KR101372767B1 - 폴리트리메틸렌 에테르 글리콜의 제조 - Google Patents
폴리트리메틸렌 에테르 글리콜의 제조 Download PDFInfo
- Publication number
- KR101372767B1 KR101372767B1 KR1020087020232A KR20087020232A KR101372767B1 KR 101372767 B1 KR101372767 B1 KR 101372767B1 KR 1020087020232 A KR1020087020232 A KR 1020087020232A KR 20087020232 A KR20087020232 A KR 20087020232A KR 101372767 B1 KR101372767 B1 KR 101372767B1
- Authority
- KR
- South Korea
- Prior art keywords
- acid
- group
- polytrimethylene ether
- ether glycol
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/46—Post-polymerisation treatment, e.g. recovery, purification, drying
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/336,004 US7164046B1 (en) | 2006-01-20 | 2006-01-20 | Manufacture of polytrimethylene ether glycol |
| US11/336,004 | 2006-01-20 | ||
| US11/599,861 | 2006-11-15 | ||
| US11/599,861 US7388115B2 (en) | 2006-01-20 | 2006-11-15 | Manufacture of polytrimethylene ether glycol |
| PCT/US2007/001374 WO2007084637A1 (en) | 2006-01-20 | 2007-01-19 | Manufacture of polytrimethylene ether glycol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20080089491A KR20080089491A (ko) | 2008-10-06 |
| KR101372767B1 true KR101372767B1 (ko) | 2014-03-10 |
Family
ID=38043013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020087020232A Active KR101372767B1 (ko) | 2006-01-20 | 2007-01-19 | 폴리트리메틸렌 에테르 글리콜의 제조 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US7388115B2 (https=) |
| EP (1) | EP1973962B1 (https=) |
| JP (1) | JP4976422B2 (https=) |
| KR (1) | KR101372767B1 (https=) |
| AU (1) | AU2007207523A1 (https=) |
| BR (1) | BRPI0706933A2 (https=) |
| CA (1) | CA2635006A1 (https=) |
| DE (1) | DE602007014179D1 (https=) |
| TW (1) | TWI419910B (https=) |
| WO (1) | WO2007084637A1 (https=) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7714174B2 (en) * | 2007-03-27 | 2010-05-11 | E. I. Du Pont De Nemours And Company | Lower-color polytrimethylene ether glycol using hydride compounds |
| US8776391B1 (en) | 2007-04-13 | 2014-07-15 | Align Technology, Inc. | System for post-processing orthodontic appliance molds |
| US7728175B1 (en) * | 2008-12-23 | 2010-06-01 | E. I. Du Pont De Nemours And Company | Linear amine functionalized poly(trimethylene ether) compositions |
| US20110257330A1 (en) | 2008-12-30 | 2011-10-20 | E.I. Du Pont De Nemours And Company | Waterborne coating composition containing polytrimethylene ether diol |
| US8114957B2 (en) * | 2009-02-09 | 2012-02-14 | E. I. Du Pont De Nemours And Company | Process for preparing poly(trimethylene ether) glycol and copolymers thereof |
| US20100204439A1 (en) * | 2009-02-09 | 2010-08-12 | E.I. Du Pont De Nemours And Company | Processes for making poly(trimethylene ether) glycol using organophosphorous compound |
| CN102575002B (zh) * | 2009-09-30 | 2014-10-22 | 纳幕尔杜邦公司 | 具有改善颜色的聚三亚甲基醚二醇或其共聚物以及它们的制备方法 |
| US20110112331A1 (en) * | 2009-11-09 | 2011-05-12 | E.I. Du Pont De Nemours And Company | Method for phase separation of polytrimethylene ether glycol in salt solution |
| US8344098B2 (en) * | 2009-12-21 | 2013-01-01 | E I Du Pont De Nemours And Company | Processes for producing polytrimethylene ether glycol and copolymers thereof |
| KR20230037280A (ko) * | 2021-09-09 | 2023-03-16 | 에스케이케미칼 주식회사 | 폴리트리메틸렌 에테르 글리콜의 제조 방법 및 이에 따라 제조된 폴리트리메틸렌 에테르 글리콜 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004014984A1 (en) | 2002-08-09 | 2004-02-19 | E. I. Du Pont De Nemours And Company | Poly(trimethylene-ethylene ether) glycols |
| US20050272911A1 (en) | 2002-11-22 | 2005-12-08 | Mitsubishi Chemical Corporation | Method for producing polyether polyol |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3926136A1 (de) * | 1989-08-08 | 1991-02-14 | Degussa | Verfahren zur herstellung von 1,3-propandiol |
| DE4132663C2 (de) * | 1991-10-01 | 1993-10-14 | Degussa | Verfahren zum Herstellen von 1,3-Propandiol durch Hydrieren von Hydroxypropionaldehyd |
| DE4138982A1 (de) * | 1991-11-27 | 1993-06-03 | Degussa | Verfahren zur herstellung von 3-hydroxyalkanalen |
| DE4138981A1 (de) * | 1991-11-27 | 1993-06-03 | Degussa | Verfahren zur herstellung von 3-hydroxyalkanalen |
| DE4218282A1 (de) * | 1992-06-03 | 1993-12-09 | Degussa | Verfahren zur Herstellung von 1,3-Propandiol |
| DE4222708A1 (de) * | 1992-07-10 | 1994-01-13 | Degussa | Verfahren zur Herstellung von 1,3-Propandiol |
| US5686276A (en) * | 1995-05-12 | 1997-11-11 | E. I. Du Pont De Nemours And Company | Bioconversion of a fermentable carbon source to 1,3-propanediol by a single microorganism |
| US5633362A (en) * | 1995-05-12 | 1997-05-27 | E. I. Du Pont De Nemours And Company | Production of 1,3-propanediol from glycerol by recombinant bacteria expressing recombinant diol dehydratase |
| DE19703383A1 (de) * | 1997-01-30 | 1998-08-06 | Degussa | Verfahren zur Herstellung von 1,3-Propandiol |
| US5962745A (en) * | 1997-02-14 | 1999-10-05 | E. I. Du Pont De Nemours And Company | Process for preparing 3-hydroxyalkanals |
| KR20010013907A (ko) * | 1997-06-18 | 2001-02-26 | 메리 이. 보울러 | 3-히드록시프로피온알데히드의 수소화에 의한1,3-프로판디올의 제조 방법 |
| US6235948B1 (en) * | 1998-08-18 | 2001-05-22 | E. I. Du Pont De Nemours And Company | Process for the purification of 1,3-propanediol |
| EP1109767B1 (en) * | 1998-09-04 | 2003-03-26 | E.I. Du Pont De Nemours And Company | Two-stage process for the production of 1,3-propanediol by catalytic hydrogenation of 3-hydroxypropanal |
| US6331264B1 (en) * | 1999-03-31 | 2001-12-18 | E. I. Du Pont De Nemours And Company | Low emission polymer compositions |
| US6277289B1 (en) * | 1999-07-01 | 2001-08-21 | E. I. Du Pont De Nemours And Company | Treatment of aqueous aldehyde waste streams |
| US6284930B1 (en) * | 1999-07-30 | 2001-09-04 | E.I. Du Pont De Nemours And Company | Process for the preparation of 3-hydroxypropanal |
| US6342646B1 (en) * | 1999-07-30 | 2002-01-29 | E. I. Du Pont De Nemours And Company | Catalytic hydrogenation of 3-hydroxypropanal to 1,3-propanediol |
| CN1238317C (zh) * | 1999-12-17 | 2006-01-25 | 纳幕尔杜邦公司 | 制备聚三亚甲基醚二醇的连续方法 |
| US6977291B2 (en) * | 1999-12-17 | 2005-12-20 | E.I. Du Pont De Nemours And Company | Production of polytrimethylene ether glycol and copolymers thereof |
| US20050227911A1 (en) * | 2001-09-28 | 2005-10-13 | Solubest Ltd. | Hydrophilic dispersions of nanoparticles of inclusion complexes of macromolecules |
| US6608168B1 (en) * | 2002-08-09 | 2003-08-19 | E. I. Du Pont De Nemours And Company | Polytrimethylene ether esters |
| JP2004182974A (ja) * | 2002-11-22 | 2004-07-02 | Mitsubishi Chemicals Corp | ポリエーテルポリオールの製造方法 |
| US7084311B2 (en) * | 2003-05-06 | 2006-08-01 | E. I. Du Pont De Nemours And Company | Hydrogenation of chemically derived 1,3-propanediol |
| EP1625224B1 (en) * | 2003-05-06 | 2010-07-28 | E.I. Du Pont De Nemours And Company | Purification of biologically-produced 1,3-propanediol |
| WO2004101482A2 (en) * | 2003-05-06 | 2004-11-25 | E.I. Dupont De Nemours And Company | Hydrogenation of biochemically derived 1,3-propanediol |
| US7074969B2 (en) * | 2004-06-18 | 2006-07-11 | E.I. Du Pont De Nemours And Company | Process for preparation of polytrimethylene ether glycols |
| JP2006342344A (ja) * | 2005-05-13 | 2006-12-21 | Mitsubishi Chemicals Corp | ポリエーテルポリオールの製造方法 |
| US7157607B1 (en) * | 2005-08-16 | 2007-01-02 | E. I. Du Pont De Nemours And Company | Manufacture of polytrimethylene ether glycol |
| US7161045B1 (en) * | 2005-08-16 | 2007-01-09 | E. I. Du Pont De Nemours And Company | Process for manufacture of polytrimethylene ether glycol |
-
2006
- 2006-11-15 US US11/599,861 patent/US7388115B2/en not_active Expired - Lifetime
-
2007
- 2007-01-19 DE DE602007014179T patent/DE602007014179D1/de active Active
- 2007-01-19 AU AU2007207523A patent/AU2007207523A1/en not_active Abandoned
- 2007-01-19 TW TW096102111A patent/TWI419910B/zh active
- 2007-01-19 CA CA002635006A patent/CA2635006A1/en not_active Abandoned
- 2007-01-19 EP EP07718321A patent/EP1973962B1/en active Active
- 2007-01-19 KR KR1020087020232A patent/KR101372767B1/ko active Active
- 2007-01-19 WO PCT/US2007/001374 patent/WO2007084637A1/en not_active Ceased
- 2007-01-19 BR BRPI0706933-2A patent/BRPI0706933A2/pt not_active IP Right Cessation
- 2007-01-19 JP JP2008551399A patent/JP4976422B2/ja active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004014984A1 (en) | 2002-08-09 | 2004-02-19 | E. I. Du Pont De Nemours And Company | Poly(trimethylene-ethylene ether) glycols |
| KR20050090977A (ko) * | 2002-08-09 | 2005-09-14 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 폴리(트리메틸렌-에틸렌 에테르) 글리콜 |
| US20050272911A1 (en) | 2002-11-22 | 2005-12-08 | Mitsubishi Chemical Corporation | Method for producing polyether polyol |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2009523894A (ja) | 2009-06-25 |
| JP4976422B2 (ja) | 2012-07-18 |
| AU2007207523A1 (en) | 2007-07-26 |
| BRPI0706933A2 (pt) | 2011-04-19 |
| CA2635006A1 (en) | 2007-07-26 |
| EP1973962A1 (en) | 2008-10-01 |
| US20070173669A1 (en) | 2007-07-26 |
| EP1973962B1 (en) | 2011-04-27 |
| KR20080089491A (ko) | 2008-10-06 |
| US7388115B2 (en) | 2008-06-17 |
| DE602007014179D1 (de) | 2011-06-09 |
| TW200738782A (en) | 2007-10-16 |
| WO2007084637A1 (en) | 2007-07-26 |
| TWI419910B (zh) | 2013-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101372767B1 (ko) | 폴리트리메틸렌 에테르 글리콜의 제조 | |
| US7157607B1 (en) | Manufacture of polytrimethylene ether glycol | |
| CN101389689A (zh) | 聚三亚甲基醚二醇的生产 | |
| KR20070024607A (ko) | 폴리트리메틸렌 에테르 글리콜의 제조 방법 | |
| US7161045B1 (en) | Process for manufacture of polytrimethylene ether glycol | |
| JP2004182974A (ja) | ポリエーテルポリオールの製造方法 | |
| KR19990063374A (ko) | 폴리에테르 폴리올 제조시의 알칼리 성분의 제거 방법 및 그의 재사용법 | |
| KR101929604B1 (ko) | 폴리트라이메틸렌 에테르 글리콜의 제조 방법 | |
| KR20140117590A (ko) | 개선된 가알칸올분해 프로세스 | |
| US20100267994A1 (en) | Processes for preparing polytrimethylene glycol using ion exchange resins | |
| JP3931421B2 (ja) | ポリテトラメチレンエーテルグリコールの製造方法 | |
| JP7742370B2 (ja) | イソブチルビニルエーテルの製造方法及びイソブチルビニルエーテルの精製方法 | |
| KR102814712B1 (ko) | 3-하이드록시프로피온산 알킬 에스터의 제조방법 | |
| JP2006342344A (ja) | ポリエーテルポリオールの製造方法 | |
| KR20120094016A (ko) | 개선된 상 분리 방법을 이용하여 폴리트라이메틸렌 에테르 글리콜을 제조하는 방법 | |
| JP6515645B2 (ja) | ポリブチレンエーテルジ(メタ)アクリレートの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20080819 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20120118 Comment text: Request for Examination of Application |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20130607 Patent event code: PE09021S01D |
|
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20131205 |
|
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 20140304 Patent event code: PR07011E01D |
|
| PR1002 | Payment of registration fee |
Payment date: 20140304 End annual number: 3 Start annual number: 1 |
|
| PG1601 | Publication of registration | ||
| FPAY | Annual fee payment |
Payment date: 20170220 Year of fee payment: 4 |
|
| PR1001 | Payment of annual fee |
Payment date: 20170220 Start annual number: 4 End annual number: 4 |
|
| FPAY | Annual fee payment |
Payment date: 20180219 Year of fee payment: 5 |
|
| PR1001 | Payment of annual fee |
Payment date: 20180219 Start annual number: 5 End annual number: 5 |
|
| FPAY | Annual fee payment |
Payment date: 20200218 Year of fee payment: 7 |
|
| PR1001 | Payment of annual fee |
Payment date: 20200218 Start annual number: 7 End annual number: 7 |
|
| PR1001 | Payment of annual fee |
Payment date: 20210218 Start annual number: 8 End annual number: 8 |
|
| PR1001 | Payment of annual fee |
Payment date: 20220216 Start annual number: 9 End annual number: 9 |
|
| PR1001 | Payment of annual fee |
Payment date: 20230330 Start annual number: 10 End annual number: 10 |