CN104918911B - 丙烯酸烷基酯的制备方法 - Google Patents

丙烯酸烷基酯的制备方法 Download PDF

Info

Publication number
CN104918911B
CN104918911B CN201380065961.4A CN201380065961A CN104918911B CN 104918911 B CN104918911 B CN 104918911B CN 201380065961 A CN201380065961 A CN 201380065961A CN 104918911 B CN104918911 B CN 104918911B
Authority
CN
China
Prior art keywords
alcohol
catalyst
reaction
alkyl acrylate
heavy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201380065961.4A
Other languages
English (en)
Chinese (zh)
Other versions
CN104918911A (zh
Inventor
A·里翁德尔
C·格雷尔
M·埃施
A·勒夫雷
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France SA filed Critical Arkema France SA
Publication of CN104918911A publication Critical patent/CN104918911A/zh
Application granted granted Critical
Publication of CN104918911B publication Critical patent/CN104918911B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN201380065961.4A 2012-12-17 2013-12-16 丙烯酸烷基酯的制备方法 Active CN104918911B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1262123 2012-12-17
FR1262123A FR2999572B1 (fr) 2012-12-17 2012-12-17 Procede de production d'acrylate d'alkyle.
PCT/FR2013/053083 WO2014096648A1 (fr) 2012-12-17 2013-12-16 Procede de production d'acrylate d'alkyle

Publications (2)

Publication Number Publication Date
CN104918911A CN104918911A (zh) 2015-09-16
CN104918911B true CN104918911B (zh) 2018-02-23

Family

ID=48128455

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380065961.4A Active CN104918911B (zh) 2012-12-17 2013-12-16 丙烯酸烷基酯的制备方法

Country Status (8)

Country Link
US (1) US10000439B2 (https=)
EP (1) EP2931695B1 (https=)
JP (2) JP6373276B2 (https=)
KR (1) KR102079840B1 (https=)
CN (1) CN104918911B (https=)
BR (1) BR112015013542B1 (https=)
FR (1) FR2999572B1 (https=)
WO (1) WO2014096648A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10308619B2 (en) * 2015-06-23 2019-06-04 Covestro Deutschland Ag Substituted triazines and a method for producing same
FR3060001B1 (fr) * 2016-12-08 2020-05-01 Arkema France Procede de fabrication d'esters (meth)acryliques
FR3069538B1 (fr) * 2017-07-25 2020-05-15 Arkema France Procede de purification d'esters (meth)acryliques.
FR3104155B1 (fr) * 2019-12-09 2021-10-29 Arkema France Procede de fabrication en continu d’acrylates d’alkyle lourds
JP7440862B2 (ja) * 2020-03-04 2024-02-29 国立大学法人東海国立大学機構 カルボン酸エステル合成用触媒、およびカルボン酸エステルの製造方法
EP4293010A1 (en) * 2022-06-15 2023-12-20 Evonik Operations GmbH Process for the discontinuous (trans)esterification of (meth)acrylate compounds
WO2023242257A1 (en) * 2022-06-15 2023-12-21 Evonik Operations Gmbh Pressure enhanced (trans)esterification of (meth)acrylate compounds
CN116143619A (zh) * 2022-12-14 2023-05-23 湖北三里枫香科技有限公司 一种酯交换法制备（甲基）丙烯酸正异丁（辛）酯的生产工艺方法及装置

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050119500A1 (en) * 2002-01-04 2005-06-02 Roehm Gmbh & Co. Kg Method for the continuous production of alkyl (meth)acrylates
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
CN101274890A (zh) * 2007-03-27 2008-10-01 罗姆有限公司 连续制造(甲基)丙烯酸烷基酯的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3728242A1 (de) * 1987-08-25 1989-03-09 Basf Ag Verfahren zur herstellung von carbonsaeureestern
JP2000016966A (ja) 1998-07-01 2000-01-18 Mitsubishi Gas Chem Co Inc アクリル酸エステルまたはメタクリル酸エステルの製造方法
DE10127939A1 (de) 2001-06-08 2002-05-29 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
DE10301007A1 (de) * 2003-01-13 2004-07-22 Röhm GmbH & Co. KG Verbessertes Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten mit mehrfacher Katalysatorrezyklierung.
US7268451B2 (en) 2004-03-22 2007-09-11 General Motors Corporation Motor resolver assembly and method of measuring speed and position of a motor rotor
JP5369438B2 (ja) * 2008-01-10 2013-12-18 東亞合成株式会社 ジアルキルアミノアルキル（メタ）アクリレートの連続製造方法
JP2009274986A (ja) * 2008-05-14 2009-11-26 Mitsubishi Rayon Co Ltd （メタ）アクリル酸アルキルエステルの製造方法
FR2946046B1 (fr) * 2009-05-26 2012-04-20 Arkema France Composition comprenant un oxyde de dialkyl etain et son utilisation comme catalyseur de transesterification pour la synthese d'esters (meth)acryliques.
JP2011126836A (ja) * 2009-12-21 2011-06-30 Toagosei Co Ltd （メタ）アクリル酸エステルの製造方法
JP5748482B2 (ja) * 2011-01-14 2015-07-15 株式会社ダイセル カルボン酸エステルの製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050119500A1 (en) * 2002-01-04 2005-06-02 Roehm Gmbh & Co. Kg Method for the continuous production of alkyl (meth)acrylates
JP2005239564A (ja) * 2004-02-24 2005-09-08 Mitsubishi Rayon Co Ltd （メタ）アクリル酸エステルの製造方法
CN101274890A (zh) * 2007-03-27 2008-10-01 罗姆有限公司 连续制造(甲基)丙烯酸烷基酯的方法

Also Published As

Publication number Publication date
KR20150095887A (ko) 2015-08-21
JP2016501271A (ja) 2016-01-18
US20150315120A1 (en) 2015-11-05
US10000439B2 (en) 2018-06-19
JP2018109019A (ja) 2018-07-12
FR2999572A1 (fr) 2014-06-20
CN104918911A (zh) 2015-09-16
JP6373276B2 (ja) 2018-08-15
EP2931695B1 (fr) 2017-04-12
BR112015013542A2 (pt) 2017-07-11
BR112015013542B1 (pt) 2020-09-24
EP2931695A1 (fr) 2015-10-21
WO2014096648A1 (fr) 2014-06-26
FR2999572B1 (fr) 2014-11-28
KR102079840B1 (ko) 2020-02-20

Similar Documents

Publication Publication Date Title
CN104918911B (zh) 丙烯酸烷基酯的制备方法
US9403750B2 (en) Method for producing 2-octyl acrylate by direct esterification
JP2016501271A5 (https=)
US9776946B2 (en) Process for producing 2-propylheptyl acrylate by transesterification
CN104053642B (zh) 通过酯交换制备丙烯酸2-辛基酯的方法
US6482976B1 (en) Processes for conducting equilibrium-limited reactions
US7569721B2 (en) Process for conducting equilibrium-limited reactions
WO2000078702A1 (en) Processes for conducting equilibrium-limited reactions
US9018410B2 (en) Method for the production of 2-octyl acrylate by means of transesterification
WO2001085666A2 (en) Improved refining processes

Legal Events

Date Code Title Description
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant