KR102046210B1 - 2,5-푸란디카르복실산의 제조 방법 - Google Patents
2,5-푸란디카르복실산의 제조 방법 Download PDFInfo
- Publication number
- KR102046210B1 KR102046210B1 KR1020157027942A KR20157027942A KR102046210B1 KR 102046210 B1 KR102046210 B1 KR 102046210B1 KR 1020157027942 A KR1020157027942 A KR 1020157027942A KR 20157027942 A KR20157027942 A KR 20157027942A KR 102046210 B1 KR102046210 B1 KR 102046210B1
- Authority
- KR
- South Korea
- Prior art keywords
- hmf
- fdca
- catalyst
- metal salt
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/75—Cobalt
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/70—Nitro radicals
- C07D307/71—Nitro radicals attached in position 5
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361782589P | 2013-03-14 | 2013-03-14 | |
| US61/782,589 | 2013-03-14 | ||
| PCT/US2014/020482 WO2014158838A1 (en) | 2013-03-14 | 2014-03-05 | Process for making 2,5-furandicarboxylic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150127182A KR20150127182A (ko) | 2015-11-16 |
| KR102046210B1 true KR102046210B1 (ko) | 2019-11-18 |
Family
ID=51625063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020157027942A Active KR102046210B1 (ko) | 2013-03-14 | 2014-03-05 | 2,5-푸란디카르복실산의 제조 방법 |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9562028B2 (enExample) |
| EP (1) | EP2970170B1 (enExample) |
| JP (1) | JP6208321B2 (enExample) |
| KR (1) | KR102046210B1 (enExample) |
| CN (1) | CN105026383A (enExample) |
| AU (1) | AU2014241870B2 (enExample) |
| BR (1) | BR112015022795B1 (enExample) |
| CA (1) | CA2902493C (enExample) |
| ES (1) | ES2663375T3 (enExample) |
| HU (1) | HUE038483T2 (enExample) |
| MX (1) | MX354925B (enExample) |
| RU (1) | RU2640203C2 (enExample) |
| WO (1) | WO2014158838A1 (enExample) |
| ZA (1) | ZA201507571B (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112017022224B1 (pt) | 2015-04-14 | 2022-05-03 | E I Du Pont De Nemours | Processo integrado para produzir ácido 2,5-furanodicarboxílico e/ou um derivado do mesmo |
| KR101715169B1 (ko) * | 2015-05-21 | 2017-03-10 | 한국생산기술연구원 | 2,5-푸란디카르복실산의 제조 방법 |
| CN108368076B (zh) * | 2015-12-10 | 2021-08-06 | 安尼基有限责任公司 | 制备2,5-呋喃二甲酸(fdca)的方法 |
| BR112018014278B1 (pt) | 2016-01-13 | 2022-07-12 | Stora Enso Oyj | Processos para a preparação de ácido 2,5-furandicarboxílico e intermediários e derivados dos mesmos |
| CN109195961A (zh) | 2016-03-24 | 2019-01-11 | 孟山都技术公司 | 用于制备杂芳基羧酸的方法 |
| JP2017190316A (ja) * | 2016-04-15 | 2017-10-19 | 三菱ケミカル株式会社 | 2,5−フランジカルボン酸の精製方法 |
| US10495130B2 (en) * | 2016-11-11 | 2019-12-03 | The Boeing Company | Fasteners having enhanced electrical energy dispersion properties |
| CN108299357B (zh) * | 2017-01-12 | 2025-08-12 | 中国科学院宁波材料技术与工程研究所 | 一种双取代呋喃化合物的制备方法 |
| CN108314667B (zh) * | 2017-01-18 | 2021-10-26 | 中国科学院过程工程研究所 | 一种非碱体系生物基2,5-呋喃二甲酸的制备方法 |
| SG11201913469PA (en) | 2017-07-12 | 2020-01-30 | Stora Enso Oyj | Purified 2,5-furandicarboxylic acid pathway products |
| CN107739354B (zh) * | 2017-10-09 | 2020-08-07 | 中国科学院过程工程研究所 | 一锅一步法由果糖制备2,5-呋喃二甲酸的方法 |
| CN110452192A (zh) * | 2018-05-07 | 2019-11-15 | 中国科学院宁波材料技术与工程研究所 | 一种制备5-羟甲基-2-呋喃甲醛的方法 |
| EP3628667A1 (en) | 2018-09-28 | 2020-04-01 | Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO | Process and salts for the preparation of 2,5-furandicarboxylic acid |
| CN113117705B (zh) * | 2019-12-31 | 2024-05-07 | 中国石油化工股份有限公司 | 一种改性钌基催化剂及由其催化制备2,5-呋喃二羧酸的方法 |
| CN115772143B (zh) * | 2021-09-08 | 2024-06-11 | 中国石油化工股份有限公司 | 一种制备2,5-呋喃二甲酸的方法 |
| CN117362251A (zh) * | 2022-06-30 | 2024-01-09 | 中国石油化工股份有限公司 | 一种2,5-呋喃二甲酸的提纯方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070232815A1 (en) * | 2006-03-28 | 2007-10-04 | Canon Kabushiki Kaisha | Method for producing furan-2,5-dicarboxylic acid |
| WO2013033058A1 (en) * | 2011-08-31 | 2013-03-07 | Archer Daniels Midland Company | Spray oxidation process for producing 2,5-furandicarboxylic acid from hydroxymethylfurfural |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU636233A1 (ru) * | 1976-06-24 | 1978-12-05 | Ордена Трудового Красного Знамени Институт Органического Синтеза Ан Латвийской Сср | Способ получени 2,5-фурандикарбоновой кислоты |
| JP5147309B2 (ja) * | 2007-06-21 | 2013-02-20 | キヤノン株式会社 | 2,5−フランジカルボン酸の製造方法 |
| JP2009013079A (ja) * | 2007-07-02 | 2009-01-22 | Canon Inc | フラン−2,5−ジカルボン酸の製造方法 |
| BRPI0819406B1 (pt) * | 2007-12-12 | 2021-07-20 | Archer Daniels Midland Co | Método para oxidar um éster de 2-hidroximetil-5-furaldeído (hmf) em ácido 2,5- furanodicarboxílico (fdca) |
| DE102009005517A1 (de) * | 2009-01-20 | 2010-07-22 | Tesa Se | Verfahren zur Korrosionsschutzbehandlung |
| CN102459214B (zh) * | 2009-05-14 | 2015-01-21 | 阿彻丹尼尔斯米德兰德公司 | 糠醛化合物的氧化 |
| US8865921B2 (en) * | 2009-10-07 | 2014-10-21 | Furanix Technologies B.V. | Method for the preparation of 2,5-furandicarboxylic acid and for the preparation of the dialkyl ester of 2,5-furandicarboxylic acid |
| JP5550303B2 (ja) * | 2009-10-19 | 2014-07-16 | キヤノン株式会社 | 2,5−フランジカルボン酸の製造方法 |
| IT1401911B1 (it) * | 2010-08-06 | 2013-08-28 | Novamont Spa | Processo per la sintesi di acido 2,5-furandicarbossilico |
| US8846960B2 (en) * | 2011-05-24 | 2014-09-30 | Eastman Chemical Company | Oxidation process to produce a crude and/or purified carboxylic acid product |
| JP2013203666A (ja) * | 2012-03-27 | 2013-10-07 | Kao Corp | 5−ヒドロキシメチルフルフラール酸化物の製造方法 |
-
2014
- 2014-03-05 MX MX2015011912A patent/MX354925B/es active IP Right Grant
- 2014-03-05 CN CN201480010774.0A patent/CN105026383A/zh active Pending
- 2014-03-05 US US14/771,832 patent/US9562028B2/en active Active
- 2014-03-05 JP JP2016500624A patent/JP6208321B2/ja active Active
- 2014-03-05 AU AU2014241870A patent/AU2014241870B2/en active Active
- 2014-03-05 WO PCT/US2014/020482 patent/WO2014158838A1/en not_active Ceased
- 2014-03-05 KR KR1020157027942A patent/KR102046210B1/ko active Active
- 2014-03-05 CA CA2902493A patent/CA2902493C/en active Active
- 2014-03-05 EP EP14773033.7A patent/EP2970170B1/en active Active
- 2014-03-05 ES ES14773033.7T patent/ES2663375T3/es active Active
- 2014-03-05 RU RU2015139511A patent/RU2640203C2/ru active
- 2014-03-05 BR BR112015022795-3A patent/BR112015022795B1/pt active IP Right Grant
- 2014-03-05 HU HUE14773033A patent/HUE038483T2/hu unknown
-
2015
- 2015-10-12 ZA ZA2015/07571A patent/ZA201507571B/en unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070232815A1 (en) * | 2006-03-28 | 2007-10-04 | Canon Kabushiki Kaisha | Method for producing furan-2,5-dicarboxylic acid |
| WO2013033058A1 (en) * | 2011-08-31 | 2013-03-07 | Archer Daniels Midland Company | Spray oxidation process for producing 2,5-furandicarboxylic acid from hydroxymethylfurfural |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2902493A1 (en) | 2014-10-02 |
| BR112015022795A2 (pt) | 2017-07-18 |
| HUE038483T2 (hu) | 2018-10-29 |
| WO2014158838A1 (en) | 2014-10-02 |
| MX354925B (es) | 2018-03-23 |
| RU2015139511A (ru) | 2017-04-17 |
| EP2970170B1 (en) | 2017-12-20 |
| CA2902493C (en) | 2019-12-24 |
| KR20150127182A (ko) | 2015-11-16 |
| AU2014241870B2 (en) | 2017-06-08 |
| EP2970170A1 (en) | 2016-01-20 |
| RU2640203C2 (ru) | 2017-12-27 |
| JP6208321B2 (ja) | 2017-10-04 |
| ES2663375T3 (es) | 2018-04-12 |
| ZA201507571B (en) | 2017-01-25 |
| AU2014241870A1 (en) | 2015-08-27 |
| BR112015022795B1 (pt) | 2021-05-18 |
| MX2015011912A (es) | 2015-12-01 |
| US9562028B2 (en) | 2017-02-07 |
| EP2970170A4 (en) | 2016-04-27 |
| JP2016513641A (ja) | 2016-05-16 |
| CN105026383A (zh) | 2015-11-04 |
| US20160016926A1 (en) | 2016-01-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
St.27 status event code: A-0-1-A10-A15-nap-PA0105 |
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| PG1501 | Laying open of application |
St.27 status event code: A-1-1-Q10-Q12-nap-PG1501 |
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| P22-X000 | Classification modified |
St.27 status event code: A-2-2-P10-P22-nap-X000 |
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| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
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| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
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| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
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| PA0302 | Request for accelerated examination |
St.27 status event code: A-1-2-D10-D17-exm-PA0302 St.27 status event code: A-1-2-D10-D16-exm-PA0302 |
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| PE0902 | Notice of grounds for rejection |
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| P11-X000 | Amendment of application requested |
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| P13-X000 | Application amended |
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| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
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| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
St.27 status event code: A-2-4-F10-F11-exm-PR0701 |
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