KR101512375B1 - 지방산 및 지방산 에스테르의 제조 방법 - Google Patents

지방산 및 지방산 에스테르의 제조 방법 Download PDF

Info

Publication number
KR101512375B1
KR101512375B1 KR1020107007538A KR20107007538A KR101512375B1 KR 101512375 B1 KR101512375 B1 KR 101512375B1 KR 1020107007538 A KR1020107007538 A KR 1020107007538A KR 20107007538 A KR20107007538 A KR 20107007538A KR 101512375 B1 KR101512375 B1 KR 101512375B1
Authority
KR
South Korea
Prior art keywords
fatty acid
added
phase
acid
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020107007538A
Other languages
English (en)
Korean (ko)
Other versions
KR20100074172A (ko
Inventor
오씨 파스티넨
시모 라아크소
산나 호크카넨
마르자타 바흐바셀카
Original Assignee
알토 유니버시티 파운데이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 알토 유니버시티 파운데이션 filed Critical 알토 유니버시티 파운데이션
Publication of KR20100074172A publication Critical patent/KR20100074172A/ko
Application granted granted Critical
Publication of KR101512375B1 publication Critical patent/KR101512375B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/02—Recovery of fats, fatty oils or fatty acids from waste materials from soap stock
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C11C1/025—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by saponification and release of fatty acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/30—Recovery of soap, e.g. from spent solutions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020107007538A 2007-09-07 2008-09-05 지방산 및 지방산 에스테르의 제조 방법 Expired - Fee Related KR101512375B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US99301407P 2007-09-07 2007-09-07
US60/993,014 2007-09-07
FI20075619 2007-09-07
FI20075619A FI20075619L (fi) 2007-09-07 2007-09-07 Rasvahapon ja rasvahappoesterin tuottaminen
PCT/FI2008/050495 WO2009030820A1 (en) 2007-09-07 2008-09-05 Production of fatty acid and fatty acid ester

Publications (2)

Publication Number Publication Date
KR20100074172A KR20100074172A (ko) 2010-07-01
KR101512375B1 true KR101512375B1 (ko) 2015-04-16

Family

ID=38572953

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020107007538A Expired - Fee Related KR101512375B1 (ko) 2007-09-07 2008-09-05 지방산 및 지방산 에스테르의 제조 방법

Country Status (13)

Country Link
EP (1) EP2188356A1 (enExample)
JP (1) JP5620818B2 (enExample)
KR (1) KR101512375B1 (enExample)
CN (1) CN101896590B (enExample)
AP (1) AP2831A (enExample)
AU (1) AU2008294648B2 (enExample)
BR (1) BRPI0816733A2 (enExample)
CA (1) CA2698642A1 (enExample)
EA (1) EA020085B1 (enExample)
FI (1) FI20075619L (enExample)
MX (1) MX2010002615A (enExample)
MY (1) MY152941A (enExample)
WO (1) WO2009030820A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102604851B1 (ko) * 2015-08-31 2023-11-21 프라운호퍼 게젤샤프트 쭈르 푀르데룽 데어 안겐반텐 포르슝 에. 베. 글리세라이드를 함유하는 윤활 혼합물
CN106866370B (zh) * 2016-12-31 2020-10-30 衡阳市晨丰生物科技有限公司 一种除去粗甘油中脂类的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006088123A1 (ja) * 2005-02-21 2006-08-24 Kagoshima University バイオディーゼル燃料の精製方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2327569A (en) * 1941-03-29 1943-08-24 Refining Inc Process of refining
JP3028282B2 (ja) * 1996-02-28 2000-04-04 有限会社染谷商店 廃食用油を原資源として精製する重油バーナー用燃料および廃食用油を原資源としての再利用方法
US6129945A (en) * 1998-12-10 2000-10-10 Michael E. George Methods to reduce free fatty acids and cholesterol in anhydrous animal fat
US6855838B2 (en) * 2002-01-09 2005-02-15 The United States Of America, As Represented By The Secretary Of Agriculture Lipid rich compositions, production of lipid rich compositions, production of fatty acid alkyl esters from heterogeneous lipid mixtures
CA2436650A1 (en) * 2003-08-06 2005-02-06 Naturia Inc. Conjugated linolenic acid (clnatm) compositions: synthesis, purification and uses
ATE362506T1 (de) * 2004-09-21 2007-06-15 Linde Ag Verfahren zur gewinnung von tallöl oder tallölbrennstoff
JP2007176973A (ja) * 2005-12-27 2007-07-12 Lion Corp 軽油代替燃料用の脂肪酸低級アルキルエステルの製造方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006088123A1 (ja) * 2005-02-21 2006-08-24 Kagoshima University バイオディーゼル燃料の精製方法

Also Published As

Publication number Publication date
CN101896590B (zh) 2014-07-30
MY152941A (en) 2014-12-15
EA020085B1 (ru) 2014-08-29
KR20100074172A (ko) 2010-07-01
AU2008294648A8 (en) 2010-04-22
EA201070258A1 (ru) 2010-10-29
AP2010005210A0 (en) 2010-04-30
FI20075619A7 (fi) 2009-03-08
EP2188356A1 (en) 2010-05-26
AU2008294648B2 (en) 2013-09-12
JP2010538140A (ja) 2010-12-09
BRPI0816733A2 (pt) 2017-06-06
AU2008294648A1 (en) 2009-03-12
CN101896590A (zh) 2010-11-24
CA2698642A1 (en) 2009-03-12
FI20075619L (fi) 2009-03-08
AP2831A (en) 2014-01-31
JP5620818B2 (ja) 2014-11-05
WO2009030820A1 (en) 2009-03-12
FI20075619A0 (fi) 2007-09-07
MX2010002615A (es) 2010-07-06

Similar Documents

Publication Publication Date Title
CN102232063B (zh) 同时酯化和醇解/水解具有包含磷脂和纤维素与肽类内容物的含油取代物的物质制备生物柴油、纤维素糖和肽
EP2114851B1 (en) Process for separating saturated and unsaturated fatty acids
KR102327852B1 (ko) 지방을 이용한 지방산알킬에스테르의 제조방법
JP2002265986A (ja) 脂肪酸アルキルエステル及びグリセリンの製造方法
US20120245371A1 (en) Process for the purification of crude alkaline glycerol
WO2009039144A1 (en) Processes for the esterification of free fatty acids and the production of biodiesel
KR101512375B1 (ko) 지방산 및 지방산 에스테르의 제조 방법
CN101531913A (zh) 一种生物柴油的制备方法
CN100500809C (zh) 废弃动植物油脂制备生物柴油的预处理生产工艺
WO2008002776A1 (en) Separating saturated and unsaturated fatty acids for producing cold-tolorant biodiesel fuel
CN100408543C (zh) 一种联产脂肪酸酯、甘油和植物粗蛋白的工艺
US8178706B2 (en) Production of fatty acid and fatty acid ester
KR101022133B1 (ko) 함초유를 이용한 바이오디젤의 제조방법
KR100790298B1 (ko) 고순도 지방산 알킬에스테르의 제조방법 및 이로부터 제조된 지방산 알킬에스테르
HK1146733B (en) Production of fatty acid and fatty acid ester
HK1146733A1 (en) Production of fatty acid and fatty acid ester
CN112457189A (zh) 一种棕榈油脂肪酸乙酯的制备方法
JP5637484B2 (ja) 高級脂肪酸アルキルエステル製造用原料油脂及び高級脂肪酸アルキルエステルの製造方法
JP5730571B2 (ja) アルカリ土類金属石けんを沈殿させる工程を含む、アルコール、石けんおよび／または脂肪酸を含有する出発原料からの脂質の発酵方法
CN101665746B (zh) 以葡萄籽油为原料制备高含量亚油酸乙酯的方法
KR101351675B1 (ko) 히드록실화 오일의 트랜스에스테르화를 위한 방법
Sathish et al. Optimization of Process Parameters to Enhance the Yield of Biodiesel by Using Heterogeneous Catalyst
RO128632B1 (ro) Procedeu de obţinere a unui biocombustibil de tip diesel din uleiuri vegetale reutilizabile () şi/sau grăsimi animale

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20180410

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20180410

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000