CA2902493C - Process for making 2,5-furandicarboxylic acid - Google Patents
Process for making 2,5-furandicarboxylic acid Download PDFInfo
- Publication number
- CA2902493C CA2902493C CA2902493A CA2902493A CA2902493C CA 2902493 C CA2902493 C CA 2902493C CA 2902493 A CA2902493 A CA 2902493A CA 2902493 A CA2902493 A CA 2902493A CA 2902493 C CA2902493 C CA 2902493C
- Authority
- CA
- Canada
- Prior art keywords
- hmf
- fdca
- catalyst
- aqueous solution
- metal salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/70—Nitro radicals
- C07D307/71—Nitro radicals attached in position 5
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361782589P | 2013-03-14 | 2013-03-14 | |
| US61/782,589 | 2013-03-14 | ||
| PCT/US2014/020482 WO2014158838A1 (en) | 2013-03-14 | 2014-03-05 | Process for making 2,5-furandicarboxylic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2902493A1 CA2902493A1 (en) | 2014-10-02 |
| CA2902493C true CA2902493C (en) | 2019-12-24 |
Family
ID=51625063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2902493A Active CA2902493C (en) | 2013-03-14 | 2014-03-05 | Process for making 2,5-furandicarboxylic acid |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US9562028B2 (enExample) |
| EP (1) | EP2970170B1 (enExample) |
| JP (1) | JP6208321B2 (enExample) |
| KR (1) | KR102046210B1 (enExample) |
| CN (1) | CN105026383A (enExample) |
| AU (1) | AU2014241870B2 (enExample) |
| BR (1) | BR112015022795B1 (enExample) |
| CA (1) | CA2902493C (enExample) |
| ES (1) | ES2663375T3 (enExample) |
| HU (1) | HUE038483T2 (enExample) |
| MX (1) | MX354925B (enExample) |
| RU (1) | RU2640203C2 (enExample) |
| WO (1) | WO2014158838A1 (enExample) |
| ZA (1) | ZA201507571B (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107848995B (zh) | 2015-04-14 | 2021-12-28 | 杜邦公司 | 用于生产2,5-呋喃二甲酸及其衍生物以及由其制成的聚合物的方法 |
| KR101715169B1 (ko) * | 2015-05-21 | 2017-03-10 | 한국생산기술연구원 | 2,5-푸란디카르복실산의 제조 방법 |
| JP6943855B2 (ja) * | 2015-12-10 | 2021-10-06 | アニッキ ゲーエムベーハーAnnikki Gmbh | 2,5−フランジカルボン酸(fdca)の製造方法 |
| SG11201805514VA (en) | 2016-01-13 | 2018-07-30 | Stora Enso Oyj | Processes for the preparation of 2,5-furandicarboxylic acid and intermediates and derivatives thereof |
| WO2017165356A1 (en) | 2016-03-24 | 2017-09-28 | Monsanto Technology Llc | Processes for the preparation of heteroaryl carboxylic acids |
| JP2017190316A (ja) * | 2016-04-15 | 2017-10-19 | 三菱ケミカル株式会社 | 2,5−フランジカルボン酸の精製方法 |
| US10495130B2 (en) * | 2016-11-11 | 2019-12-03 | The Boeing Company | Fasteners having enhanced electrical energy dispersion properties |
| CN108299357B (zh) * | 2017-01-12 | 2025-08-12 | 中国科学院宁波材料技术与工程研究所 | 一种双取代呋喃化合物的制备方法 |
| CN108314667B (zh) * | 2017-01-18 | 2021-10-26 | 中国科学院过程工程研究所 | 一种非碱体系生物基2,5-呋喃二甲酸的制备方法 |
| EP3652161A1 (en) | 2017-07-12 | 2020-05-20 | Stora Enso Oyj | Purified 2,5-furandicarboxylic acid pathway products |
| CN107739354B (zh) * | 2017-10-09 | 2020-08-07 | 中国科学院过程工程研究所 | 一锅一步法由果糖制备2,5-呋喃二甲酸的方法 |
| CN110452192A (zh) * | 2018-05-07 | 2019-11-15 | 中国科学院宁波材料技术与工程研究所 | 一种制备5-羟甲基-2-呋喃甲醛的方法 |
| EP3628667A1 (en) | 2018-09-28 | 2020-04-01 | Nederlandse Organisatie voor toegepast- natuurwetenschappelijk onderzoek TNO | Process and salts for the preparation of 2,5-furandicarboxylic acid |
| CN113117705B (zh) * | 2019-12-31 | 2024-05-07 | 中国石油化工股份有限公司 | 一种改性钌基催化剂及由其催化制备2,5-呋喃二羧酸的方法 |
| CN115772143B (zh) * | 2021-09-08 | 2024-06-11 | 中国石油化工股份有限公司 | 一种制备2,5-呋喃二甲酸的方法 |
| CN117362251A (zh) * | 2022-06-30 | 2024-01-09 | 中国石油化工股份有限公司 | 一种2,5-呋喃二甲酸的提纯方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU636233A1 (ru) * | 1976-06-24 | 1978-12-05 | Ордена Трудового Красного Знамени Институт Органического Синтеза Ан Латвийской Сср | Способ получени 2,5-фурандикарбоновой кислоты |
| JP4804187B2 (ja) * | 2006-03-28 | 2011-11-02 | キヤノン株式会社 | フラン−2,5−ジカルボン酸の製造方法 |
| JP5147309B2 (ja) * | 2007-06-21 | 2013-02-20 | キヤノン株式会社 | 2,5−フランジカルボン酸の製造方法 |
| JP2009013079A (ja) * | 2007-07-02 | 2009-01-22 | Canon Inc | フラン−2,5−ジカルボン酸の製造方法 |
| KR101576313B1 (ko) * | 2007-12-12 | 2015-12-09 | 아처 다니엘 미드랜드 캄파니 | 탄수화물의 히드록시메틸퓨르퓨랄(hmf) 및 그 유도체로의 전환 |
| DE102009005517A1 (de) * | 2009-01-20 | 2010-07-22 | Tesa Se | Verfahren zur Korrosionsschutzbehandlung |
| EP3257845A1 (en) * | 2009-05-14 | 2017-12-20 | Archer Daniels Midland Company | Preparation of 2,5-furandicarboxylic acid by oxidation of 5-(acetoxymethyl)furfural in the presence of a bromide, oxygen and a cobalt(ii) or cerium(iii) catalyst |
| EP3666764A1 (en) * | 2009-10-07 | 2020-06-17 | Furanix Technologies B.V | Method for the preparation of 2,5-furandicarboxylic acid and for the preparation of the dialkyl ester of 2,5-furandicarboxylic acid |
| JP5550303B2 (ja) * | 2009-10-19 | 2014-07-16 | キヤノン株式会社 | 2,5−フランジカルボン酸の製造方法 |
| IT1401911B1 (it) * | 2010-08-06 | 2013-08-28 | Novamont Spa | Processo per la sintesi di acido 2,5-furandicarbossilico |
| US8846960B2 (en) * | 2011-05-24 | 2014-09-30 | Eastman Chemical Company | Oxidation process to produce a crude and/or purified carboxylic acid product |
| PT2750789T (pt) * | 2011-08-31 | 2018-10-30 | Archer Daniels Midland Co | Processo de oxidação em spray para produzir ácido 2,5- furandicarboxílico a partir de hidroxi-metilfurfural |
| JP2013203666A (ja) * | 2012-03-27 | 2013-10-07 | Kao Corp | 5−ヒドロキシメチルフルフラール酸化物の製造方法 |
-
2014
- 2014-03-05 RU RU2015139511A patent/RU2640203C2/ru active
- 2014-03-05 CN CN201480010774.0A patent/CN105026383A/zh active Pending
- 2014-03-05 MX MX2015011912A patent/MX354925B/es active IP Right Grant
- 2014-03-05 EP EP14773033.7A patent/EP2970170B1/en active Active
- 2014-03-05 HU HUE14773033A patent/HUE038483T2/hu unknown
- 2014-03-05 CA CA2902493A patent/CA2902493C/en active Active
- 2014-03-05 US US14/771,832 patent/US9562028B2/en active Active
- 2014-03-05 JP JP2016500624A patent/JP6208321B2/ja active Active
- 2014-03-05 BR BR112015022795-3A patent/BR112015022795B1/pt active IP Right Grant
- 2014-03-05 AU AU2014241870A patent/AU2014241870B2/en active Active
- 2014-03-05 WO PCT/US2014/020482 patent/WO2014158838A1/en not_active Ceased
- 2014-03-05 KR KR1020157027942A patent/KR102046210B1/ko active Active
- 2014-03-05 ES ES14773033.7T patent/ES2663375T3/es active Active
-
2015
- 2015-10-12 ZA ZA2015/07571A patent/ZA201507571B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU2014241870B2 (en) | 2017-06-08 |
| MX354925B (es) | 2018-03-23 |
| ES2663375T3 (es) | 2018-04-12 |
| RU2015139511A (ru) | 2017-04-17 |
| BR112015022795B1 (pt) | 2021-05-18 |
| HUE038483T2 (hu) | 2018-10-29 |
| AU2014241870A1 (en) | 2015-08-27 |
| EP2970170B1 (en) | 2017-12-20 |
| CA2902493A1 (en) | 2014-10-02 |
| JP6208321B2 (ja) | 2017-10-04 |
| EP2970170A4 (en) | 2016-04-27 |
| KR20150127182A (ko) | 2015-11-16 |
| KR102046210B1 (ko) | 2019-11-18 |
| US20160016926A1 (en) | 2016-01-21 |
| MX2015011912A (es) | 2015-12-01 |
| WO2014158838A1 (en) | 2014-10-02 |
| CN105026383A (zh) | 2015-11-04 |
| JP2016513641A (ja) | 2016-05-16 |
| US9562028B2 (en) | 2017-02-07 |
| EP2970170A1 (en) | 2016-01-20 |
| RU2640203C2 (ru) | 2017-12-27 |
| ZA201507571B (en) | 2017-01-25 |
| BR112015022795A2 (pt) | 2017-07-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20190305 |
|
| MPN | Maintenance fee for patent paid |
Free format text: FEE DESCRIPTION TEXT: MF (PATENT, 11TH ANNIV.) - STANDARD Year of fee payment: 11 |
|
| U00 | Fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U00-U101 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE REQUEST RECEIVED Effective date: 20250220 |
|
| U11 | Full renewal or maintenance fee paid |
Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-U102 (AS PROVIDED BY THE NATIONAL OFFICE); EVENT TEXT: MAINTENANCE FEE PAYMENT PAID IN FULL Effective date: 20250808 |