KR101014356B1 - 메타크릴산 제조용 촉매의 제조방법 - Google Patents

메타크릴산 제조용 촉매의 제조방법 Download PDF

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Publication number
KR101014356B1
KR101014356B1 KR1020057022309A KR20057022309A KR101014356B1 KR 101014356 B1 KR101014356 B1 KR 101014356B1 KR 1020057022309 A KR1020057022309 A KR 1020057022309A KR 20057022309 A KR20057022309 A KR 20057022309A KR 101014356 B1 KR101014356 B1 KR 101014356B1
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KR
South Korea
Prior art keywords
water
compound containing
catalyst
slurry
insoluble substance
Prior art date
Application number
KR1020057022309A
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English (en)
Korean (ko)
Other versions
KR20060015289A (ko
Inventor
아츠시 스도
요시마사 세오
타츠히코 구라카미
Original Assignee
니폰 가야꾸 가부시끼가이샤
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Publication of KR20060015289A publication Critical patent/KR20060015289A/ko
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Publication of KR101014356B1 publication Critical patent/KR101014356B1/ko

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • B01J27/199—Vanadium with chromium, molybdenum, tungsten or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0219—Coating the coating containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/377—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
KR1020057022309A 2003-05-30 2004-05-27 메타크릴산 제조용 촉매의 제조방법 KR101014356B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JPJP-P-2003-00154000 2003-05-30
JP2003154000 2003-05-30

Publications (2)

Publication Number Publication Date
KR20060015289A KR20060015289A (ko) 2006-02-16
KR101014356B1 true KR101014356B1 (ko) 2011-02-15

Family

ID=33487308

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020057022309A KR101014356B1 (ko) 2003-05-30 2004-05-27 메타크릴산 제조용 촉매의 제조방법

Country Status (12)

Country Link
US (1) US20070010394A1 (fr)
EP (1) EP1629889B1 (fr)
JP (1) JP4421558B2 (fr)
KR (1) KR101014356B1 (fr)
CN (1) CN100518935C (fr)
BR (1) BRPI0410816A (fr)
MX (1) MXPA05012783A (fr)
MY (1) MY144127A (fr)
RU (1) RU2351395C2 (fr)
TW (1) TWI365103B (fr)
WO (1) WO2004105941A1 (fr)
ZA (1) ZA200510251B (fr)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI341219B (en) * 2003-02-20 2011-05-01 Nippon Kayaku Kk Catalyst for producing methacrylic acid and preparation method thereof
US7229945B2 (en) * 2003-12-19 2007-06-12 Saudi Basic Industrics Corporation Process of making mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins
JP4756890B2 (ja) * 2005-03-29 2011-08-24 日本化薬株式会社 メタクリル酸製造用触媒及びその製造方法
JP2006314923A (ja) * 2005-05-12 2006-11-24 Nippon Kayaku Co Ltd メタクリル酸製造用触媒の製造方法
US7732367B2 (en) * 2005-07-25 2010-06-08 Saudi Basic Industries Corporation Catalyst for methacrolein oxidation and method for making and using same
JP4825030B2 (ja) * 2006-03-22 2011-11-30 三菱レイヨン株式会社 メタクリル酸製造用触媒の製造方法
US8178718B2 (en) * 2007-02-05 2012-05-15 Saudi Basic Industries Corporation Catalyst for oxidation of saturated and unsaturated aldehydes to unsaturated carboxylic acid, method of making and method of using thereof
JP4881229B2 (ja) * 2007-06-13 2012-02-22 三菱レイヨン株式会社 メタクリル酸製造用触媒、その製造方法及びこれを用いたメタクリル酸の製造方法
WO2010052909A1 (fr) * 2008-11-06 2010-05-14 日本化薬株式会社 Procédé de fabrication d'acide méthacrylique et catalyseur utilisable à cet effet
JP4900449B2 (ja) * 2009-10-30 2012-03-21 住友化学株式会社 メタクリル酸製造用触媒の製造方法及びメタクリル酸の製造方法
JP5768326B2 (ja) * 2010-04-22 2015-08-26 三菱レイヨン株式会社 触媒の製造方法およびメタクリル酸の製造方法
EP2934215B1 (fr) * 2012-12-21 2019-03-13 NIKE Innovate C.V. Tige tissée d'article chaussant comportant un verrouillage
MY189907A (en) * 2016-09-14 2022-03-21 Mitsubishi Chem Corp Catalyst for production of methacrylic acid, method of producing the same, method of producing methacrylic acid, and method of producing methacrylic acid ester
CN109305899B (zh) * 2017-07-28 2021-09-03 中国石油化工股份有限公司 甘油脱水生产丙烯醛的方法
CN109304193B (zh) * 2017-07-28 2021-11-30 中国石油化工股份有限公司 用于甘油制丙烯醛的催化剂
KR102463952B1 (ko) * 2018-04-26 2022-11-04 미쯔비시 케미컬 주식회사 메타크릴산 제조용 촉매의 제조 방법, 및 메타크릴산 및 메타크릴산 에스터의 제조 방법
EP3760608A1 (fr) 2019-07-05 2021-01-06 Röhm GmbH Procédé de fabrication de méthacrylates d'alkyle et éventuellement d'acides méthacryliques
EP3889127A1 (fr) 2020-04-03 2021-10-06 Röhm GmbH Procédé sécurisé amélioré pour l'oxydation c-4 en tandem en acide méthacrylique
EP3945086B1 (fr) 2020-07-30 2022-10-26 Röhm GmbH Procédé basé sur le c-4 destiné à la fabrication de mma à l'aide du recyclage et du recyclage de la méthacroleine
EP3945088A1 (fr) 2020-07-30 2022-02-02 Röhm GmbH Procédé de minimisation de perte d'activité lors des étapes réactionnelles exécutées en fonctionnement en circuit
CN114425377B (zh) * 2020-09-24 2023-10-10 中国石油化工股份有限公司 一种邻苯二甲醛催化剂、制备方法及应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0531368A (ja) * 1990-11-14 1993-02-09 Mitsui Toatsu Chem Inc メタクリル酸製造用触媒及びメタクリル酸の製造方法
JPH1143314A (ja) 1997-07-25 1999-02-16 Mitsubishi Chem Corp 複合酸化物の製造方法
JPH11226411A (ja) 1998-02-13 1999-08-24 Mitsui Chem Inc メタクリル酸製造用触媒及びメタクリル酸の製造方法
JP2002233760A (ja) 2000-09-21 2002-08-20 Nippon Kayaku Co Ltd メタクリル酸製造用触媒、被覆触媒及びその製法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4000088A (en) * 1974-06-03 1976-12-28 Nippon Kayaku Co., Ltd. Oxidation catalyst for the manufacture of methacrylic acid
JPS54161594A (en) * 1978-06-13 1979-12-21 Mitsubishi Chem Ind Ltd Production of catalyst composition
JPS55124734A (en) * 1979-03-22 1980-09-26 Nippon Kayaku Co Ltd Preparation of methacrylic acid
US5198579A (en) * 1990-11-14 1993-03-30 Mitsui Toatsu Chemicals, Inc. Catalyst for oxidizing methacrolein and method for preparing methacrylic acid

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0531368A (ja) * 1990-11-14 1993-02-09 Mitsui Toatsu Chem Inc メタクリル酸製造用触媒及びメタクリル酸の製造方法
JPH1143314A (ja) 1997-07-25 1999-02-16 Mitsubishi Chem Corp 複合酸化物の製造方法
JPH11226411A (ja) 1998-02-13 1999-08-24 Mitsui Chem Inc メタクリル酸製造用触媒及びメタクリル酸の製造方法
JP2002233760A (ja) 2000-09-21 2002-08-20 Nippon Kayaku Co Ltd メタクリル酸製造用触媒、被覆触媒及びその製法

Also Published As

Publication number Publication date
EP1629889A4 (fr) 2007-10-03
TWI365103B (en) 2012-06-01
CN100518935C (zh) 2009-07-29
JP4421558B2 (ja) 2010-02-24
ZA200510251B (en) 2006-10-25
JPWO2004105941A1 (ja) 2006-07-20
EP1629889B1 (fr) 2012-05-02
TW200510061A (en) 2005-03-16
RU2005139392A (ru) 2007-06-27
CN1795047A (zh) 2006-06-28
BRPI0410816A (pt) 2006-06-27
WO2004105941A1 (fr) 2004-12-09
MY144127A (en) 2011-08-15
MXPA05012783A (es) 2006-02-22
US20070010394A1 (en) 2007-01-11
RU2351395C2 (ru) 2009-04-10
KR20060015289A (ko) 2006-02-16
EP1629889A1 (fr) 2006-03-01

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