KR101850562B1 - 원료 1,3-부타디엔으로부터 순수한 1,3-부타디엔의 증류 추출을 위한 방법 및 장치 - Google Patents

원료 1,3-부타디엔으로부터 순수한 1,3-부타디엔의 증류 추출을 위한 방법 및 장치 Download PDF

Info

Publication number
KR101850562B1
KR101850562B1 KR1020127026467A KR20127026467A KR101850562B1 KR 101850562 B1 KR101850562 B1 KR 101850562B1 KR 1020127026467 A KR1020127026467 A KR 1020127026467A KR 20127026467 A KR20127026467 A KR 20127026467A KR 101850562 B1 KR101850562 B1 KR 101850562B1
Authority
KR
South Korea
Prior art keywords
butadiene
column
fraction
stream
extractive distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020127026467A
Other languages
English (en)
Korean (ko)
Other versions
KR20130016264A (ko
Inventor
베른트 하이다
란돌프 휴고
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20130016264A publication Critical patent/KR20130016264A/ko
Application granted granted Critical
Publication of KR101850562B1 publication Critical patent/KR101850562B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/12—Alkadienes
    • C07C11/16—Alkadienes with four carbon atoms
    • C07C11/167—1, 3-Butadiene

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020127026467A 2010-03-11 2011-03-08 원료 1,3-부타디엔으로부터 순수한 1,3-부타디엔의 증류 추출을 위한 방법 및 장치 Active KR101850562B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010011014.0 2010-03-11
DE102010011014A DE102010011014A1 (de) 2010-03-11 2010-03-11 Verfahren und Vorrichtung zur destillativen Gewinnung von Rein-1,3-Butadien aus Roh-1,3-Butadien
PCT/EP2011/053473 WO2011110562A1 (de) 2010-03-11 2011-03-08 Verfahren und vorrichtung zur destillativen gewinnung von rein-1,3-butadien aus roh-1,3-butadien

Publications (2)

Publication Number Publication Date
KR20130016264A KR20130016264A (ko) 2013-02-14
KR101850562B1 true KR101850562B1 (ko) 2018-04-19

Family

ID=43806920

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127026467A Active KR101850562B1 (ko) 2010-03-11 2011-03-08 원료 1,3-부타디엔으로부터 순수한 1,3-부타디엔의 증류 추출을 위한 방법 및 장치

Country Status (8)

Country Link
EP (1) EP2545019B1 (https=)
JP (1) JP5758922B2 (https=)
KR (1) KR101850562B1 (https=)
CN (1) CN102781892B (https=)
DE (1) DE102010011014A1 (https=)
PL (1) PL2545019T3 (https=)
TW (1) TWI500601B (https=)
WO (1) WO2011110562A1 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103958647B (zh) * 2011-12-05 2017-07-21 巴斯夫欧洲公司 提供气态经纯化的c4粗馏分作为进料流用于使用选择性溶剂的萃取蒸馏工艺的方法
US8642828B2 (en) 2012-01-03 2014-02-04 Basf Se Process for purifying a recycle stream from a 1,3-butadiene processing plant
KR102043048B1 (ko) * 2012-01-03 2019-11-11 바스프 에스이 1,3-부타디엔 공정 설비로부터 나오는 재순환 스트림의 정제 방법
US8766029B2 (en) 2012-01-11 2014-07-01 Basf Se Process for providing a vaporous purified crude C4 cut as a feed steam for an extractive distillation with a selective solvent
TR201818750T4 (tr) * 2012-09-20 2019-01-21 Lummus Technology Inc Butadien özütlemesine yönelik ön soğurucu.
CN102942437A (zh) * 2012-11-22 2013-02-27 万达集团股份有限公司 Nmp法丁二烯一段抽提方法
WO2016005359A1 (de) * 2014-07-08 2016-01-14 Basf Se Kolonne mit trennwirksamen einbauten zur auftrennung eines gemisches von kohlenwasserstoffen und/oder kohlenwasserstoffderivaten durch extraktivdestillation mit einem selektiven lösungsmittel
US11034631B2 (en) 2017-01-25 2021-06-15 Basf Se Method for obtaining pure 1,3-butadiene
WO2018166961A1 (de) 2017-03-13 2018-09-20 Basf Se Vereinfachtes verfahren zur gewinnung von rein-1,3-butadien
EP3997053B1 (en) * 2019-09-13 2025-10-01 SABIC Global Technologies, B.V. Integrated systems and methods for producing 1,3-butadiene via extractive distillation, distillation, and/or selective hydrogenation

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4277311A (en) 1976-06-14 1981-07-07 Bethlehem Steel Corporation Apparatus for distillation
FR2440984A1 (fr) * 1978-11-10 1980-06-06 Inst Francais Du Petrole Procede de traitement d'une coupe d'hydrocarbures c4 en vue de la recuperation du butadiene
US4277313A (en) * 1980-03-27 1981-07-07 El Paso Products Company Recovery of 1,3-butadiene
JPS5754129A (ja) * 1980-09-18 1982-03-31 Japan Synthetic Rubber Co Ltd Butajenmatahaisopurennoseiseihoho
JPS57123123A (en) * 1981-01-23 1982-07-31 Nippon Oil Co Ltd Preparation of high purity butadiene
DE19818810A1 (de) * 1998-04-27 1999-10-28 Basf Ag Verfahren zum Trennen eines C4-Kohlenwasserstoffgemisches
DE10056841A1 (de) * 2000-11-16 2002-05-23 Basf Ag Verfahren und Vorrichtung zur destillativen Gewinnung von 1,3-Reinbutadien aus 1,3-Rohbutadien
DE10105660A1 (de) * 2001-02-08 2002-08-14 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien durch Extraktivdestillation aus einem C4-Schnitt
DE10233621A1 (de) * 2002-07-24 2004-02-19 Basf Ag Verfahren zur Aufarbeitung von Roh-1,3-Butadien
DE10322655A1 (de) 2003-05-20 2004-12-09 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien aus einem C4-Schnitt
CN101172929B (zh) 2006-10-31 2010-05-19 中国石油化工股份有限公司 Nmp法丁二烯一段抽提方法
KR101111015B1 (ko) * 2008-07-17 2012-04-04 에스케이이노베이션 주식회사 아세틸렌 전환공정을 이용한 ｃ4 유분으로부터1,3-부타디엔을 분리하는 방법
CN101665399B (zh) * 2008-09-05 2012-07-25 中国石油化工股份有限公司 丁二烯生产方法

Also Published As

Publication number Publication date
EP2545019A1 (de) 2013-01-16
JP2013522175A (ja) 2013-06-13
CN102781892B (zh) 2016-05-04
TW201139368A (en) 2011-11-16
PL2545019T3 (pl) 2014-08-29
KR20130016264A (ko) 2013-02-14
EP2545019B1 (de) 2014-03-05
TWI500601B (zh) 2015-09-21
WO2011110562A1 (de) 2011-09-15
JP5758922B2 (ja) 2015-08-05
CN102781892A (zh) 2012-11-14
DE102010011014A1 (de) 2011-09-15

Similar Documents

Publication Publication Date Title
KR101850562B1 (ko) 원료 1,3-부타디엔으로부터 순수한 1,3-부타디엔의 증류 추출을 위한 방법 및 장치
US4277313A (en) Recovery of 1,3-butadiene
MXPA02010906A (es) Metodo y dispositivo para tratar una fraccion de c4.
JP2013522175A5 (https=)
EP2897928B1 (en) Butadiene extraction pre-absorber
KR100203555B1 (ko) 추출 증류에 의해 부텐과 부탄을 분리하는 방법
US3317627A (en) High purity alkadienes by extractive distillation
KR101084866B1 (ko) 조 ｃ4 분획의 분리방법
US7393992B2 (en) Method for working up crude 1,3-butadiene
KR100198897B1 (ko) 추출 증류에 의한 부탄 및 부텐의 분리 방법
CN110198923B (zh) 获得纯1,3-丁二烯的方法
EP3010874B1 (en) Co-extraction systems for separation and purification of butadiene and isoprene
KR102597623B1 (ko) 순수 1,3-부타디엔을 얻기 위한 단순화된 방법
JPH0413330B2 (https=)
CA1042834A (en) Solvent for the separation of diolefins from mixtures containing the same
JPH0641428B2 (ja) 抽出蒸留によりｃ４−炭化水素混合物を分離する方法
US20160207853A1 (en) Extractive distillation process

Legal Events

Date Code Title Description
E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

FPAY Annual fee payment

Payment date: 20210330

Year of fee payment: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20220325

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

U11 Full renewal or maintenance fee paid

Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-OTH-PR1001 (AS PROVIDED BY THE NATIONAL OFFICE)

Year of fee payment: 9