KR102079840B1 - 알킬 아크릴레이트의 제조 방법 - Google Patents
알킬 아크릴레이트의 제조 방법 Download PDFInfo
- Publication number
- KR102079840B1 KR102079840B1 KR1020157019055A KR20157019055A KR102079840B1 KR 102079840 B1 KR102079840 B1 KR 102079840B1 KR 1020157019055 A KR1020157019055 A KR 1020157019055A KR 20157019055 A KR20157019055 A KR 20157019055A KR 102079840 B1 KR102079840 B1 KR 102079840B1
- Authority
- KR
- South Korea
- Prior art keywords
- catalyst
- reaction
- heavy
- column
- octanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
- C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
- C07C69/54—Acrylic acid esters; Methacrylic acid esters
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1262123 | 2012-12-17 | ||
| FR1262123A FR2999572B1 (fr) | 2012-12-17 | 2012-12-17 | Procede de production d'acrylate d'alkyle. |
| PCT/FR2013/053083 WO2014096648A1 (fr) | 2012-12-17 | 2013-12-16 | Procede de production d'acrylate d'alkyle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150095887A KR20150095887A (ko) | 2015-08-21 |
| KR102079840B1 true KR102079840B1 (ko) | 2020-02-20 |
Family
ID=48128455
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020157019055A Active KR102079840B1 (ko) | 2012-12-17 | 2013-12-16 | 알킬 아크릴레이트의 제조 방법 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10000439B2 (https=) |
| EP (1) | EP2931695B1 (https=) |
| JP (2) | JP6373276B2 (https=) |
| KR (1) | KR102079840B1 (https=) |
| CN (1) | CN104918911B (https=) |
| BR (1) | BR112015013542B1 (https=) |
| FR (1) | FR2999572B1 (https=) |
| WO (1) | WO2014096648A1 (https=) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10308619B2 (en) * | 2015-06-23 | 2019-06-04 | Covestro Deutschland Ag | Substituted triazines and a method for producing same |
| FR3060001B1 (fr) * | 2016-12-08 | 2020-05-01 | Arkema France | Procede de fabrication d'esters (meth)acryliques |
| FR3069538B1 (fr) * | 2017-07-25 | 2020-05-15 | Arkema France | Procede de purification d'esters (meth)acryliques. |
| FR3104155B1 (fr) * | 2019-12-09 | 2021-10-29 | Arkema France | Procede de fabrication en continu d’acrylates d’alkyle lourds |
| JP7440862B2 (ja) * | 2020-03-04 | 2024-02-29 | 国立大学法人東海国立大学機構 | カルボン酸エステル合成用触媒、およびカルボン酸エステルの製造方法 |
| EP4293010A1 (en) * | 2022-06-15 | 2023-12-20 | Evonik Operations GmbH | Process for the discontinuous (trans)esterification of (meth)acrylate compounds |
| WO2023242257A1 (en) * | 2022-06-15 | 2023-12-21 | Evonik Operations Gmbh | Pressure enhanced (trans)esterification of (meth)acrylate compounds |
| CN116143619A (zh) * | 2022-12-14 | 2023-05-23 | 湖北三里枫香科技有限公司 | 一种酯交换法制备(甲基)丙烯酸正异丁(辛)酯的生产工艺方法及装置 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005239564A (ja) * | 2004-02-24 | 2005-09-08 | Mitsubishi Rayon Co Ltd | (メタ)アクリル酸エステルの製造方法 |
| JP2006503795A (ja) * | 2002-01-04 | 2006-02-02 | レーム ゲゼルシャフト ミツト ベシュレンクテル ハフツング ウント コンパニー コマンディートゲゼルシャフト | アルキル(メタ)アクリレートの連続的製造方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3728242A1 (de) * | 1987-08-25 | 1989-03-09 | Basf Ag | Verfahren zur herstellung von carbonsaeureestern |
| JP2000016966A (ja) | 1998-07-01 | 2000-01-18 | Mitsubishi Gas Chem Co Inc | アクリル酸エステルまたはメタクリル酸エステルの製造方法 |
| DE10127939A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10301007A1 (de) * | 2003-01-13 | 2004-07-22 | Röhm GmbH & Co. KG | Verbessertes Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten mit mehrfacher Katalysatorrezyklierung. |
| US7268451B2 (en) | 2004-03-22 | 2007-09-11 | General Motors Corporation | Motor resolver assembly and method of measuring speed and position of a motor rotor |
| CN101274890A (zh) * | 2007-03-27 | 2008-10-01 | 罗姆有限公司 | 连续制造(甲基)丙烯酸烷基酯的方法 |
| JP5369438B2 (ja) * | 2008-01-10 | 2013-12-18 | 東亞合成株式会社 | ジアルキルアミノアルキル(メタ)アクリレートの連続製造方法 |
| JP2009274986A (ja) * | 2008-05-14 | 2009-11-26 | Mitsubishi Rayon Co Ltd | (メタ)アクリル酸アルキルエステルの製造方法 |
| FR2946046B1 (fr) * | 2009-05-26 | 2012-04-20 | Arkema France | Composition comprenant un oxyde de dialkyl etain et son utilisation comme catalyseur de transesterification pour la synthese d'esters (meth)acryliques. |
| JP2011126836A (ja) * | 2009-12-21 | 2011-06-30 | Toagosei Co Ltd | (メタ)アクリル酸エステルの製造方法 |
| JP5748482B2 (ja) * | 2011-01-14 | 2015-07-15 | 株式会社ダイセル | カルボン酸エステルの製造方法 |
-
2012
- 2012-12-17 FR FR1262123A patent/FR2999572B1/fr not_active Expired - Fee Related
-
2013
- 2013-12-16 WO PCT/FR2013/053083 patent/WO2014096648A1/fr not_active Ceased
- 2013-12-16 BR BR112015013542-0A patent/BR112015013542B1/pt active IP Right Grant
- 2013-12-16 US US14/650,906 patent/US10000439B2/en active Active
- 2013-12-16 KR KR1020157019055A patent/KR102079840B1/ko active Active
- 2013-12-16 CN CN201380065961.4A patent/CN104918911B/zh active Active
- 2013-12-16 JP JP2015547127A patent/JP6373276B2/ja active Active
- 2013-12-16 EP EP13824608.7A patent/EP2931695B1/fr active Active
-
2018
- 2018-02-09 JP JP2018021660A patent/JP2018109019A/ja not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006503795A (ja) * | 2002-01-04 | 2006-02-02 | レーム ゲゼルシャフト ミツト ベシュレンクテル ハフツング ウント コンパニー コマンディートゲゼルシャフト | アルキル(メタ)アクリレートの連続的製造方法 |
| JP2005239564A (ja) * | 2004-02-24 | 2005-09-08 | Mitsubishi Rayon Co Ltd | (メタ)アクリル酸エステルの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20150095887A (ko) | 2015-08-21 |
| JP2016501271A (ja) | 2016-01-18 |
| US20150315120A1 (en) | 2015-11-05 |
| US10000439B2 (en) | 2018-06-19 |
| JP2018109019A (ja) | 2018-07-12 |
| FR2999572A1 (fr) | 2014-06-20 |
| CN104918911A (zh) | 2015-09-16 |
| JP6373276B2 (ja) | 2018-08-15 |
| CN104918911B (zh) | 2018-02-23 |
| EP2931695B1 (fr) | 2017-04-12 |
| BR112015013542A2 (pt) | 2017-07-11 |
| BR112015013542B1 (pt) | 2020-09-24 |
| EP2931695A1 (fr) | 2015-10-21 |
| WO2014096648A1 (fr) | 2014-06-26 |
| FR2999572B1 (fr) | 2014-11-28 |
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St.27 status event code: A-0-1-A10-A15-nap-PA0105 |
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| A201 | Request for examination | ||
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
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