KR101682225B1 - A method for refining horse oil and a cosmetic composition comprising the refined horse oil - Google Patents

Abstract

The present invention relates to a method for refining a horse oil and a cosmetic composition containing the horse oil. The present invention relates to a method for refining a horse oil which is effective for deodorizing the odor of a horse oil extract by using citrus fruit juice in refining the horse oil, A cosmetic composition can be provided.

Description

[0001] The present invention relates to a cosmetic composition containing a refined horse oil and a cosmetic composition,

The present invention relates to a method for refining a horse oil and a cosmetic composition containing the horse oil. The present invention relates to a method for refining a horse oil which is effective for deodorizing the odor of a horse oil extract by using citrus fruit juice in refining the horse oil, A cosmetic composition can be provided.

Further, the present invention can omit the step of removing the material used for deodorizing the odor of the hemp oil, and further prevent the odor of the hemp oil from being deodorized at a high temperature, It is possible to produce the cosmetic composition by a simple process so that the production cost can be reduced.

The cultivation area of citrus fruits in Jeju was increased from 189% to 18,802 hectares in 1980 to 14,80 hectares in 1996, and the resulting citrus production increased by 256% from 187,407 to 479,980 tons. The cultivation area and yield of these citrus fruits It is increasing gradually. With the increase in production of these citrus fruits, a variety of citrus processed foods are being developed to suit consumers' preferences. However, to date, most citrus processed foods have been supplied to consumers using ripe citrus fruits (hereinafter referred to as "citrus fruit juice").

On the other hand, it conducts annual insemination every year to obtain a high quality reproduction ripe citrus fruit. The enemy is to remove some citrus peel from the citrus tree branches to obtain a stable fruiting of citrus, prevent the avalanche and to obtain the finest citrus fruit ripe fruit. The citrus fruit which is thus removed is suitable for use as a product or a processing food Do not dispose of it.

As the cultivation area of citrus grows gradually, the yield of citrus unripe is increasing. Studies on the utilization of the uncooked citrus fruits that are disposed of in this way are very limited.

On the other hand, Mayu is an oil of horses and it is said to be beneficial for the prevention of fine lines and aging due to abundant vitamin E, and has been used for skin aesthetics for a long time in folk remedies. Mayu is known to be very effective for burning, which is effective for burning and relieving inflammation. It is a major component of sebum that protects human skin. It contains a large amount of palmitoleic acid, which has strong antimicrobial action. It is known that a protective film is formed to give a high moisturizing effect to the skin. It also contains a large amount of Vitamin E, which makes the blood circulating. It is also used in beauty cosmetics because oil itself can act as a good cosmetic product. In addition, Maou is the closest component to sebum, and because it has almost the same composition ratio, fatty acid composition and moisture balance, it has high affinity with human skin and contains about 60% or more of unsaturated fatty acid. It is known as a substance.

However, due to the unique odor of horse radish extracted from fat, which is a by-product of horse, deodorization is required for use as a cosmetic composition. In the existing Korean Patent Registration No. 10-0912706, active clay and activated carbon are used but they are used at high temperature to cause problems such as oxidization and compositional change of horseradish, and further, acid clay or activated carbon used for deodorization There is a problem in that a production cost is increased due to the necessity of a step of removing the catalyst.

In addition, in 2014, Jeju region was designated as a special zone for horse industry, and has been developing, developing and securing many horse related industries. Mayu, which is a by-product of horse, is made into pure oil form through refining process and goes through defection and deoxidation in refining process. Generally, phosphoric acid and hydrochloric acid are mainly used for the deodorization process, and caustic soda is used for treatment and neutralization of acid residues in the deoxidation process. However, since the process of removing them is essential, the production cost is also increased There is a problem that skin irritation can be caused by acid clay, activated charcoal, phosphoric acid, hydrochloric acid, caustic soda which can not be removed, and there is still a limit to remove the unpleasant smell of Maeyu.

The present inventors have studied a method and a material capable of eliminating the odor of hemp, and have found that the process is simple, without using hydrochloric acid and phosphoric acid, and is effective for purifying the odor of hemp oil, To provide a cosmetic composition.

Another problem to be solved by the present invention is to eliminate the step of removing the material used for deodorizing the odor of maize and further to prevent the oxidation and composition change of the bean oil without deodorizing the odor of the maize at a high temperature And a cosmetic composition containing the hemp purified by the method.

Another object to be solved by the present invention is to provide a method for purifying horse meat using by-products and a cosmetic composition containing the horse oil purified by the method.

The present invention can include the following means in order to solve the above-described problems.

The method for refining horse oil according to the present invention comprises: a first step of extracting a first step oil extract from ground horse meat, crushing horse meat fat and refined water; Citrus immature and citrus fruit forming an extract and extract forming step; Mixing the primary milk extract and the citrus fruit with an extract to form a mixture; And a contaminant removal step of removing contaminants from the mixture.

In the primary milk extraction step, the crude horse meat fat and the purified water are mixed at a weight ratio of 1: 1 to 1.5, and the extract is extracted at 90 to 130 ° C.

Meanwhile, in the citrus immature and extract-forming steps, the citrus immature fruit and the extract have a pH of 2.5 to 3.5.

According to another embodiment of the present invention, the citrus immature and extract-forming step comprises: a precipitation step of forming citrus immature fruit juice by precipitating the juice in an immature citrus fruit; Wherein the citrus fruit juice filtration step further comprises filtering the citrus fruit juice obtained in the precipitation step to form a citrus fruit undiluted extract and an extract.

Wherein the citrus immature and extract forming step further comprises a pH control step of further mixing a citrus extract extracted from a citrus fruit to adjust the pH of the citrus fruit and the extract, It is preferable that the line extract is derived from one or more selected from lemon, citrus orange, orange, avocado, lime, grapefruit and their immature.

In the mixing step, the primary milk extract and the citrus fruit extract are mixed at a weight ratio of 1: 0.001 to 0.3.

Meanwhile, the mixing step may include a reaction step of mixing the extract of the first order milk oil with the extract of the citrus fruit and the extract and allowing the reaction to proceed for 6 to 36 hours; And further comprising a hot water bath step at 50 to 80 ° C after the reaction step.

The method further comprises the step of removing impurities and crushing the paraffin using a microfilter after the step of removing the impurities.

According to another embodiment of the present invention, the method for the preparation of a hair further comprises a stabilization step for stabilizing the purified tablet, the stabilizing step comprising: a cooling step for cooling the purified tablet to form a cooled tablet tablet; A cold-aging step of firstly aging the cooled purified tablet; And aging at room temperature for secondary aging after the refrigeration aging step.

The purified tablet according to another embodiment of the present invention is prepared by the above method.

The cosmetic composition according to another embodiment of the present invention contains the above purified tablet.

According to another embodiment of the present invention, refined hemp oil is formed so as to suppress the smell of hemp by containing immature fruit and extract.

The cosmetic composition according to still another embodiment of the present invention contains citrus unripe, extract, and purified horse oil.

The present invention can provide a method for purifying the muscle oil which is effective for immersing the citrus fruit and extracts and deodorizing the odor of the horse oil, and a cosmetic composition containing the purified horse oil and the purified horse oil.

Further, the present invention can omit the step of removing the material used for deodorizing the odor of the hemp oil, and further prevent the odor of the hemp oil from being deodorized at a high temperature, It is possible to produce the cosmetic composition by a simple process so that the production cost can be reduced.

In addition, there is an effect of providing purified tablet and cosmetic composition which has a high preference and can be absorbed well on the skin.

Advantages and features of the present invention and methods of achieving them will become apparent with reference to the embodiments described in detail below. The present invention may, however, be embodied in many different forms and should not be construed as being limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete, and will fully convey the scope of the invention to those skilled in the art. Is provided to fully convey the scope of the invention to those skilled in the art, and the invention is only defined by the scope of the claims.

Unless defined otherwise, all terms (including technical and scientific terms) used herein may be used in a sense commonly understood by one of ordinary skill in the art to which this invention belongs. And commonly used predefined terms are not ideally or excessively interpreted unless expressly defined otherwise. In the meantime, 'refined beverage' referred to in the present invention can be interpreted to include not only refined beef by the method of the present invention but also refined beef by a generally known method.

Hereinafter, the present invention will be described in detail.

The method for preparing a horsebean oil according to the present invention includes a step of extracting a primary tea oil, an immature citrus fruit and an extract forming step, a mixing step, and a contaminant removal step.

Preferably, the ground horse meat fat and meat juice are mixed at a weight ratio of 1: 1 to 1.5, and the mixture is heated at 90 to 130 ° C in a heating furnace. And extracting the liquefied primary tea oil extract.

The citrus immature and extract forming step is a step of forming an extract of Citrus unripe and citrus fruit in the Citrus unripe lotus, and it is found that the citrus citrus fruit of the present invention contains about 4 times as many polyphenols as the ripe lotus, It has citric acid and vitamin C and is known to have high acidity. In particular, it was found that the effective amount of the functional substance which is more effective than Hesperidin and Naringin, which has been reported in the Wonju citron mite area, which is effective from July to September, has a great effect on the whitening activity and the inhibition of fatty liver, In particular, it is known that rats administered with the immature and extract have excellent effects in improving blood lipids and prevention of fatty liver.

Meanwhile, it is preferable that the immature fruit of the citrus fruit and the extract are generally used in the period from July to September, and it is preferable that the pH is set to 2.5 to 3.5 in order to facilitate the removal of impurities at a later time. The citrus immature and extract-forming steps may further comprise a precipitation step, a citrus immature fruit filtration step and a pH control step.

The precipitation step is a step in which citrus fruit juice is squeezed to precipitate the fiber to precipitate citrus fruit juice. The precipitation of the fiber while keeping the citrus fruit juice in the refrigerator for 6 hours or more can remove the contaminants more easily, Do.

In the citrus fruit immature fruit filtration step, the citrus fruit juice formed in the precipitation step is filtered using a nonwoven fabric or the like to form an immature fruit and extract.

The pH controlling step may further include mixing the citrus fruit extract extracted from citrus fruit to control the pH of the citrus fruit and the extract when the citrus fruit and the extract have an acidity of 2.5 to 3.5. Preferably, the citrus-based extract is derived from one or more selected from among lemon, citrus orange, orange, avocado, lime, grapefruit, and their immature, and there is no need to remove the pH adjuster again later Specific components of the citrus series are attached to the ground Maula particles to further suppress the odor peculiar to the Maule and to give a refreshing feeling, which is suitable for increasing the feeling of use.

The mixing step is a step of mixing the first-order milk extract and the citrus fruit with the extract to form a mixture. The components of the citrus fruit and the extract can suppress the odor peculiar to the tea and improve refreshing feeling, thereby enhancing the feeling of use.

Meanwhile, in the mixing step, it is preferred that the extract of the first order milk oil and the extract of the citrus fruit are mixed at a weight ratio of 1: 0.001-0.3. In the mixing step, the reaction step and the bathing step May be further included.

The reaction step is a step for increasing the degree of deodorization by mixing the extract of the first order milk oil with the citrus fruit and extract, The reaction is carried out for 6 to 36 hours.

The soaking step is a step of warming the mixture at 50 to 80 ° C after the reaction step, thereby lumping the protein or phospholipid, thereby facilitating the contaminant removal step at a later stage. In addition, it is preferable to keep the water-soluble phase at 50 to 80 ° C so that citric acid immature fruit and citric acid vitamin C contained in the extract are not deformed as much as possible.

The contaminant removing step is a step of removing contaminants from the mixture formed in the mixing step through a sieve or the like.

According to another embodiment of the present invention, in the method for cleaning the surface, after removing the impurities, the impurities remaining in the secondary are removed using a microfilter that can be purchased commercially, and the fine oil is finely pulverized It is possible to further include an effect of increasing the absorbency of the skin and an impurity removing step of increasing the purity.

On the other hand, there is a method of finely pulverizing the refined marrow and increasing the purity by repeatedly finishing the purified refined beef two to five times so as to finely grind the refined beef and increase the purity. And should be construed as falling within the scope of the invention.

Meanwhile, according to another embodiment of the present invention, the method for preparing a muscle oil may further comprise a stabilization step for stabilizing the purified muscle oil. The stabilizing step may include a cooling step, a refrigeration aging step, and a room temperature aging step.

The cooling step is a step of cooling to -20 캜 or lower for about 24 hours, thereby preventing the fragrance from flying and preventing the separation of oil from being caused.

In the refrigeration-aging step, the cooled tableted milk is firstly aged for about 5 days in a refrigerated state at 5 ° C or less. When the refrigerated aged step is not performed, the shape of the sol is closer to liquid than gel at room temperature And is not easy to use.

At the room temperature aging step, after the refrigeration aging step, it is aged at room temperature for 15 days to gel the purified tablet, thereby facilitating handling and use.

The present invention does not use a material such as acidic clay or activated carbon to deodorize the odor of horse radish by the method described above, and can eliminate the step of removing such a material. Furthermore, since the odor of horse radish is not deodorized at high temperature, It is possible to prevent the oxidation and the component change of the catalyst. Furthermore, it is possible to provide a cosmetic composition capable of deodorizing a specific odor of a horse radish extract by a simple process in producing a cosmetic composition containing a horse radish extract.

The purified hemp oil prepared by the above method can be used as a raw material for foods, medicines and cosmetics because it can catch the unique odor of hemp.

In addition, when the citrus fruit is immature and the extract contains the extract, the smell of the maruyu can be suppressed, and it can be used as a composition of the cosmetic composition containing immature citrus fruit, extract and purified tea.

The cosmetic composition of the present invention may contain at least one active ingredient which exhibits the same or similar function in addition to the citrus unripe, extract and purified tablet.

Cosmetics made from the cosmetic composition containing the extract of the present invention as an active ingredient can be prepared in the form of a general emulsified formulation and a solubilized formulation. Cosmetics of emulsified form include nutrition lotion, cream, essence, etc., and cosmetics of solubilized form have softening longevity. In addition to cosmetics containing the extract of the present invention, it can also be prepared in the form of an adjuvant which can be applied topically or systemically, which is conventionally used in the field of dermatology by containing a dermatologically acceptable medium or base.

Suitable cosmetic formulations include, for example, solutions, gels, solid or kneaded anhydrous products, emulsions obtained by dispersing the oil phase in water, suspensions, microemulsions, microcapsules, microgranules or ionic (liposomes) In the form of a foliar dispersant, in the form of a cream, a skin, a lotion, a powder, an ointment, a spray or a conceal stick. It can also be prepared in the form of a foam or an aerosol composition further containing a compressed propellant.

The cosmetic composition of the present invention may further contain at least one selected from the group consisting of fatty substances, organic solvents, solubilizers, thickeners and gelling agents, softening agents, antioxidants, suspending agents, stabilizers, foaming agents, perfumes, Or any other conventionally used in cosmetics such as nonionic emulsifiers, fillers, sequestering and chelating agents, preservatives, vitamins, barrier agents, wetting agents, essential oils, dyes, pigments, hydrophilic or lipophilic active agents, ≪ RTI ID = 0.0 > cosmetics < / RTI > such as botanical ingredients, or adjuvants conventionally used in the field of dermatology. And, the above ingredients can be introduced in amounts commonly used in the field of dermatology.

Examples of products to which the cosmetic composition of the present invention can be added include cosmetics such as astringent lotion, softening longevity lotion, nutrition lotion, various creams, essences, packs, foundation and the like, cleansing, cleanser, soap, .

As a specific formulation of the cosmetic composition of the present invention, there may be mentioned a skin lotion, a skin softener, a skin toner, an astringent, a lotion, a milk lotion, a moisturizing lotion, a nutrition lotion, a massage cream, And includes formulations such as soap, shampoo, cleansing foam, cleansing lotion, cleansing cream, body lotion, body cleanser, milky lotion, press powder, loose powder, eye shadow and the like.

Hereinafter, preferred embodiments and experimental examples are provided to facilitate understanding of the present invention. However, the following examples and experimental examples are provided only for the purpose of easier understanding of the present invention, and the present invention is not limited by the examples.

[ Example  One] Refined Mayu  Produce

1 kg of horse meat and fat were crushed and compressed, and 1 kg of water was mixed and primary muscle oil was extracted with steam at 100 ° C.

The jujube juice was squeezed out on July 21, washed with juice, stored in refrigerator for more than 6 hours to precipitate the fiber, and the juice was filtered using nonwoven fabric and the liquid component was stored at 8 ° C or less.

The primary extracts were mixed with chilled and stored immature fruit juice at a ratio of 1: 0.3, reacted for 24 hours, and liquified at 60 ℃.

After removing the contaminants through a screen, they were cooled at -25 ° C for 24 hours, refrigerated at 4 ° C for 5 days, and aged at room temperature for 15 days to prepare citrus fruit juice and extract-containing tablets.

[Example 2] Refined Mayu  Produce

1 kg of horse meat and fat were crushed and compressed, and 1 kg of water was mixed and primary muscle oil was extracted with steam at 100 ° C.

The jujube juice was squeezed out on July 21, washed with juice, stored in refrigerator for more than 6 hours to precipitate the fiber, and the juice was filtered using nonwoven fabric and the liquid component was stored at 8 ° C or less.

The primary extracts were mixed with chilled and stored immature fruit juice at a ratio of 1: 0.3, reacted for 24 hours, and liquified at 60 ℃.

The contaminants were removed through a filter net and put into a microfilter to remove second residual impurities and foreign matter.

It was cooled at -25 ℃ for 24 hours, then cooled at 4 ℃ for 5 days, and then aged at room temperature for 15 days to prepare purified citrus fruit juice and citrus fruit juice containing extract.

[ Experimental Example  1] Deodorizing effect sensory test

Using the above-mentioned Examples 1 and 2 and purified tablet (J) sold in the market as a comparative example, it was determined whether or not the odor of hemp was deodorized and the degree of stickiness when it was applied to the skin and skin, The results of the sensory evaluation were shown in Table 1 below.

Example 1 Example 2 Comparative Example Degree of deodorization 4.5 4.6 1.2 Likelihood 4.4 4.7 1.3 Degree of stickiness 2.6 4.2 2.1

[Review]

As can be seen from the above Table 1, the degree of deodorization and preference specific to Maey were high in Examples 1 and 2 according to the present invention. However, the degree of tackiness in the skin patch test was not as good as in Experimental Example 1 compared with the Comparative Example, but in Example 2 using the microfilter, the degree of tackiness was significantly better than that of Comparative Example. This is presumed to be the result of finely pulverizing the purified tablet by the microfilter and penetrating the skin well.

Claims (14)

A primary tea oil extraction step of grinding horse meat, mixing the ground horse meat with purified water, and then extracting a primary tea oil extract;
Citrus immature and citrus fruit forming an extract and extract forming step;
Mixing the primary milk extract and the citrus fruit with an extract to form a mixture;
And removing contaminants from the mixture to form a purified tablet. 2. The method according to claim 1,
Wherein the crude horse meat fat and the purified water are mixed at a weight ratio of 1: 1 to 1.5, and the first-order milk oil extract is extracted at 90 to 130 ° C. The method according to claim 1,
Wherein the citrus juicy extract and the extract have a pH of 2.5 to 3.5. [2] The method of claim 1,
A precipitation step of squeezing the juice from the citrus fruit premix to precipitate the fiber to form citrus juice;
Wherein the citrus fruit juice filtration step further comprises filtering the citrus fruit juice obtained in the precipitation step to filtrate the citrus fruit juice and filtering the citrus fruit juice. [5] The method of claim 3,
Further comprising a pH controlling step of further mixing the citrus extract extracted from fruits of the citrus series to control the pH of the citrus fruit and the extract. 6. The method according to claim 5, wherein the citrus-
Lemon, citrus fruit, orange, avocado, lime, grapefruit, and their immature seeds. 2. The method of claim 1,
Wherein the crude oil extract and the citrus fruit are mixed at a weight ratio of 1: 0.001 to 0.3. 8. The method of claim 7,
A reaction step of mixing the extract of the first order tea oil with the extract of the citrus fruit and the extract and allowing the reaction to proceed for 6 to 36 hours;
Further comprising a hot water bath step at 50-80 < 0 > C after said reaction step. The method according to claim 1,
Further comprising the step of removing impurities and crushing the paraffin using a microfilter after passing through the impurity removing step. The method according to claim 1,
Further comprising a stabilization step to stabilize the purified tablet,
Wherein the stabilizing step comprises:
Cooling the purified tablets to form cooled tablet tablets;
A cold-aging step of firstly aging the cooled purified tablet;
And aging at room temperature for the second aging after the refrigeration-aging step. 10. A purified tablet prepared by the method according to any one of claims 1 to 10. 12. The cosmetic composition according to claim 11, wherein the composition comprises the tablet of the present invention. It contains refined citrus fruits and extracts, and is formulated to inhibit the odor of maruyu. delete