerria in nature and improves user preference. The composition for expressing fragrance of kerria according to the present invention, based on the components of kerria analyzed by a head space method, adjusts constituent components to express the unique fragrance of kerria, and at the same time, provide excellent preference to users.

Description

Composition for expressing the fragrance of kerria

The present invention relates to a fragrance reproducing composition of yellow plum, specifically, to a fragrance reproducing composition of yellow plum, which directly reproduces the fragrance of the yellow plum and improves the palatability of the fragrance without damaging the natural yellow plum.

Plum belongs to the family Prunus, and refers to the flowers of plum trees or plum trees. Plum blossoms bloom before the leaves, and they burst into a clear scent with blooming flowers. Plum blossoms have a unique and mellow fragrance that can't be easily forgotten once they have been taken, and many attempts have been made to reproduce the fragrance of plum blossoms.

Yellow plum is a kind of plum, grows in a humid place, is weak in the shade, and is about 2m high. The leaves of the plum blossom are misaligned, long egg-shaped, with double teeth on the edges. Flowers of yellow plum blossoms in yellow from April to May.

Gapsa duck forest in Gyeryongsan National Park in Chungnam is famous as the largest colony of yellow plum blossoms in Korea, and is characterized by the shape of flowers resembling plum blossoms and an elegant and elegant fragrance.

Existing fragrance components include a solvent extraction method in which an organic solvent is used to form an absolute, and a vapor distillation method in which the fragrance component is made into essential oil. However, most of the above methods extract components of plant metabolites or plant tissues together with fragrance components by heating and organic solvent treatment in the extraction process, and some fragrance components are destroyed and deteriorated into other components in the heating process. In addition, since the processing process is complicated and takes a lot of time, there may be many differences from the original scent of the flower.

Recently, in order to compensate for the above-mentioned disadvantages, a head space method and a solid phase micro extraction (SPME) method have been developed. These methods, unlike the conventional extraction method, do not use a solvent and do not require a pre-treatment process, so that the fragrance components can be analyzed quickly and simply as well as being evaluated as a technique for reproducing the original fragrance of a flower.

However, when the scent component analyzed through the above methods is directly combined, there is a problem that the intensity of the scent of the composition is too high, or the component causing allergies may be excessively contained, and it may not be favored by the user due to low palatability. have.

The present invention is to solve the above problems, and aims to provide a composition for reproducing a fragrance of yellow plum, which improves the palatability of a user, while reproducing the original fragrance of yellow plum without damaging the natural yellow plum.

The technical problems of the present invention are not limited to the technical problems mentioned above, and other technical problems not mentioned will be clearly understood by those skilled in the art from the following descriptions.

According to an embodiment of the present invention, the composition for reproducing the smell of yellow pluming is a group consisting of phenoxanol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate Characterized in that it comprises at least one selected from.

Preferably, the composition for reproducing the odor of the yellow plum is 10 to 30% by weight of phenoxanol; Alpha-hexyl cinnamic aldehyde 15 to 35% by weight; And 5 to 26% by weight of methyl dihydro jasmonate.

Preferably, the composition for reproducing the odor of sulfurization is butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, and di-limonene ), phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarine and benzyl alcohol It may further include one or more selected.

In addition, preferably, the composition for reproducing the odor of the yellow plum is 0.1 to 1.5% by weight of butyl butyrate; And 0.1 to 1.5% by weight of cis-3-hexenyl acetate.

In addition, the odor rejuvenation composition of the yellowing, 3-(4-tetra-butylphenyl) butanal (3-(4-tert-butylphenyl)butanal) and one or more selected from the group consisting of bergamot oil (bergamot oil) It may further include.

In addition, preferably, the fragrance reproduction composition of the sulfurization may include 10 to 30% by weight of 3-(4-tetra-butylphenyl)butanal and 0.1 to 10% by weight of bergamot oil.

In one embodiment of the present invention, it is possible to provide a composition for external application for skin, including a composition for reproducing odor of yellow plum.

In addition, in one embodiment of the present invention, it is possible to provide a cosmetic composition comprising a fragrance reproducing composition of yellow plum.

In one embodiment of the present invention, it is possible to provide a personal care product comprising a fragrance reproducing composition of yellow plum.

In addition, in one embodiment of the present invention, it is possible to provide a home care product comprising a fragrance reproducing composition of yellow plum.

The fragrance reproducing composition of the yellow plum according to the present invention has an effect capable of reproducing the natural fragrance of the yellow plum as it is without damaging the natural yellow plum.

In addition, the odor reproducing composition of the plum blossom according to the present invention is based on the components of the plum blossom analyzed by the head space method, by adjusting the constituent components, while reproducing the flavor of the yellow plum, while simultaneously providing excellent palatability to the user Can.

Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by a person skilled in the art to which the present invention pertains. In general, the nomenclature used herein is well known and commonly used in the art. In addition, in describing the embodiments of the present invention, when it is determined that detailed descriptions of related well-known configurations or functions interfere with the understanding of the embodiments of the present invention, detailed descriptions thereof will be omitted. In addition, although the embodiments of the present invention will be described below, the technical spirit of the present invention is not limited or limited thereto, and can be variously implemented by a person skilled in the art.

Hereinafter, the present invention will be described in detail.

The present invention relates to a odor rejuvenation composition of the yellow plum, the odor rejuvenation composition of the yellow plum, phenoxanol (Phenoxanol), alpha-hexyl cinnamic aldehyde (Alpha-hexyl cinnamic aldehyde) and methyl dihydro jasmonate (methyl dihydro jasmonate) may include one or more selected from the group consisting of.

As described above, in the case of combining the fragrance components analyzed through the head space method for the sulfurization, the intensity of the fragrance may be too high, or the components causing allergies may be excessively contained, and the palatability is low. There is a problem that may not be preferred from the user.

In consideration of these problems, the present inventor is known as an allergen component among the odor components of the yellow plum which are analyzed through the head space method, and the strength of the scent is too high and the amount of ?t is high, benzyl benzoate ), it was replaced with methyl dihydro jasmonate which is not allergen and has a soft, similar flavor.

In addition, butyl butyrate and cis-3-hexenyl acetate among the odorous components of the yellow plum which are analyzed through the head space method also have very high scent strength, and when applied as they are. Because of the unnatural and artificial feel, most of the two components were replaced by alpha-hexyl cinnamic aldehyde and phenoxanol, which have similar flavors but give a mild nuance.

As described above, the odor reproducing composition of the yellow plum according to the present invention is not simply a combination of odor components analyzed through a head space method, but is a new alternative component of phenoxanol, alpha-hexyl cinnamic aldehyde and methyl dihydro It is characterized by reproducing the scent of yellow plum by including one or more of the sumonates.

The fragrance reproducing composition of yellowing according to an embodiment of the present invention may include 10 to 30% by weight of phenoxanol, preferably 12 to 28% by weight, and more preferably 15 to 25% It may contain a weight percent, most preferably 18 to 22 weight percent.

The fragrance reproduction composition of yellowing according to an embodiment of the present invention may include 15 to 35% by weight of alpha-hexyl cinnamic aldehyde, preferably 18 to 32% by weight, and more preferably 20 to 30% by weight, and most preferably 23 to 27% by weight.

The fragrance reproduction composition of yellowing according to an embodiment of the present invention may include 5 to 26% by weight of methyl dihydro jasmonate, preferably 7 to 24% by weight, and more preferably It may contain 10 to 20% by weight, most preferably 13 to 18% by weight.

When the content of each of phenoxanol, alpha-hexyl cinnamic aldehyde and methyl dihydro jasmonate is within the above range, the reproducibility of the aroma is excellent, and the strength of the aroma is appropriate to improve palatability.

The composition for reproducing the odor of yellow plum according to an embodiment of the present invention may further include the odor component of the yellow plum analyzed by the head space method. When the odorizing component of the yellowing flower analyzed by the head space method is further included, the similarity of the smell of the yellowing flower can be improved.

The odorous components of sulfurization analyzed by the head space method are butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, and di-limonene (D- limonene, phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarine, and benzyl alcohol do.

The odor-reproducing composition of the yellowing according to the present invention includes phenoxanol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate, as well as butyl butyrate, cis-, which are the odorous components analyzed by the head space method. Scent of sulfurization by further comprising at least one member selected from the group consisting of 3-hexenyl acetate, benzyl benzoate, di-limonene, phenyl ethyl alcohol, 2-ethyl-1-hexanol, benzaldehyde, coumarin and benzyl alcohol Similarity can be improved.

Specifically, the fragrance reproducing composition of yellowing according to the present invention includes phenoxy phenol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate, among odor components analyzed by the headspace method, butyl butyrate, cis-3- Hexenyl acetate, di-limonene, benzaldehyde and coumarin.

Among the odorous components of the yellow plumbing analyzed by the head space method, the main components that produce the natural odor of the yellow plum are butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, di-limonene, benzaldehyde and coumarin. At this time, since benzyl benzoate is an allergen component, the intensity of the fragrance is too high and the content is high, in one embodiment of the present invention, the total amount of benzyl benzoate is replaced with methyl dihydro jasmonate. In other words, the composition for reproducing the odor of sulfurization according to an embodiment of the present invention is butyl butyrate, cis-3-hexenyl acetate, di-limonene, benzaldehyde, which are the main components that produce the intrinsic odor of yellowing except benzyl benzoate. And by further including coumarin, to improve the aroma similarity of yellowing, and to minimize artificial feeling.

The fragrance reproducing composition of the yellowing according to the present invention, as the fragrance component of the yellowing analyzed by the headspace method, may include 0.1 to 1.5% by weight of butyl butyrate, preferably 0.2 to 1.3% by weight, , More preferably, it may contain 0.3 to 1.2% by weight, most preferably 0.5 to 1% by weight.

The odor reproducing composition of the yellow plum according to the present invention, as the odor component of the yellow plum analyzed by the headspace method, may include 0.1 to 1.5% by weight of cis-3-hexenyl acetate, preferably 0.2 to 1.3% by weight It may include, more preferably, it may include 0.3 to 1.2% by weight, most preferably it may contain 0.5 to 1% by weight.

Specifically, butyl butyrate and cis-3-hexenyl acetate, as described above, have a very high intensity of fragrance, and when applied as it is, it has a natural and artificial feeling, so it has a similar fragrance but has a mild nuance. Alpha-hexyl cinnamic aldehyde and phenoxanol, which give (nuance), are mostly replaced. However, when butyl butyrate and cis-3-hexenyl acetate are completely replaced with other components, the similarity of flavor may be deteriorated. Therefore, a small amount of butyl butyrate and cis-3-hexenyl acetate can be added to enhance the similarity. At this time, when butyl butyrate and cis-3-hexenyl acetate are added in an amount of 1.5% by weight or more, it is preferable to add it in an amount of 1.5% by weight or less, because the artificial feeling is strong and unnatural. When butyl butyrate and cis-3-hexenyl acetate are each included in a trace amount of about 0.1 to 1.5% by weight, the similarity in flavor of sulfurization is improved, and palatability can be somewhat improved.

The fragrance reproducing composition of the yellow plum according to the present invention, as the fragrance component of the yellow plum analyzed by the headspace method, may include 0.1 to 10% by weight of di-limonene, preferably 0.5 to 8% by weight And more preferably 1 to 7% by weight, and most preferably 3 to 6% by weight.

The odor reproducing composition of the yellow plum according to the present invention, as the odor component of the yellow plum analyzed by the headspace method, may include 0.1 to 1% by weight of benzaldehyde, preferably 0.1 to 0.8% by weight, , More preferably, it may contain 0.1 to 0.6% by weight, most preferably 0.1 to 0.5% by weight.

The fragrance reproducing composition of the yellow plum according to the present invention, as the fragrance component of the yellow plum analyzed by the headspace method, may include 0.1 to 1% by weight of coumarin, preferably 0.1 to 0.8% by weight, More preferably, it may contain 0.1 to 0.6% by weight, most preferably 0.1 to 0.5% by weight.

The composition for reproducing the fragrance of yellowing according to the present invention is at least one selected from the group consisting of 3-(4-tert-butylphenyl)butanal and bergamot oil. It may further include. The fragrance reproducing composition of the yellow plum can further give a natural and rich feeling by further including 3-(4-tetra-butylphenyl)butanal, and by further containing the bergamot oil, the palatability is improved, and the peculiar fragrance of the yellow plum It is possible to achieve a fresh feeling without harming.

Specifically, the fragrance reproducing composition of the yellowing according to the present invention may include 10 to 30% by weight of 3-(4-tetra-butylphenyl)butanal, preferably 12 to 28% by weight, , More preferably 15 to 25% by weight, and most preferably 18 to 22% by weight. The odor reproducing composition of the yellow plum can include 3-(4-tetra-butylphenyl) butanal within the above range, thereby realizing a natural and rich feeling as a whole.

In addition, specifically, the fragrance reproducing composition of the yellowing according to the present invention may include 0.1 to 10% by weight of bergamot oil, preferably 0.5 to 8% by weight, and more preferably 1 to 6 It may contain a weight%, most preferably 2 to 5% by weight. By including the bergamot oil within the above range, the odor rejuvenation composition of the yellow plum can realize a fresh feeling without impairing the peculiar flavor of the yellow plum, and the palatability can be greatly improved.

As a result of sensory evaluation of the taste similarity and palatability with the yellow plum blossom, the similarity and palatability with the above composition and content showed the highest results. The sensory evaluation will be described in detail below.

The composition for reproducing yellowed odor according to the present invention may be included in a composition for external application for skin, a personal care product, a cosmetic composition, and a home care product. At this time, the blending amount may be appropriately selected and blended to achieve the desired effect according to techniques conventional in the art.

Specifically, the composition for external application for skin refers to an agent that acts on external application of skin among the external preparations, and refers to an external preparation for skin having a distinctive scent unique to yellowing by containing the composition for reproducing the yellowing flavor according to the present invention as an active ingredient. Specifically, the external preparation for skin may be prepared as a pharmaceutical or quasi-drug product in the form of an external preparation for skin, such as cream, gel, patch, spray, ointment, warning, lotion, linement, pasta, or cataplasma, but is not limited thereto. It is not.

For example, when the composition for reproducing the yellowing odor according to the present invention is made of an ointment that is an external preparation for skin, it may be included in an amount of 0.01 to 5% by weight, preferably 0.05 to 3% by weight, more preferably 0.05 to 2% by weight , Most preferably 0.1 to 0.5% by weight.

Personal care products include cosmetics, hair care products, toiletries, cosmeceuticals, beauty aids, insect repellents, personal hygiene and cleansing products applied to the body, including human and animal skin, hair, scalp, and nails. Including, but not limited to, it can be applied to all personal care compositions are added fragrance.

For example, the personal care products include deodorant, antiperspirant, spray, shaving agent, skin, lotion, moisturizer, toner, bath, cleansing agent, shampoo, conditioner, conditioner, mousse, styling gel, perfume, hair Spray, hair dye, hair colorant, hair bleach, remover, nail cream, exfoliant, sunscreen, insect repellent, anti-aging agent, lipstick, foundation, face powder, eyeliner, eye shadow, mascara, soap, hand liquid, personal care Non-woven products, makeup remover, facial cleansing agent, cold cream, face mask, cologne, lotion, hair cuticle coat, shower gel, body wash, scrubbing cleanser, nail conditioner, lip balm, lip gloss, acne skin preparation, mouthwash, massage oil , Toothpaste, ointment base, topical wound healing agent, mist, hair removal agent, personal care lubricant and nail coloring aids.

The composition for reproducing the yellowed odor according to the present invention may be included in 3 to 30% by weight, preferably 5 to 20% by weight, more preferably 5 to 15% by weight, and most preferably, when it is made of a perfume that is a personal care product It may be included in 10 to 15% by weight.

The composition for reproducing the yellowing odor according to the present invention may be included in a cosmetic composition.

The cosmetic composition is not only basic products such as cream, serum, essence, skin, lotion, body oil, body lotion, etc., but also lipstick, foundation, lip balm, blusher, shading, highlighter, sun stick, lipstick, makeup base, foundation, pact, concealer And makeup products such as skin covers.

For example, when the composition for reproducing yellowed odor according to the present invention is prepared as a cosmetic composition cream, it may be included in an amount of 0.01 to 5% by weight, preferably 0.05 to 3% by weight, more preferably 0.05 to 2% by weight, Most preferably 0.1 to 0.5% by weight.

In addition, for example, when the composition for reproducing yellowed odor according to the present invention is made of an essence as a cosmetic composition, it may be included in an amount of 0.01 to 5% by weight, preferably 0.05 to 3% by weight, and more preferably 0.05 to 2% by weight %, most preferably 0.1 to 0.5% by weight.

Home care products, such as those in the kitchen and bathroom, are used for household use to clean surfaces or maintain hygiene (eg, hard surface cleaners, manual and automatic dish care, toilet cleaners and disinfectants, dishwashing agents), textile care And products for use in laundry products such as washing (for example, detergents, fabric softeners, pretreatment stain removers), fragrances that emit fragrance compounds to remove odors or, in some cases, fragrances. , It is not limited thereto, and may be applied to all of home care compositions into which spices are added.

For example, home care products include laundry detergent, laundry detergent additive, laundry bar, fabric softener, dishwashing agent, wood polish, bath and tile cleaner, toilet bowl cleaner, hard surface cleaner, window cleaner, anti-fog agent, drain cleaner, carpet cleaner , Prewash spotter, rust stain cleaner, descaling agent, deodorant and fragrance, but is not limited thereto.

The present invention will be described in more detail through the following examples. These examples are only for illustrating the present invention, it will be apparent to those skilled in the art that the scope of the present invention is not to be construed as limited by these examples.

Example 1: Preparation of the fragrance reproduction composition of yellow plum

(1) Analysis of the odorous components of Hwangmaehwa through the headspace method

The present invention analyzed the scent of the yellow plum using the head space method to analyze the components of the yellow scent of plum without damaging the natural yellow plum. Specifically, after placing the yellow plum in a closed container, and injecting the fine micro-extracted fiber (SPME Fiber (75㎛ Carboxen/PDMS)) and adsorbing the aroma of the yellow plum for 1 hour, holding the Agilent 7890A GC machine for 60 seconds Analysis was performed. As a result, as shown in Table 1, the odorous components of the yellow plum were derived.

No. ingredient CAS.NO. Content (% by weight) One Butyl butyrate 109-21-7 20.5 2 Cis-3-hexenyl acetate 36181-71-8 25 3 Benzyl benzoate 120-51-4 15.67 4 D-limonene 5989-27-5 5.4 5 Phenyl ethyl alcohol 60-12-8 5 6 2-ethyl-1-hexanol 104-76-7 5 7 Benzaldehyde 100-52-7 0.2 8 Coumarin 91-64-5 0.2 9 Benzyl alcohol 100-51-6 0.8 10 Etc - 22.23 Total content 100

(2) Determination of the constituent components of the composition for reproducing the flavor of yellow plum based on the analysis results

Prepared on the basis of the odor component of the yellow plum which was analyzed using the head space method, the other component using a dipropylene glycol (dipropylene glycol, DPG) as a solvent to prepare a odor reproducing composition of the yellow plum.

Ten professional sensory panelists performed sensory evaluation on the above-mentioned prepared yellowing odor reproducing composition and natural yellowing odor, and as a result, the major scent components of yellowing were butyl butarate, cis-3-hexenyl acetate, benzyl benzoate , Di-limonene, benzaldehyde and coumarin were confirmed to be a total of six components.

On the other hand, benzyl benzoate, which is an allergen component, has high fragrance strength, and has a high content, is replaced with methyl dihydro jasmonate. It was judged that it would feel unnatural and artificial, and it was decided to replace it with alpha-hexyl cinnamic aldehyde and phenoxanol, each of which has a similar scent but mild nuance.

(3) Preparation of the fragrance reproducing composition of the yellow plum according to the present invention

On the basis of the above analysis, a composition for reproducing the smell of yellow plum according to the present invention of Example 1 was prepared. The components and contents are shown in Table 2 below.

No. ingredient CAS.NO. Content (% by weight) One Butyl butyrate 109-21-7 0 2 Cis-3-hexenyl acetate 36181-71-8 0 3 D-limonene 5989-27-5 5.4 4 Benzaldehyde 100-52-7 0.2 5 Coumarin 91-64-5 0.2 6 Phenoxanol 55066-48-3 20.5 7 Alpha-hexyl cinnamic aldehyde 101-86-0 25 8 Methyl dihydro jasmonate 24851-98-7 15.67 9 Dipropylene glycol - 33.03 Total content 100

Experimental Example 1: Sensory evaluation of the fragrance reproduction composition of the yellow plum prepared in Example 1

Sensory evaluation was carried out on the fragrance reproducing composition of the yellow plum of Example 1 prepared under the conditions of Table 2 above. Specifically, the sensory evaluation was conducted for 20 males and females 20 to 39 years of age, and by taking the smell of living yellow plum and the composition of Example 1, respectively, and answering the questionnaire, with actual yellow plum Similarity and palatability were investigated. Specifically, in the questionnaire, question 1 about similarity (how similar is the odor of the composition according to the example of yellowing and yellowing) is 1 if not similar at all, 2 if not very similar, 3 when normal, 4 when somewhat similar, If it is very similar, it was written as 5, and for Question 2 (how much do you like the scent of the composition according to the example?) for palatability, 1 if not good at all, 2 if not good, 3 if it is normal, 4 if it is slightly good, very If it is good, it should be indicated as 5. The results are shown in Table 3 below.

Evaluation agent Question 1 (similarity) Question 2 (symbolism) One 3 2 2 4 5 3 3 2 4 3 3 5 2 3 6 2 2 7 3 2 8 3 2 9 4 2 10 4 3 11 3 3 12 3 3 13 4 3 14 3 4 15 2 2 16 3 2 17 4 3 18 2 3 19 3 2 20 4 2 Average 3.1 2.65

Referring to Table 3, the composition for reproducing the scent of the yellow plum according to Example 1 was similar to the scent of the yellow plum, showing a moderate degree of similarity, and a slightly lower palatability.

Examples 2 to 4: Preparation of the fragrance reproduction composition of yellow plum

Although it is the main odor component of the yellowing in Example 1, when the strength of the fragrance is very high, it is judged to have an unnatural and artificial feeling when applied as it is, and the cis-3-hexenyl acetate and butyl butyrate are replaced with the smell similarity of the yellowing. To improve the scent was added in small portions to prepare a fragrance reproducing composition of the yellow plum according to Examples 2 to 4. At this time, in order to minimize the artificial feeling, the content of each component was adjusted not to exceed 1.5% by weight. The specific components and contents of the fragrance reproducing composition of the yellow plum according to Examples 2 to 4 are shown in Table 4 below.

No. ingredient Example 2 Example 3 Example 4 Content (% by weight) Content (% by weight) Content (% by weight) One Butyl butyrate 0.5 One 1.5 2 Cis-3-hexenyl acetate 0.5 One 1.5 3 D-limonene 5.4 5.4 5.4 4 Benzaldehyde 0.2 0.2 0.2 5 Coumarin 0.2 0.2 0.2 6 Phenoxanol 20.5 20.5 20.5 7 Alpha-hexyl cinnamic aldehyde 25 25 25 8 Methyl dihydro jasmonate 15.67 15.67 15.67 9 Dipropylene glycol 32.03 31.03 30.03 Total content 100 100 100

Experimental Example 2: Sensory evaluation of the odor reproducing composition of the yellow plum prepared in Examples 2 to 4

Sensory evaluation of similarity and palatability was performed for the odor reproducing compositions of the yellowing of Examples 2 to 4 prepared under the conditions of Table 4 above. At this time, the sensory evaluation conditions were the same as in Experimental Example 1, and a rest period of 10 minutes was given between each question to avoid paralysis of the sense of smell. The evaluation results are shown in Table 5 below.

Evaluation agent Question 1 (similarity) Question 2 (symbolism) Example 2 Example 3 Example 4 Example 2 Example 3 Example 4 One 5 4 4 4 3 3 2 4 4 3 3 3 3 3 5 5 3 3 4 4 4 5 3 4 3 3 2 5 4 5 3 3 4 3 6 5 4 3 4 3 3 7 4 5 3 2 4 2 8 5 5 2 3 4 3 9 3 3 2 2 3 2 10 4 5 3 5 3 4 11 3 4 4 2 2 2 12 4 5 2 5 3 2 13 5 3 3 4 2 2 14 3 3 3 3 2 4 15 5 3 4 4 3 4 16 3 4 4 2 3 4 17 5 4 3 4 4 3 18 5 5 3 3 5 3 19 3 4 4 5 3 2 20 5 5 4 4 5 3 Average 4.25 4.15 3.2 3.4 3.3 2.9

Referring to Table 5, in the case of Example 4 containing at least 1.5% by weight of butyl butyrate and cis-3-hexenyl acetate, the similarity was slightly improved compared to Example 1, but it was confirmed that the palatability was lowered, and butyl butyrate When the and cis-3-hexenyl acetate was included in the range of 0.1 to 1% by weight, the similarity was greatly improved, and the palatability was also slightly improved.

Examples 5 to 7: Preparation of odor reproducing composition of yellow plum

In order to further improve the palatability of Examples 2 and 3, which showed excellent similarity and improved palatability in Experimental Example 2, bergamot oil (CAS.NO 8007-75-8, which gives a fresh feeling without inhibiting the peculiar flavor of yellow plum) 68648-33-9, 85049-52-1) and 3-(4-tetra-butylphenyl)butanal (CAS.NO. 80-54-6), which give a natural and rich feeling as a whole, are further added to the Examples A odor reproducing composition of yellowing according to 5 to 7 was prepared. At this time, the content of cis-3-hexenyl acetate and butyl butyrate was adjusted to 0.8% by weight, which is the middle of Examples 2 and 3, and the content of 3-(4-tetra-butylphenyl)butanal was 20% by weight. It was fixed to, and was prepared by varying the content of bergamot oil to 1 to 10% by weight. The specific components and contents of the fragrance reproducing composition of the yellow plum according to Examples 5 to 7 are shown in Table 6 below.

No. ingredient Example 5 Example 6 Example 7 Content (% by weight) Content (% by weight) Content (% by weight) One Butyl butyrate 0.8 0.8 0.8 2 Cis-3-hexenyl acetate 0.8 0.8 0.8 3 D-limonene 5.4 5.4 5.4 4 Benzaldehyde 0.2 0.2 0.2 5 Coumarin 0.2 0.2 0.2 6 Phenoxanol 20.5 20.5 20.5 7 Alpha-hexyl cinnamic aldehyde 25 25 25 8 Methyl dihydro jasmonate 15.67 15.67 15.67 9 3-(4-tetra-butylphenyl)butanal 20 20 20 10 Bergamot oil 2 5 10 11 Dipropylene glycol 9.43 6.43 1.43 Total content 100 100 100

Experimental Example 3: Sensory evaluation of the odor reproducing composition of the yellow plum prepared in Examples 5 to 7

Sensory evaluation for palatability was carried out for the odor reproducing compositions of yellowing of Examples 5 to 7 prepared under the conditions of Table 6 above. At this time, the sensory evaluation conditions were the same as in Experimental Example 1, and a rest period of 10 minutes was given between each question to avoid paralysis of the sense of smell. The evaluation results are shown in Table 7 below.

Evaluation agent Question 2 (symbolism) Example 5 Example 6 Example 7 One 4 4 3 2 4 3 4 3 5 5 3 4 5 5 3 5 5 4 2 6 5 3 4 7 4 4 2 8 4 5 2 9 4 3 3 10 5 4 5 11 4 4 3 12 5 5 3 13 4 5 3 14 5 4 4 15 4 3 2 16 4 5 3 17 4 4 2 18 3 5 3 19 5 4 3 20 4 5 3 Average 4.35 4.2 3

Referring to Table 7, the palatability of Example 7 containing 10% by weight or more of bergamot oil is moderate, but in Examples 5 and 6 containing bergamot oil in a range of 1 to 5% by weight, excellent palatability I could confirm.

Example 8: Perfume preparation

Perfume was prepared by mixing the compositions for reproducing the yellowed odor according to Examples 5 and 6 above. Specifically, the perfumes according to the present invention were prepared by blending 80% by weight of alcohol and 5% by weight of purified water, respectively, to 15% by weight of each of the compositions for reproducing the yellowed odor according to Examples 5 and 6, respectively. Through this, it was possible to produce a perfume similar to the scent of the best yellow plum and excellent palatability.

Example 9: Essence preparation

Essence was prepared by blending the composition for reproducing the yellowed odor according to Example 5 above. Specifically, each component was added in an amount described in Table 8, and an appropriate amount of preservative and purified water was added thereto to prepare an essence. Through this, it was possible to prepare an essence having a scent of yellow plum.

No. ingredient Content (% by weight) One glycerin 5 2 1,3-butylene glycol 2 3 Polyethylene glycol 2 4 Carbomer One 5 Sodium hyaluronate 0.1 6 Polyacrylamide 2 7 Hydroxyethylcellulose 0.2 8 ethanol 3 9 Antioxidant 0.3 10 Triethanolamine 0.1 11 EDTA 0.1 12 A composition for reproducing a yellow plum flavor according to Example 5 0.1

Example 10: Preparation of nutrition cream

A nutritional cream was prepared by blending the composition for reproducing the yellowing odor according to Example 5 above. Specifically, each component was added in an amount described in Table 9, and an appropriate amount of preservative and purified water was added thereto to prepare a cream. Through this, it was possible to prepare a nutritional cream having a scent of yellow plum.

No. ingredient Content (% by weight) One 1,3-butylene glycol 3 2 glycerin 3 3 Hydrogenated lecithin One 4 Trioctanoin 2 5 Stearic Acid 1.5 6 Polysorbate 60 1.5 7 Sorbitan sesquioleate 2 8 Dimethicone 3 9 Antioxidant 0.3 10 Shotgun Sword 0.2 11 Triethanolamine 0.1 12 EDTA 0.1 13 A composition for reproducing a yellow plum flavor according to Example 5 0.2

Example 11: Preparation of ointment

Ointment was prepared by blending the composition for reproducing the yellowing odor according to Example 5 above. Specifically, each component was added in an amount described in Table 10, and an appropriate amount of preservative, pigment, and purified water was added thereto to prepare an ointment. Through this, it was possible to prepare an ointment having a scent of yellow plum.

No. ingredient Content (% by weight) One glycerin 8 2 1,3-butylene glycol 4 3 Floating paraffin 15 4 Beta glucan 7 5 Carbomer 0.1 6 Caprylic/Capric Triglyceride 3 7 Squalane One 8 Cetylaryl glucoside 1.5 9 Sorbitan stearate 0.4 10 Cetearyl alcohol One 11 A composition for reproducing a yellow plum flavor according to Example 5 0.3

The specific parts of the present invention have been described in detail above. For those skilled in the art, this specific technique is only a preferred embodiment, and the scope of the present invention is not limited thereby. It will be obvious. Accordingly, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

Claims (10)

Phenoxanol, alpha-hexyl cinnamic aldehyde, and methyl dihydro jasmonate, comprising at least one member selected from the group consisting of a yellowing odor rejuvenating composition. According to claim 1,
The fragrance reproduction composition of the yellow plum,
Phenoxanol 10 to 30% by weight;
15-35% by weight of alpha-hexyl cinnamic aldehyde; And
Characterized in that it contains 5 to 26% by weight of methyl dihydro jasmonate, the fragrance reproduction composition of the yellow plum. According to claim 1,
The fragrance reproduction composition of the yellow plum,
Butyl butyrate, cis-3-hexenyl acetate, benzyl benzoate, D-limonene, phenyl ethyl alcohol, 2 -Ethyl-1-hexanol (2-ethyl-1-hexanol), benzaldehyde (benzaldehyde), characterized in that it further comprises at least one selected from the group consisting of coumarine (coumarine) and benzyl alcohol (benzyl alcohol) , Hwangmaehwa odor reproducing composition. The method of claim 3,
The fragrance reproduction composition of the yellow plum,
Butyl butyrate 0.1 to 1.5 wt%; And
Characterized in that it contains 0.1 to 1.5% by weight of cis-3-hexenyl acetate, odor reproducing composition of the yellow plum. According to claim 1,
The fragrance reproduction composition of the yellow plum,
Characterized in that it further comprises at least one member selected from the group consisting of 3-(4-tetra-butylphenyl)butanal and bergamot oil. Fragrance reproduction composition. The method of claim 5,
The fragrance reproduction composition of the yellow plum,
Characterized in that it contains 10 to 30% by weight of 3-(4-tetra-butylphenyl)butanal and 0.1 to 10% by weight of bergamot oil, a composition for reproducing the smell of yellow plum. A composition for external application for skin comprising the composition for reproducing the fragrance of yellowing according to any one of claims 1 to 6. A cosmetic composition comprising the composition for reproducing the odor of yellowing according to any one of claims 1 to 6. A personal care product comprising the fragrance reproducing composition of yellowing according to any one of claims 1 to 6. A home care product comprising the fragrance reproducing composition of yellowing according to any one of claims 1 to 6.