KR101925339B1 - 2,3,3,3-테트라플루오로-2-프로펜의 제조방법 - Google Patents

2,3,3,3-테트라플루오로-2-프로펜의 제조방법 Download PDF

Info

Publication number
KR101925339B1
KR101925339B1 KR1020137021634A KR20137021634A KR101925339B1 KR 101925339 B1 KR101925339 B1 KR 101925339B1 KR 1020137021634 A KR1020137021634 A KR 1020137021634A KR 20137021634 A KR20137021634 A KR 20137021634A KR 101925339 B1 KR101925339 B1 KR 101925339B1
Authority
KR
South Korea
Prior art keywords
tcp
tetrafluoro
tetrachloropropene
propene
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020137021634A
Other languages
English (en)
Korean (ko)
Other versions
KR20140004725A (ko
Inventor
스티븐 에이. 코트렐
유온 치유
할루크 콥칼리
슈에 성 퉁
케빈 디. 유리치
피터 쉐이들
Original Assignee
허니웰 인터내셔널 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 허니웰 인터내셔널 인코포레이티드 filed Critical 허니웰 인터내셔널 인코포레이티드
Publication of KR20140004725A publication Critical patent/KR20140004725A/ko
Application granted granted Critical
Publication of KR101925339B1 publication Critical patent/KR101925339B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/21—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms with simultaneous increase of the number of halogen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/18—Arsenic, antimony or bismuth
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/07—Preparation of halogenated hydrocarbons by addition of hydrogen halides
    • C07C17/087—Preparation of halogenated hydrocarbons by addition of hydrogen halides to unsaturated halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020137021634A 2011-01-19 2012-01-13 2,3,3,3-테트라플루오로-2-프로펜의 제조방법 Expired - Fee Related KR101925339B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201161434005P 2011-01-19 2011-01-19
US61/434,005 2011-01-19
US13/313,649 US9890096B2 (en) 2011-01-19 2011-12-07 Methods of making 2,3,3,3-tetrafluoro-2-propene
US13/313,649 2011-12-07
PCT/US2012/021158 WO2012099776A1 (en) 2011-01-19 2012-01-13 Methods of making 2,3,3,3-tetrafluoro-2-propene

Publications (2)

Publication Number Publication Date
KR20140004725A KR20140004725A (ko) 2014-01-13
KR101925339B1 true KR101925339B1 (ko) 2019-02-27

Family

ID=46491269

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020137021634A Expired - Fee Related KR101925339B1 (ko) 2011-01-19 2012-01-13 2,3,3,3-테트라플루오로-2-프로펜의 제조방법

Country Status (8)

Country Link
US (1) US9890096B2 (enExample)
EP (1) EP2665696B1 (enExample)
JP (1) JP5953317B2 (enExample)
KR (1) KR101925339B1 (enExample)
CN (2) CN103534228A (enExample)
ES (1) ES2666489T3 (enExample)
MX (1) MX2013008287A (enExample)
WO (1) WO2012099776A1 (enExample)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8927791B2 (en) * 2010-04-29 2015-01-06 Honeywell International Inc. Method for producing tetrafluoropropenes
EP2755937B1 (en) 2011-09-15 2019-10-30 Daikin Industries, Ltd. Method for purifying chlorinated hydrocarbon
ES2709201T3 (es) 2013-03-12 2019-04-15 Honeywell Int Inc Un método de mitigar la formación de HCF-245cb durante la hidrofluoración de HCFO-1233xf en HCFC-244bb
WO2014165094A1 (en) * 2013-03-13 2014-10-09 Honeywell International Inc. Staged fluorination process and reactor system
US9272968B2 (en) 2013-03-14 2016-03-01 Honeywell International Inc. Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture
US9353029B2 (en) 2013-03-14 2016-05-31 Honeywell International, Inc. Fluorination process and reactor
US20140275651A1 (en) * 2013-03-15 2014-09-18 Honeywell International Inc. Process for producing 2,3,3,3-tetrafluoropropene
EP2986583B1 (en) * 2013-04-18 2019-07-17 Honeywell International Inc. Reaction system and process to produce fluorinated organics
JP2017512133A (ja) * 2014-02-10 2017-05-18 ハネウェル・インターナショナル・インコーポレーテッド 液相フッ素化のための反応器デザイン
KR20160122786A (ko) * 2014-02-10 2016-10-24 허니웰 인터내셔날 인코포레이티드 액상 플루오르화 반응을 위한 반응기
US9975824B2 (en) 2014-09-30 2018-05-22 Daikin Industries, Ltd. Method for producing 2,3,3,3-tetrafluoropropene
JP6210073B2 (ja) * 2015-01-21 2017-10-11 ダイキン工業株式会社 フルオロプロペンの製造方法
EP3286160A4 (en) * 2015-04-24 2019-01-16 Honeywell International Inc. METHOD FOR REDUCING 1233XF CONCENTRATION IN 244BB
CN107635955A (zh) * 2015-05-21 2018-01-26 科慕埃弗西有限公司 通过SbF5进行的1233xf至244bb的氢氟化
GB201512510D0 (en) 2015-07-17 2015-08-19 Mexichem Fluor Sa De Cv Process
GB2540427B (en) 2015-07-17 2017-07-19 Mexichem Fluor Sa De Cv Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf)
US9938213B2 (en) * 2015-08-19 2018-04-10 Honeywell International Inc. Methods for removing acidic impurities from halogenated propenes
GB201701099D0 (en) * 2017-01-23 2017-03-08 Mexichem Fluor Sa De Cv Process
KR101992230B1 (ko) 2017-08-08 2019-06-25 (주)후성 기상 촉매를 이용한 1,1,1-트리플루오로-2-클로로프로펜과 1,1,1,2-테트라플루오로프로펜의 동시 제조 방법
US10233137B1 (en) 2017-10-13 2019-03-19 Honeywell International Inc. Method for removing unsaturated halogenated impurities from 2,3,3,3-tetrafluoropropene (HFO-1234yf)
US10351494B1 (en) 2018-01-08 2019-07-16 Honeywell International Inc. Systems and methods for reducing the formation of impurities during 244bb dehydrochlorination to 1234yf
US10246389B1 (en) 2018-01-08 2019-04-02 Honeywell International Inc. Compositions containing 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb)
CN119118781A (zh) 2018-06-06 2024-12-13 霍尼韦尔国际公司 用于HCFC-244bb的脱氯化氢以制备HFO-1234yf的方法
US10941091B2 (en) 2018-12-03 2021-03-09 Honeywell International Inc. Processes for producing high-purity trifluoroiodomethane
US20220080243A1 (en) * 2020-09-11 2022-03-17 Honeywell International Inc. Azeotrope or azeotrope-like compositions of trifluoroiodomethane (cf3i) and water

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007079431A2 (en) 2006-01-03 2007-07-12 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2008054779A1 (en) 2006-10-31 2008-05-08 E. I. Du Pont De Nemours And Company Processes for producing 2,3,3,3-tetrafluoropropene and/or 1,2,3,3-tetrafluoropropene
US20090240090A1 (en) * 2004-04-29 2009-09-24 Honeywell International Inc. Integrated process to produce 2,3,3,3-tetrafluoropropene
WO2009140563A1 (en) 2008-05-15 2009-11-19 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2010059493A1 (en) * 2008-11-19 2010-05-27 Arkema Inc. Process for the manufacture of hydrofluoroolefins

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5271918A (en) * 1991-03-11 1993-12-21 Alliedsignal Inc. Furnace gas - sulfuric acid contact process for HF manufacture
ES2155201T3 (es) * 1995-10-10 2001-05-01 Ici Plc Procedimiento para la recuperacion de fluoruro de hidrogeno.
US7880040B2 (en) * 2004-04-29 2011-02-01 Honeywell International Inc. Method for producing fluorinated organic compounds
US8084653B2 (en) * 2004-04-29 2011-12-27 Honeywell International, Inc. Method for producing fluorinated organic compounds
US9102579B2 (en) * 2004-04-29 2015-08-11 Honeywell International Inc. Method for producing fluorinated organic compounds
US8664455B2 (en) * 2008-08-08 2014-03-04 Honeywell International Inc. Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb)
US8071825B2 (en) * 2006-01-03 2011-12-06 Honeywell International Inc. Method for producing fluorinated organic compounds
GB0611742D0 (en) * 2006-06-14 2006-07-26 Ineos Fluor Holdings Ltd Desiccants for fluids
GB0625214D0 (en) * 2006-12-19 2007-01-24 Ineos Fluor Holdings Ltd Process
CN101597209A (zh) * 2008-03-20 2009-12-09 霍尼韦尔国际公司 用于制备2,3,3,3-四氟丙烯的一体式方法
GB0806389D0 (en) 2008-04-09 2008-05-14 Ineos Fluor Holdings Ltd Process
GB0808836D0 (en) 2008-05-15 2008-06-18 Ineos Fluor Ltd Process
US8916733B2 (en) * 2008-06-17 2014-12-23 Honeywell International Inc. Processes for hydrofluorination of 2-chloro-3,3,3-trifluoropropene to 2-chloro-1,1,1,2-tetrafluoropropane
JP2011525925A (ja) 2008-06-26 2011-09-29 アーケマ・インコーポレイテッド １２３０ｘａから１２３４ｙｆへの触媒的気相フッ素化
FR2933402B1 (fr) 2008-07-03 2010-07-30 Arkema France Procede de purification de 2,3,3,3-tetrafluoro-1-propene (hfo1234yf)
ES2365303T3 (es) * 2008-08-08 2011-09-28 Honeywell International Inc. Proceso mejorado para fabricar 2-cloro-1,1,1,2-tetrafluoropropano (hcfc-244bb).
US8618340B2 (en) 2009-11-03 2013-12-31 Honeywell International Inc. Integrated process for fluoro-olefin production
SI3581631T1 (sl) 2009-12-22 2025-04-30 The Chemours Company Fc, Llc Sestavki, ki obsegajo 2,3,3,3-tetrafluoropropen
WO2011077191A1 (en) 2009-12-23 2011-06-30 Arkema France Catalytic gas phase fluorination of 1230xa to 1234yf
EP2545021B1 (en) 2010-03-10 2016-09-28 Arkema France Process of fluorination in liquid phase

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090240090A1 (en) * 2004-04-29 2009-09-24 Honeywell International Inc. Integrated process to produce 2,3,3,3-tetrafluoropropene
WO2007079431A2 (en) 2006-01-03 2007-07-12 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2008054779A1 (en) 2006-10-31 2008-05-08 E. I. Du Pont De Nemours And Company Processes for producing 2,3,3,3-tetrafluoropropene and/or 1,2,3,3-tetrafluoropropene
JP2009227675A (ja) 2008-03-20 2009-10-08 Honeywell Internatl Inc ２，３，３，３−テトラフルオロプロペンを生成するための総合プロセス
WO2009140563A1 (en) 2008-05-15 2009-11-19 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2010059493A1 (en) * 2008-11-19 2010-05-27 Arkema Inc. Process for the manufacture of hydrofluoroolefins

Also Published As

Publication number Publication date
MX2013008287A (es) 2013-09-13
ES2666489T3 (es) 2018-05-04
JP2014510716A (ja) 2014-05-01
CN108358745A (zh) 2018-08-03
EP2665696A1 (en) 2013-11-27
US9890096B2 (en) 2018-02-13
WO2012099776A1 (en) 2012-07-26
US20120184785A1 (en) 2012-07-19
EP2665696A4 (en) 2015-12-23
CN103534228A (zh) 2014-01-22
KR20140004725A (ko) 2014-01-13
EP2665696B1 (en) 2018-03-14
JP5953317B2 (ja) 2016-07-20

Similar Documents

Publication Publication Date Title
KR101925339B1 (ko) 2,3,3,3-테트라플루오로-2-프로펜의 제조방법
JP5732062B2 (ja) フルオロオレフィンを製造するための統合方法
KR101869851B1 (ko) 트랜스-1-클로로-3,3,3-트리플루오로프로펜, 트랜스-1,3,3,3-테트라플루오로 프로펜, 및 1,1,1,3,3-펜타플루오로프로판을 공동으로 제조하는 통합 방법
US9682905B2 (en) Integrated process for the production of 1-chloro-3,3,3-trifluoropropene
JP6220352B2 (ja) ＨＣＦＣ−１２３３ｚｄの生産方法
EP2611761B1 (en) Continuous low-temperature process to produce trans-1-chloro-3,3,3-trifluoropropene
JP2015515464A (ja) ｔｒａｎｓ−１−クロロ−３，３，３−トリフルオロプロペン、ｔｒａｎｓ−１，３，３，３−テトラフルオロプロペンおよび１，１，１，３，３−ペンタフルオロプロパンを併産するための統合プロセス

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20211130

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20211130