KR101157278B1 - 1개의 흡착 단계 및 2개의 이성질화 단계를 포함하는 파라크실렌의 제조 방법 - Google Patents

1개의 흡착 단계 및 2개의 이성질화 단계를 포함하는 파라크실렌의 제조 방법 Download PDF

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KR101157278B1
KR101157278B1 KR1020067012754A KR20067012754A KR101157278B1 KR 101157278 B1 KR101157278 B1 KR 101157278B1 KR 1020067012754 A KR1020067012754 A KR 1020067012754A KR 20067012754 A KR20067012754 A KR 20067012754A KR 101157278 B1 KR101157278 B1 KR 101157278B1
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xylene
stream
para
raffinate
column
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KR20060116215A (ko
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필리베르 르플라비에
뤽 울프
제라르 오띠에르
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아이에프피 에너지스 누벨
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
    • C07C5/2767—Changing the number of side-chains
    • C07C5/277—Catalytic processes
    • C07C5/2775—Catalytic processes with crystalline alumino-silicates, e.g. molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/02—Monocyclic hydrocarbons
    • C07C15/067—C8H10 hydrocarbons
    • C07C15/08—Xylenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
    • C07C5/2729—Changing the branching point of an open chain or the point of substitution on a ring
    • C07C5/2732—Catalytic processes
    • C07C5/2737—Catalytic processes with crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020067012754A 2003-11-26 2004-11-23 1개의 흡착 단계 및 2개의 이성질화 단계를 포함하는 파라크실렌의 제조 방법 Expired - Fee Related KR101157278B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0313964 2003-11-26
FR0313964A FR2862638B1 (fr) 2003-11-26 2003-11-26 Procede de production de paraxylene comprenant une etape d'adsorption et deux etapes d'isomerisation
PCT/FR2004/002984 WO2005054161A2 (fr) 2003-11-26 2004-11-23 Procédé de production de paraxylène comprenant une etape d'adsorption et deux etapes d'isomerisation

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KR20060116215A KR20060116215A (ko) 2006-11-14
KR101157278B1 true KR101157278B1 (ko) 2012-06-15

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Country Link
US (1) US7915471B2 (https=)
EP (1) EP1689695B1 (https=)
JP (1) JP4966664B2 (https=)
KR (1) KR101157278B1 (https=)
CN (1) CN1886357B (https=)
AT (1) ATE422195T1 (https=)
DE (1) DE602004019343D1 (https=)
ES (1) ES2321198T3 (https=)
FR (1) FR2862638B1 (https=)
WO (1) WO2005054161A2 (https=)

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FR2883283B1 (fr) * 2005-03-16 2007-05-18 Inst Francais Du Petrole Procede de production combinee de paraxylene et de benzene de productivite amelioree
KR101048568B1 (ko) 2006-04-25 2011-07-12 엑손모빌 케미칼 패턴츠 인코포레이티드 파라-크실렌의 생산방법
US7683233B2 (en) 2006-09-14 2010-03-23 Exxonmobil Chemical Patents Inc. Process for producing para-xylene
KR100843436B1 (ko) * 2007-04-27 2008-07-03 삼성토탈 주식회사 유사 이동층 크실렌 혼합물 전처리 공정 및 추가의 크실렌이성질화 공정을 포함하는 방향족 화합물의 분리 방법
US20100004493A1 (en) * 2008-07-02 2010-01-07 Porter John R Integrated Process
US7960600B2 (en) * 2009-05-28 2011-06-14 Uop Llc Process for improved meta-xylene yield from C8 aromatics
CN102372587A (zh) * 2010-08-23 2012-03-14 中国石油化工股份有限公司 芳烃甲基化的流化床方法
KR20130056357A (ko) * 2010-10-29 2013-05-29 엑손모빌 케미칼 패턴츠 인코포레이티드 파라자일렌의 제조 방법
US20120108868A1 (en) * 2010-10-29 2012-05-03 Dana Lynn Pilliod Process for the Production of Paraxylene
SG189199A1 (en) * 2010-10-29 2013-05-31 Exxonmobil Chem Patents Inc Process for the production of purified xylene isomers
US20120108867A1 (en) * 2010-10-29 2012-05-03 Dana Lynn Pilliod Process for the Production of Purified Xylene Isomers
US8697928B2 (en) 2011-12-15 2014-04-15 Uop Llc Process and apparatus for para-xylene production using multiple adsorptive separation units
US8558049B2 (en) 2011-12-15 2013-10-15 Uop Llc Process and apparatus for para-xylene production using multiple adsorptive separation units and multiple adsorptive bed feed points
US8937209B2 (en) 2011-12-15 2015-01-20 Uop Llc Process and apparatus for para-xylene production using multiple adsorptive separation units with shared raffinate processing
US8802914B2 (en) 2011-12-15 2014-08-12 Uop Llc Process and apparatus for para-xylene production using multiple adsorptive separation units and a split fractionating column
US20150251973A1 (en) * 2012-10-09 2015-09-10 Exxonmobil Chemical Patents Inc. Purge Streams in Paraxylene Production
US9309169B2 (en) 2012-11-30 2016-04-12 Exxonmobil Chemical Patents Inc. Process for the production of purified xylene isomers
SG11201503951WA (en) * 2012-11-30 2015-06-29 Exxonmobil Chem Patents Inc Energy efficient processes for xylenes production
US8933288B2 (en) * 2013-03-20 2015-01-13 Uop Llc System and process for flushing residual fluid from transfer lines in simulated moving bed adsorption
US9328041B2 (en) 2013-09-24 2016-05-03 Uop Llc Methods and systems for separating para-xylene using a radial flow simulated moving bed chamber
US9302955B2 (en) 2013-09-27 2016-04-05 Uop Llc Systems and methods for separating xylene isomers using selective adsorption
US9950972B2 (en) * 2013-09-27 2018-04-24 Uop Llc Apparatuses and methods for forming C8 aromatic streams with selected amounts of C9 aromatics
US9090523B1 (en) 2014-03-03 2015-07-28 Uop Llc Process for flushing top and bottom heads of a vessel
WO2015142454A1 (en) 2014-03-20 2015-09-24 Exxonmobil Chemical Patents Inc. Paraxylene separation process
FR3023840B1 (fr) * 2014-07-18 2016-07-15 Ifp Energies Now Procede de production de paraxylene a haute purete a partir d'une coupe xylenes, utilisant deux unites de separation en lit mobile simule fonctionnant en serie et deux unites d'isomerisation.
FR3023841B1 (fr) * 2014-07-18 2016-07-15 Ifp Energies Now Procede de production de paraxylene comprenant deux unites de separation en lit mobile simule et deux unites d'isomerisation dont l'une en phase gaz
FR3023842B1 (fr) * 2014-07-18 2017-11-24 Ifp Energies Now Procede de production de paraxylene a haute purete a partir d'une coupe xylene, procede utilisant une unite de separation en lit mobile simule et deux unites d'isomerisation, l'une en phase gaz l'autre en phase liquide.
US10226719B2 (en) * 2014-09-30 2019-03-12 Exxonmobil Chemical Patents Inc. Adsorptive separation of multi-component fluid mixtures
WO2016148755A1 (en) * 2015-03-19 2016-09-22 Exxonmobil Chemical Patents Inc. Process and apparatus for the production of para-xylene
US9517979B2 (en) 2015-03-19 2016-12-13 Exxonmobil Chemical Patents Inc. Process and apparatus for the production of para-xylene
US9517980B2 (en) 2015-04-30 2016-12-13 Exxonmobil Chemical Patents Inc. Process and apparatus for the production of para-xylene
CN107531590B (zh) * 2015-04-30 2020-11-06 埃克森美孚化学专利公司 用于生产对二甲苯的方法和装置
US9850186B2 (en) 2016-02-26 2017-12-26 Exxonmobil Chemical Patents Inc. Paraxylene separation process
EP3455195B1 (en) * 2016-03-31 2022-06-08 Uop Llc Processes and apparatuses for naphthene recycle in the production of aromatic products
US10351489B2 (en) * 2016-06-30 2019-07-16 Exxonmobil Chemical Patents Inc. Processes for recovering paraxylene
US10300404B2 (en) * 2016-06-30 2019-05-28 Exxonmobil Chemical Patents Inc. Process for the recovering of paraxylene
US10577293B2 (en) * 2017-04-19 2020-03-03 Uop Llc Process and apparatus for improved para-xylene yield in an aromatic complex
CN108786913B (zh) * 2017-04-26 2021-05-14 中国石油化工股份有限公司 C9以上重芳烃轻质化催化剂及制备方法与应用
CN111655355B (zh) * 2017-12-05 2022-06-07 英力士美国化学公司 对二甲苯回收系统的改装方法
FR3083230B1 (fr) 2018-06-29 2021-04-23 Axens Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement via une colonne de 3 coupes
FR3083231B1 (fr) 2018-06-29 2020-07-17 Axens Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions
ES2972823T3 (es) * 2018-07-20 2024-06-17 Scg Chemicals Co Ltd Proceso para la separación de etilbenceno de otros compuestos aromáticos C8
TWI773974B (zh) 2019-03-29 2022-08-11 美商艾克頌美孚化學專利股份有限公司 新穎沸石，其製法，及其於轉化芳族烴之用途
WO2020205354A1 (en) 2019-03-29 2020-10-08 Exxonmobil Chemical Patents Inc. Mel-type zeolite for converting aromatic hydrocarbons, process for making and catalytic composition comprising said zeolite
CN110330403B (zh) * 2019-06-28 2022-02-18 中国石油天然气集团有限公司 设有甲苯择形歧化的吸附结晶耦合芳烃生产方法及系统
JP7571131B2 (ja) 2019-09-29 2024-10-22 中国石油化工股▲ふん▼有限公司 エチルベンゼンを含むＣ８芳香族化合物からｐ－キシレンおよびエチルベンゼンを製造する方法
FR3104572B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Conversion de composés aromatiques par alkylation de toluène par du CO et de benzène par l’éthanol pour production de paratolualdéhyde
FR3104571B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de toluène par du CO pour production de paratolualdéhyde
FR3104577B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de toluène par du CO
FR3104576B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de benzène par l’éthanol
FR3104575B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de benzène par du CO
FR3104579B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de benzène par de l’éthylène
FR3104574B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de toluène par du CO et de benzène par l’éthanol
FR3104573B1 (fr) 2019-12-17 2021-12-31 Ifp Energies Now Dispositif et procédé de conversion de composés aromatiques par alkylation de toluène par du méthanol
CN113461471B (zh) * 2020-03-30 2023-10-10 中国石油化工股份有限公司 一种对二甲苯的生产装置及生产工艺
FR3112774B1 (fr) 2020-07-27 2023-06-02 Ifp Energies Now Dispositif et procédé de production d’aromatiques par pyrolyse de biomasse et conversion de gaz à l'eau inversée.
FR3112773B1 (fr) 2020-07-27 2023-06-02 Ifp Energies Now Dispositif et procédé de production d’aromatiques à partir d’un gaz de pyrolyse de biomasse
FR3126976A1 (fr) 2021-09-10 2023-03-17 IFP Energies Nouvelles Oxycombustion de composés hydrocarbonés riches en oxygène pour la production de xylènes.
FR3126977A1 (fr) 2021-09-10 2023-03-17 IFP Energies Nouvelles Combustion en boucle chimique de composés hydrocarbonés riches en oxygène pour la production de xylènes.
FR3130833B1 (fr) 2021-12-21 2024-10-11 Ifp Energies Now Unité de production et de séparation des aromatiques avec valorisation d’un extrait et/ou d’un raffinat provenant d’un procédé d’extraction liquide-liquide
FR3143029A1 (fr) 2022-12-13 2024-06-14 IFP Energies Nouvelles Procédé et dispositif de production d’aromatiques et de monoéthylène glycol à partir d’un gaz de pyrolyse de biomasse
CN118949456B (zh) * 2023-05-15 2025-11-25 中国石油化工股份有限公司 低能耗生产对二甲苯系统和方法

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US4313015A (en) * 1980-02-07 1982-01-26 Uop Inc. Separation process
FR2782714A1 (fr) 1998-08-26 2000-03-03 Inst Francais Du Petrole Procede de coproduction de metaxylene et de paraxylene
FR2808270A1 (fr) 2000-04-27 2001-11-02 Inst Francais Du Petrole Procede de coproduction de metaxylene et de paraxylene

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FR2728894A1 (fr) * 1994-12-29 1996-07-05 Inst Francais Du Petrole Procede de separation de paraxylene comportant au moins deux etages de cristallisation a haute temperature
US5763714A (en) * 1997-01-08 1998-06-09 Catalytic Distillation Technologies Process and apparatus for the production and recovery of p-xylene
DE19809418A1 (de) * 1998-03-05 1999-09-09 Basf Ag Verfahren zur Hydrierung von Carbonylverbindungen
EP1165471A1 (en) * 1999-03-31 2002-01-02 Chevron Chemical Company LLC Process for the separation of para-xylene using an ether as desorbent
FR2792632B1 (fr) * 1999-04-22 2004-02-13 Inst Francais Du Petrole Procede de production de paraxylene comprenant une etape d'adsorption, une etape d'isomerisation en phase liquide et une etape d'isomerisation en phase gazeuse avec une zeolithe de type eu0
FR2795407B1 (fr) * 1999-06-22 2001-10-05 Inst Francais Du Petrole Procede de production d'au moins un isomere des xylenes comprenant une etape d'adsorption et une etape d'isomerisation avec un catalyseur de type structural euo
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FR2822820B1 (fr) * 2001-03-29 2003-05-30 Inst Francais Du Petrole Procede de coproduction de paraxylene et de metaxylene comprenant deux etapes de separation
FR2844790B1 (fr) * 2002-09-20 2004-10-22 Inst Francais Du Petrole Procede de coproduction de paraxylene et de styrene

Patent Citations (3)

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US4313015A (en) * 1980-02-07 1982-01-26 Uop Inc. Separation process
FR2782714A1 (fr) 1998-08-26 2000-03-03 Inst Francais Du Petrole Procede de coproduction de metaxylene et de paraxylene
FR2808270A1 (fr) 2000-04-27 2001-11-02 Inst Francais Du Petrole Procede de coproduction de metaxylene et de paraxylene

Also Published As

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CN1886357B (zh) 2012-09-05
DE602004019343D1 (de) 2009-03-19
JP2007512293A (ja) 2007-05-17
US20080262282A1 (en) 2008-10-23
CN1886357A (zh) 2006-12-27
EP1689695B1 (fr) 2009-02-04
US7915471B2 (en) 2011-03-29
ES2321198T3 (es) 2009-06-03
FR2862638A1 (fr) 2005-05-27
WO2005054161A3 (fr) 2005-09-09
KR20060116215A (ko) 2006-11-14
FR2862638B1 (fr) 2005-12-30
ATE422195T1 (de) 2009-02-15
WO2005054161A2 (fr) 2005-06-16
EP1689695A2 (fr) 2006-08-16
JP4966664B2 (ja) 2012-07-04

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