KR100954045B1 - 개선된 아크릴산 제조용 촉매의 합성방법 - Google Patents

개선된 아크릴산 제조용 촉매의 합성방법 Download PDF

Info

Publication number
KR100954045B1
KR100954045B1 KR1020070081258A KR20070081258A KR100954045B1 KR 100954045 B1 KR100954045 B1 KR 100954045B1 KR 1020070081258 A KR1020070081258 A KR 1020070081258A KR 20070081258 A KR20070081258 A KR 20070081258A KR 100954045 B1 KR100954045 B1 KR 100954045B1
Authority
KR
South Korea
Prior art keywords
acid
catalyst
salt
acrylic acid
sulfuric acid
Prior art date
Application number
KR1020070081258A
Other languages
English (en)
Korean (ko)
Other versions
KR20090016919A (ko
Inventor
송은경
차경용
김진도
조현주
Original Assignee
주식회사 엘지화학
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 주식회사 엘지화학 filed Critical 주식회사 엘지화학
Priority to KR1020070081258A priority Critical patent/KR100954045B1/ko
Priority to PCT/KR2008/001126 priority patent/WO2009022780A1/en
Priority to CN200880102720.1A priority patent/CN101778669B/zh
Priority to JP2010520921A priority patent/JP5180303B2/ja
Publication of KR20090016919A publication Critical patent/KR20090016919A/ko
Application granted granted Critical
Publication of KR100954045B1 publication Critical patent/KR100954045B1/ko

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08Heat treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002Mixed oxides other than spinels, e.g. perovskite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24Chromium, molybdenum or tungsten
    • B01J23/28Molybdenum
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/053Sulfates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/057Selenium or tellurium; Compounds thereof
    • B01J27/0576Tellurium; Compounds thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/04Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing carboxylic acids or their salts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02Impregnation, coating or precipitation
    • B01J37/0236Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00Constitutive chemical elements of heterogeneous catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020070081258A 2007-08-13 2007-08-13 개선된 아크릴산 제조용 촉매의 합성방법 KR100954045B1 (ko)

Priority Applications (4)

Application Number Priority Date Filing Date Title
KR1020070081258A KR100954045B1 (ko) 2007-08-13 2007-08-13 개선된 아크릴산 제조용 촉매의 합성방법
PCT/KR2008/001126 WO2009022780A1 (en) 2007-08-13 2008-02-27 Method of preparing improved catalyst for production of acrylic acid
CN200880102720.1A CN101778669B (zh) 2007-08-13 2008-02-27 制备用于生产丙烯酸的改良催化剂的方法
JP2010520921A JP5180303B2 (ja) 2007-08-13 2008-02-27 改善したアクリル酸製造用触媒の製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020070081258A KR100954045B1 (ko) 2007-08-13 2007-08-13 개선된 아크릴산 제조용 촉매의 합성방법

Publications (2)

Publication Number Publication Date
KR20090016919A KR20090016919A (ko) 2009-02-18
KR100954045B1 true KR100954045B1 (ko) 2010-04-20

Family

ID=40350821

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020070081258A KR100954045B1 (ko) 2007-08-13 2007-08-13 개선된 아크릴산 제조용 촉매의 합성방법

Country Status (4)

Country Link
JP (1) JP5180303B2 (zh)
KR (1) KR100954045B1 (zh)
CN (1) CN101778669B (zh)
WO (1) WO2009022780A1 (zh)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2900775C (en) * 2015-08-20 2023-10-10 Nova Chemicals Corporation Improved oxidative dehydrogenation catalyst
WO2018016155A1 (ja) * 2016-07-20 2018-01-25 東亞合成株式会社 金属酸化物触媒の製造方法
CA2993683A1 (en) 2018-02-02 2019-08-02 Nova Chemicals Corporation Method for in situ high activity odh catalyst
CN113492017A (zh) * 2020-04-08 2021-10-12 中国石油天然气股份有限公司 一种负载型丙烷催化氧化制丙烯酸催化剂及其制备方法与应用
CN116328796B (zh) * 2021-12-22 2024-06-04 中国石油天然气股份有限公司 一种Mo-V-Te-Nb体系催化剂及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050215818A1 (en) 2004-03-25 2005-09-29 Nippon Shokubai Co., Ltd. Catalyst for production of acrylic acid and process for production of acrylic acid using this catalyst
US7109144B2 (en) 2000-12-13 2006-09-19 Asahi Kasei Kabushiki Kaisha Oxide catalyst for oxidation or ammoxidation

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0813777B2 (ja) * 1986-12-11 1996-02-14 三菱化学株式会社 アクリル酸の製造法
JP4845325B2 (ja) * 2000-06-15 2011-12-28 旭化成ケミカルズ株式会社 プロパンまたはイソブタンの気相接触酸化反応または気相接触アンモ酸化反応用触媒
US6642173B2 (en) * 2001-04-25 2003-11-04 Rohm And Haas Company Catalyst
US6841699B2 (en) * 2001-04-25 2005-01-11 Rohm And Haas Company Recalcined catalyst
US6645905B2 (en) * 2001-04-25 2003-11-11 Rohm And Haas Company Annealed and promoted catalyst
US6645906B2 (en) * 2001-04-30 2003-11-11 Rohm And Haas Company High temperature mixing
BRPI0500615B1 (pt) * 2004-03-10 2015-07-14 Rohm & Haas Catalisador modificado, e, sistema de catalisador modificado
US20070203022A1 (en) * 2004-07-22 2007-08-30 Fritz Haber Institut Der Max Planck Gesellschaft Metal Oxide Catalyst And Method For The Preparation Thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7109144B2 (en) 2000-12-13 2006-09-19 Asahi Kasei Kabushiki Kaisha Oxide catalyst for oxidation or ammoxidation
US20050215818A1 (en) 2004-03-25 2005-09-29 Nippon Shokubai Co., Ltd. Catalyst for production of acrylic acid and process for production of acrylic acid using this catalyst

Also Published As

Publication number Publication date
KR20090016919A (ko) 2009-02-18
CN101778669A (zh) 2010-07-14
JP2010535628A (ja) 2010-11-25
JP5180303B2 (ja) 2013-04-10
CN101778669B (zh) 2014-02-12
WO2009022780A1 (en) 2009-02-19

Similar Documents

Publication Publication Date Title
US7544633B2 (en) Catalyst for partial oxidation and preparation method thereof
CN108325545B (zh) 一种磷酸氧钒催化剂、其制备方法及用途
KR100954045B1 (ko) 개선된 아크릴산 제조용 촉매의 합성방법
EP1968928B1 (en) Process for synthesizing a heteropoly acid catalyst for oxidation of unsaturated aldehydes to unsaturated carboxylic acid
JP5100520B2 (ja) α,β−不飽和カルボン酸合成用触媒の製造方法
JP5362370B2 (ja) メタクリル酸合成用触媒の製造方法
CN106881101B (zh) 复合氧化物催化剂及其制备方法和用途
JP5560596B2 (ja) メタクリル酸製造用触媒の製造方法
JP2004188231A (ja) メタクリル酸製造用触媒の製造方法およびメタクリル酸の製造方法
KR100970084B1 (ko) 활성 물질의 소실을 억제한 촉매의 제조방법
JPH0615178A (ja) メタクリル酸製造用触媒の調製方法
KR100954046B1 (ko) 반응성 볼밀링을 이용한 아크릴산 제조용 촉매의 제조방법
KR100982831B1 (ko) 헤테로폴리산계 촉매의 제조방법
JP4629886B2 (ja) メタクロレインおよび/またはメタクリル酸製造用触媒、その製造方法、および、メタクロレインおよび/またはメタクリル酸の製造方法
KR100280372B1 (ko) 다성분계 복합산화물 촉매와 이의 제조방법
KR102346234B1 (ko) 촉매 전구체, 촉매의 제조 방법, 메타크릴산 및 아크릴산의 제조 방법, 및 메타크릴산 에스터 및 아크릴산 에스터의 제조 방법
JP2003154273A (ja) メタクリル酸製造用触媒の製造方法、メタクリル酸製造用触媒、および、メタクリル酸の製造方法
CN112547082B (zh) 用于丙烯醛氧化制丙烯酸的催化剂及其制备方法和应用
JP2002095972A (ja) メタクリル酸製造用触媒、その製造方法、およびメタクリル酸の製造方法
JP2009095713A (ja) メタクリル酸製造用触媒およびその製造方法、並びにメタクリル酸の製造方法

Legal Events

Date Code Title Description
A201 Request for examination
E701 Decision to grant or registration of patent right
GRNT Written decision to grant
FPAY Annual fee payment

Payment date: 20130410

Year of fee payment: 4

FPAY Annual fee payment

Payment date: 20140318

Year of fee payment: 5

FPAY Annual fee payment

Payment date: 20170328

Year of fee payment: 8

FPAY Annual fee payment

Payment date: 20180403

Year of fee payment: 9

FPAY Annual fee payment

Payment date: 20190401

Year of fee payment: 10