KR102046210B1 - 2,5-푸란디카르복실산의 제조 방법 - Google Patents

2,5-푸란디카르복실산의 제조 방법 Download PDF

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KR102046210B1
KR102046210B1 KR1020157027942A KR20157027942A KR102046210B1 KR 102046210 B1 KR102046210 B1 KR 102046210B1 KR 1020157027942 A KR1020157027942 A KR 1020157027942A KR 20157027942 A KR20157027942 A KR 20157027942A KR 102046210 B1 KR102046210 B1 KR 102046210B1
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hmf
fdca
catalyst
metal salt
aqueous solution
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KR20150127182A (ko
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알렉산드라 산보른
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아처 다니엘 미드랜드 캄파니
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74Iron group metals
    • B01J23/75Cobalt
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/70Nitro radicals
    • C07D307/71Nitro radicals attached in position 5
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
KR1020157027942A 2013-03-14 2014-03-05 2,5-푸란디카르복실산의 제조 방법 Active KR102046210B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361782589P 2013-03-14 2013-03-14
US61/782,589 2013-03-14
PCT/US2014/020482 WO2014158838A1 (en) 2013-03-14 2014-03-05 Process for making 2,5-furandicarboxylic acid

Publications (2)

Publication Number Publication Date
KR20150127182A KR20150127182A (ko) 2015-11-16
KR102046210B1 true KR102046210B1 (ko) 2019-11-18

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Country Status (14)

Country Link
US (1) US9562028B2 (enExample)
EP (1) EP2970170B1 (enExample)
JP (1) JP6208321B2 (enExample)
KR (1) KR102046210B1 (enExample)
CN (1) CN105026383A (enExample)
AU (1) AU2014241870B2 (enExample)
BR (1) BR112015022795B1 (enExample)
CA (1) CA2902493C (enExample)
ES (1) ES2663375T3 (enExample)
HU (1) HUE038483T2 (enExample)
MX (1) MX354925B (enExample)
RU (1) RU2640203C2 (enExample)
WO (1) WO2014158838A1 (enExample)
ZA (1) ZA201507571B (enExample)

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BR112017022224B1 (pt) 2015-04-14 2022-05-03 E I Du Pont De Nemours Processo integrado para produzir ácido 2,5-furanodicarboxílico e/ou um derivado do mesmo
KR101715169B1 (ko) * 2015-05-21 2017-03-10 한국생산기술연구원 2,5-푸란디카르복실산의 제조 방법
CN108368076B (zh) * 2015-12-10 2021-08-06 安尼基有限责任公司 制备2,5-呋喃二甲酸(fdca)的方法
BR112018014278B1 (pt) 2016-01-13 2022-07-12 Stora Enso Oyj Processos para a preparação de ácido 2,5-furandicarboxílico e intermediários e derivados dos mesmos
CN109195961A (zh) 2016-03-24 2019-01-11 孟山都技术公司 用于制备杂芳基羧酸的方法
JP2017190316A (ja) * 2016-04-15 2017-10-19 三菱ケミカル株式会社 2,5−フランジカルボン酸の精製方法
US10495130B2 (en) * 2016-11-11 2019-12-03 The Boeing Company Fasteners having enhanced electrical energy dispersion properties
CN108299357B (zh) * 2017-01-12 2025-08-12 中国科学院宁波材料技术与工程研究所 一种双取代呋喃化合物的制备方法
CN108314667B (zh) * 2017-01-18 2021-10-26 中国科学院过程工程研究所 一种非碱体系生物基2,5-呋喃二甲酸的制备方法
SG11201913469PA (en) 2017-07-12 2020-01-30 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
CN107739354B (zh) * 2017-10-09 2020-08-07 中国科学院过程工程研究所 一锅一步法由果糖制备2,5-呋喃二甲酸的方法
CN110452192A (zh) * 2018-05-07 2019-11-15 中国科学院宁波材料技术与工程研究所 一种制备5-羟甲基-2-呋喃甲醛的方法
EP3628667A1 (en) 2018-09-28 2020-04-01 Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO Process and salts for the preparation of 2,5-furandicarboxylic acid
CN113117705B (zh) * 2019-12-31 2024-05-07 中国石油化工股份有限公司 一种改性钌基催化剂及由其催化制备2,5-呋喃二羧酸的方法
CN115772143B (zh) * 2021-09-08 2024-06-11 中国石油化工股份有限公司 一种制备2,5-呋喃二甲酸的方法
CN117362251A (zh) * 2022-06-30 2024-01-09 中国石油化工股份有限公司 一种2,5-呋喃二甲酸的提纯方法

Citations (2)

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US20070232815A1 (en) * 2006-03-28 2007-10-04 Canon Kabushiki Kaisha Method for producing furan-2,5-dicarboxylic acid
WO2013033058A1 (en) * 2011-08-31 2013-03-07 Archer Daniels Midland Company Spray oxidation process for producing 2,5-furandicarboxylic acid from hydroxymethylfurfural

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SU636233A1 (ru) * 1976-06-24 1978-12-05 Ордена Трудового Красного Знамени Институт Органического Синтеза Ан Латвийской Сср Способ получени 2,5-фурандикарбоновой кислоты
JP5147309B2 (ja) * 2007-06-21 2013-02-20 キヤノン株式会社 2,5−フランジカルボン酸の製造方法
JP2009013079A (ja) * 2007-07-02 2009-01-22 Canon Inc フラン−2,5−ジカルボン酸の製造方法
BRPI0819406B1 (pt) * 2007-12-12 2021-07-20 Archer Daniels Midland Co Método para oxidar um éster de 2-hidroximetil-5-furaldeído (hmf) em ácido 2,5- furanodicarboxílico (fdca)
DE102009005517A1 (de) * 2009-01-20 2010-07-22 Tesa Se Verfahren zur Korrosionsschutzbehandlung
CN102459214B (zh) * 2009-05-14 2015-01-21 阿彻丹尼尔斯米德兰德公司 糠醛化合物的氧化
US8865921B2 (en) * 2009-10-07 2014-10-21 Furanix Technologies B.V. Method for the preparation of 2,5-furandicarboxylic acid and for the preparation of the dialkyl ester of 2,5-furandicarboxylic acid
JP5550303B2 (ja) * 2009-10-19 2014-07-16 キヤノン株式会社 2,5−フランジカルボン酸の製造方法
IT1401911B1 (it) * 2010-08-06 2013-08-28 Novamont Spa Processo per la sintesi di acido 2,5-furandicarbossilico
US8846960B2 (en) * 2011-05-24 2014-09-30 Eastman Chemical Company Oxidation process to produce a crude and/or purified carboxylic acid product
JP2013203666A (ja) * 2012-03-27 2013-10-07 Kao Corp 5−ヒドロキシメチルフルフラール酸化物の製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070232815A1 (en) * 2006-03-28 2007-10-04 Canon Kabushiki Kaisha Method for producing furan-2,5-dicarboxylic acid
WO2013033058A1 (en) * 2011-08-31 2013-03-07 Archer Daniels Midland Company Spray oxidation process for producing 2,5-furandicarboxylic acid from hydroxymethylfurfural

Also Published As

Publication number Publication date
CA2902493A1 (en) 2014-10-02
BR112015022795A2 (pt) 2017-07-18
HUE038483T2 (hu) 2018-10-29
WO2014158838A1 (en) 2014-10-02
MX354925B (es) 2018-03-23
RU2015139511A (ru) 2017-04-17
EP2970170B1 (en) 2017-12-20
CA2902493C (en) 2019-12-24
KR20150127182A (ko) 2015-11-16
AU2014241870B2 (en) 2017-06-08
EP2970170A1 (en) 2016-01-20
RU2640203C2 (ru) 2017-12-27
JP6208321B2 (ja) 2017-10-04
ES2663375T3 (es) 2018-04-12
ZA201507571B (en) 2017-01-25
AU2014241870A1 (en) 2015-08-27
BR112015022795B1 (pt) 2021-05-18
MX2015011912A (es) 2015-12-01
US9562028B2 (en) 2017-02-07
EP2970170A4 (en) 2016-04-27
JP2016513641A (ja) 2016-05-16
CN105026383A (zh) 2015-11-04
US20160016926A1 (en) 2016-01-21

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