KR100840212B1 - Method of manufacturing lacquer with allergen-free components and its manufacturing apparatus and printed matter using this lacquer - Google Patents

Method of manufacturing lacquer with allergen-free components and its manufacturing apparatus and printed matter using this lacquer Download PDF

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KR100840212B1
KR100840212B1 KR1020070111380A KR20070111380A KR100840212B1 KR 100840212 B1 KR100840212 B1 KR 100840212B1 KR 1020070111380 A KR1020070111380 A KR 1020070111380A KR 20070111380 A KR20070111380 A KR 20070111380A KR 100840212 B1 KR100840212 B1 KR 100840212B1
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lacquer
distillation
water
tank
high pressure
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KR1020070111380A
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Korean (ko)
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한을수
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주식회사원주옻식품
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

A method for preparing lacquer liquor, its preparation apparatus, and a printed product using the lacquer liquor prepared by the method are provided to obtain the allergy inducing component-free lacquer liquor in liquid state. A method for preparing lacquer liquor comprises the steps of heating (distilling) 1 kg of a lacquer tree cut by a size of 5-50 mm with 6-10 L of water at 150-300 deg.C; and supplying the distilled solution to a filter(30) to remove the impurities, wherein the distillation is carried out under the high pressure oxygen of 1.5-2.5 atm., 3-5 L of the vapor generated at the distillation process is extracted through a cooler(15), and the solution (water) remaining in the distillation tank(10) is sprayed together with oxygen of 4.5-5 atm by a high pressure to a purification tank before the filtering process.

Description

알러지 유발성분이 제거된 옻물 제조방법과 그 제조장치 및 이 옻물을 이용한 인쇄물{omitted}Method for manufacturing lacquer with allergen-free components and its manufacturing apparatus and printed matter using the lacquer

본 발명은 건조시키지 않은 생옻나무로부터 알러지 유발성분을 제거함으로써 다양한 용도로 사용할 수 있는 옻물을 얻을 수 있도록 하는 방법과 그 제조장치 및 이 옻물을 이용한 인쇄물를 제공하기 위한 것이다.The present invention is to provide a method for producing a lacquer that can be used for a variety of purposes by removing allergens from undecided raw lacquer and its production apparatus and a printed matter using the lacquer.

옻나무(rhus vernicflua)는 옻나무과에 속하는 낙엽고목으로 중국이 원산지이며 대한민국,일본,중국 등 주로 동북아시아에서 재배되고 있으며, 옻나무의 수액인 옻은 일종의 식물생리상 분비물로써 주로 수피의 2차 사부조직(secondary phloem) 내에 존재하는 것으로 오래전부터 천연도료 및 약재로 이용되었다.Rhus vernicflua is a deciduous tree belonging to the family Lacaceae and is native to China and is cultivated mainly in Northeast Asia such as Korea, Japan and China. The lacquer sap is a kind of plant physiological secretion and is mainly composed of bark secondary quadruples ( It has been used as a natural paint and medicine for a long time.

동양에서는 옻이 여성의 생리기 이상, 위장약, 구충제, 혈액순환, 노화방지 등의 처방제로 전래되어 왔으며, 우리나라에서는 옻나무를 옻닭, 옻오리 등에 이용하여 중풍,고혈압 등에 효과가 있는 몸보신용 식품으로 애용 하여왔다.In the Orient, lacquer has been introduced as a prescription medicine for women's menstrual disorders, gastrointestinal drugs, insect repellents, blood circulation, and anti-aging.In Korea, lacquer is used as a food for body care that is effective in stroke, hypertension, etc. Has been.

옻나무에서 발견된 성분들은 주로 후라보노이드계 물질로서 피세틴(fisetin)및 푸스틴(fustin)과 같은 후라보노이드는 혈관이나 모세혈관을 보호하는 작용이 있다고 알려져 있다.The components found in the lacquer tree are mainly flavonoid-based substances, and flavonoids such as fisetin and fustin are known to protect blood vessels or capillaries.

상술한 바와 같이 옻나무는 인체 건강증진에 좋은 원료로 이용이 가능함에도 불구하고 알러지 유발성분이 있어 복용할 수 없거나 미량 밖에는 복용할 수 없었으나 본원출원인은 건조되지 않은 생옻나무에서 알러지 유발성분인 우루시올(urushiol)을 제거하여 누구나 안심하고 음용할 수 있는 옻물을 제조하였고, 이 옻물을 식품,화장품,음료 및 건강보조식품의 원료로 사용할 수 있음을 확인함으로써 본 발명을 완성하게 되었다.As mentioned above, although lacquer trees can be used as a good raw material for human health promotion, they can not be taken because of allergen-causing ingredients or only a small amount. urushiol) was removed to prepare a lacquer that can be safely drink anyone, the present invention was completed by confirming that the lacquer can be used as a raw material of food, cosmetics, beverages and health supplements.

본 발명이 해결하고자 하는 과제는 물에 넣어진 생옻나무를 가압상태에서 가열하는 과정에서 증류 시켜 알러지 유발성분인 우루시올을 제거한후 남은 물만을 정제탱크 내에 고압으로 분사하여 여과 시키는 방법으로 알러지 성분을 제거한 옻물을 제조함으로써 건조되지 않은 상태의 옻나무를 원재료로 사용할 수 있도록 한 옻물 제조 방법 및 그 장치 및 이 옻물을 이용한 인쇄물을 제공하기 위한 것이다.The problem to be solved by the present invention is to remove the allergen component by the method of distilling the raw lacquer in water in the process of heating under pressure to remove urushiol which is the allergen causing component and spraying only the remaining water at high pressure into the refining tank. The present invention provides a method and apparatus for producing a lacquer and a printed matter using the lacquer, by which a lacquer in an undried state can be used as a raw material by preparing the lacquer.

본 발명의 과제는 5~50㎜ 크기로 절단된 생옻나무 1㎏에 대하여 물 6~10ℓ를 증류탱크에 넣어 교반익으로 섞어주는 상태에서 150~300℃로 가열하는 증류공정; 상기 증류공정에서 얻은 물을 여과기로 공급하여 불순물을 제거하는 여과공정;으로 이루어진 것에 있어서, 1.5~2.5기압의 고압산소가 증류탱크에 공급되어 생옻나무가 가압되는 상태에서 상기 증류공정이 이루어지고, 상기 증류공정에서 발생된 증기는 냉각기를 통해 3~5ℓ추출해내며, 상기 증류탱크에 남은 물만을 4.5~5기압의 산소와 함께 정제탱크 내에 고압으로 분사하는 정제공정을 더 거친후 여과공정이 이루어지도록 한 것을 특징으로 하는 알러지 유발성분이 제거된 옻물 제조방법에 의하여 달성되어진다.The problem of the present invention is a distillation step of heating to 150 ~ 300 ℃ in the state of mixing 6 ~ 10L of water into a distillation tank with respect to 1kg of raw lacquer wood cut into 5-50mm size; A filtration step of removing impurities by supplying water obtained in the distillation step with a filter; wherein the distillation step is performed while a high pressure oxygen of 1.5 to 2.5 atm is supplied to the distillation tank to pressurize the live lacquer. The steam generated in the distillation process is extracted 3 to 5 L through a cooler, and after the purification process is performed through a refining process in which only water remaining in the distillation tank is sprayed with high pressure into the refining tank with oxygen of 4.5 to 5 atm. It is achieved by the method for producing lacquer water from which the allergen causing ingredient is removed.

상기 옻물 제조 방법은, 모터에 의해 구동되는 교반익이 내부에 설치되고, 외부에는 가열수단이 설치되어 물과 생옻나무가 넣어지는 증류탱크; 한쪽이 상기 증류탱크와 연결 설치된 물공급라인; 상기 물공급라인의 다른 쪽에 연결 설치된 정제탱크; 상기 정제탱크와 여과라인에 의해 연결 설치된 여과기;로 이루어진 것에 있어서, 상기 증류탱크에 1.5~2.5기압의 고압산소를 공급하여 생옻나무를 가압하는 고압산소 공급라인과 냉각기가 중간에 설치된 증기 배출라인을 각각 연결 설치하고, 상기 물공급라인의 다른 쪽에는 상기 정제탱크 내부에 위치하는 다수의 노즐공을 형성하며, 상기 물공급라인의 중간에 4.5~5기압의 고압산소를 공급하는 고압산소 공급라인을 연결설치 하여서 된 것을 특징으로 하는 알러지 유발성분이 제거된 옻물 제조장치에 의하여 이루어진다.The method for producing lacquer is a distillation tank in which a stirring vane driven by a motor is installed inside and a heating means is installed outside to put water and raw lacquer; A water supply line having one side connected to the distillation tank; A purification tank connected to the other side of the water supply line; A high pressure oxygen supply line for supplying high pressure oxygen having a pressure of 1.5 to 2.5 atm to the distillation tank and pressurizing a raw lacquer, and a steam discharge line provided with a cooler in the middle; Connected to each installation, the other side of the water supply line to form a plurality of nozzle holes located in the purification tank, the high pressure oxygen supply line for supplying high pressure oxygen of 4.5 to 5 atm in the middle of the water supply line It is made by the lacquer manufacturing apparatus is removed from the allergens, characterized in that the connection was made.

상기 가열수단은 히터와 상기 히터에 의해 가열되어 증류탱크의 온도를 균일하게 올려주는 열매체로 이루어진다.The heating means is made of a heating medium heated by the heater and the heater to uniformly raise the temperature of the distillation tank.

상기 옻물 제조 방법과 그 장치를 이용하여 얻어진 옻물은 다양한 용도로 사용될 수 있으며 본 발명에서는 상기 제조방법에 의해 얻어진 옻물에 함침된 원지를 드라이기로 이송하여 건조시키고 이를 옻물이 공급되는 인쇄로울러에 통과시켜 무늬가 인쇄 되도록 한 인쇄물를 일실시예로 제시한다.The method of manufacturing the lacquer and the lacquer obtained by using the apparatus can be used for various purposes. In the present invention, the base paper impregnated with the lacquer obtained by the manufacturing method is transferred to a dryer and dried, and passed through a printing roller supplied with the lacquer. In one embodiment, a printed material on which a pattern is printed is presented.

본 발명의 실시를 위한 구체적인 내용을 상세히 설명하면 다음과 같다.Detailed description for carrying out the present invention will be described below.

도 1은 본 발명의 옻물 제조 장치를 보인 도면으로써, 이것은 도시된 바와 같이 모터(11)에 의해 구동되는 교반익(12)이 내부에 설치되고, 외부에는 가열수단(13)이 설치되며, 냉각기(15)가 중간에 설치된 증기 배출라인(14)과 고압산소 공급라인(16)이 각각 연결설치된 증류탱크(10); 고압산소 공급라인(21)과 중간부분이 연결되고, 한쪽 끝은 상기 증류탱크(10)와 연결되며, 다른 쪽에는 다수의 노즐공(23)이 형성된 물공급라인(22); 상기 노즐공(23)이 내부에 위치하도록 물공급라인(22)의 다른 쪽에 연결설치된 정제탱크(20); 상기 정제탱크(20)와 여과라인(31)에 의해 연결설치된 여과기(30);로 이루어진 것이다.1 is a view showing the lacquer manufacturing apparatus of the present invention, which is a stirring vane 12 driven by the motor 11 as shown therein, the heating means 13 is installed outside, the cooler A distillation tank 10 in which a steam discharge line 14 and a high-pressure oxygen supply line 16 are respectively connected to each other; A high pressure oxygen supply line 21 and an intermediate portion are connected, one end is connected to the distillation tank 10, and the other side is provided with a water supply line 22 having a plurality of nozzle holes 23; A purification tank 20 connected to the other side of the water supply line 22 so that the nozzle hole 23 is located inside; It consists of; filter 30 is connected by the purification tank 20 and the filtration line 31.

상기 가열수단(13)은 히터와 상기 히터에 의해 가열되어 증류탱크의 온도를 균일하게 올려주는 열매체로 이루어진다.The heating means 13 is made of a heating medium heated by the heater and the heater to uniformly raise the temperature of the distillation tank.

상기 여과기(30)가 설치된 여과라인(31)에는 사용되는 필터의 종류에 따라 고압산소 공급라인(32)을 부가할 수 있다.The high pressure oxygen supply line 32 may be added to the filtration line 31 in which the filter 30 is installed, depending on the type of filter used.

이렇게 구성된 옻물 제조 장치를 이용하여 본 발명을 실시하기 위해서는 먼저 건조시키지 않은 생옻나무를 5~50㎜ 크기로 절단한후 아래와 같은 공정을 거친다. In order to carry out the present invention using the lacquer manufacturing apparatus configured as described above, the raw lacquer is not dried and then cut to a size of 5 to 50 mm.

[증류 공정]Distillation process

증류탱크(10)에 5~50㎜ 크기로 절단된 생옻나무 1㎏에 대하여 물 6~10ℓ를 넣고 교반익(12)에 의해 섞어주면서 고압산소 공급라인(16)을 통해 1.5~2.5기압의 고압산소를 공급하는 상태에서 가열수단(13)에 의해 증류탱크(10)의 내부온도가 150~300℃를 유지하도록 40~80분간 가열한다.6 to 10 liters of water was added to 1 kg of the raw lacquer tree cut to the size of 5 to 50 mm in the distillation tank 10 and mixed by the stirring blade 12, and the high pressure of 1.5 to 2.5 atm through the high pressure oxygen supply line 16. In the state of supplying oxygen, the heating means 13 heats 40 to 80 minutes to maintain the internal temperature of the distillation tank 10 at 150 to 300 ° C.

본 발명에서 사용되는 생옻나무는 채취한 그대로 전체를 5~50㎜ 크기로 절단한 것이다.The raw lacquer tree used in the present invention is cut into the entire 5-50 mm size as it is collected.

증류탱크(10)의 온도가 상승하여 끓게 되면 증기가 발생되는데 이 증기는 냉각기(15)에서 액체로 냉각되어 증기 배출라인(14)을 통해 외부로 배출된다.When the temperature of the distillation tank 10 rises and boils, steam is generated. The steam is cooled with liquid in the cooler 15 and discharged to the outside through the steam discharge line 14.

이렇게 증기 배출라인(14)의 냉각기(15)를 통해 외부로 배출되는 액체에는 생옻나무의 알러지 유발물질인 우루시올이 다량 함유되어 있으며, 우루시올의 증류 추출시 물과 생옻나무를 교반시키는 동시에 고압산소를 공급하는 이유는 생옻나무를 가압 시켜줌으로써 생옻나무를 발로 밟아주며 수액을 짜내는 것과 같은 상태가 되도록 하여 우루시올을 효율적으로 증류시키기 위한 것이다.The liquid discharged to the outside through the cooler 15 of the steam discharge line 14 contains a large amount of urushiol, which is an allergen of the raw lacquer tree, while stirring the water and the raw lacquer tree during the distillation extraction of the urushiol, The reason for supplying is to press the raw lacquer to press down on the bare lacquer and to distill urushiol in such a state as to squeeze out the sap.

[정제 공정][Refining process]

증류탱크(10)의 내부온도가 150~300℃를 유지하도록 40~80분간 가열하여 증류된 우루시올 추출액의 양이 3~5ℓ가 되면 가열수단(13)을 정지시키고 밸브(160)을 작동시켜 고압산소 공급라인(16)를 차단한다.When the internal temperature of the distillation tank 10 is maintained for 150 ~ 300 ℃ 40 ~ 80 minutes the amount of distilled urushiol extract is 3 ~ 5l when the heating means 13 is stopped and the valve 160 is operated to operate the high pressure The oxygen supply line 16 is shut off.

물공급 라인(22)의 밸브(220)를 열고 고압산소 공급라인(21)을 통해 4.5~5기압의 산소를 공급하면 물공급 라인(22)을 통해 상기 증류탱크(10)의 물이 정제 탱크(20) 내부에 위치하는 노즐공(23)으로 분사되며, 이때 고압산소는 물이 정제 탱크(20)내에서 강하게 분사되도록 하는 역할을 한다. When the valve 220 of the water supply line 22 is opened and oxygen of 4.5 to 5 atm is supplied through the high pressure oxygen supply line 21, the water of the distillation tank 10 is purified through the water supply line 22. 20 is injected into the nozzle hole 23 located inside, wherein the high pressure oxygen serves to strongly spray the water in the purification tank (20).

이때 노즐공(23)을 통해 분사된 물과 불순물은 산소가 최대한 공급되는 상태로 미립화 되는데 이 과정에서 물성이 보다 균일해지게 된다.At this time, the water and impurities sprayed through the nozzle hole 23 are atomized in a state where oxygen is supplied as much as possible, and in this process, the physical properties become more uniform.

[여과 공정][Filtration process]

증류 탱크(10)의 물이 모두 정제 탱크(20) 내부에 분사되면 밸브(210)을 작동시켜 고압가스 공급라인(21)를 차단하고 밸브(310)을 열어 여과라인(31)의 여과기(30)로 정제 탱크(20)의 물을 공급하여 불순물을 여과 시킴으로써 3~5ℓ의 옻물을 얻는다.When all the water in the distillation tank 10 is injected into the purification tank 20, the valve 210 is operated to block the high pressure gas supply line 21 and open the valve 310 to filter the filter 30 of the filtration line 31. 3-5 L of lacquer water is obtained by supplying water from the purification tank 20 and filtering impurities.

이와같은 공정을 통해 얻어진 옻물은 증류 공정에서 알러지를 유발하는 우루시올이 완전히 제거되었기 때문에 식품,화장품,음료 및 건강보조식품 등의 원료로 사용할 수 있다.Lacquer water obtained through such a process can be used as a raw material for food, cosmetics, beverages and health supplements because urushiol is completely removed from the distillation process.

또한 우루시올 성분은 암에 효과가 있는 것으로 알려져 있으므로 증류 공정에서 얻어진 우루시올 추출액은 약물 원료로 활용될 수 있을 것으로 기대한다.In addition, since the urushiol component is known to be effective in cancer, the urushiol extract obtained in the distillation process is expected to be used as a drug raw material.

[실시예 1] 옻물 추출과정Example 1 Lacquer Extraction Process

강원도 일대에서 재배한 생옻나무를 5~50㎜ 크기로 절단하고, 절단된 생옻나무 1㎏을 물 8ℓ와 함께 증류탱크에 넣어 1.5기압의 고압산소를 공급하는 동시에 교반하면서 200∼230℃의 온도에서 증류된 우루시올 추출액이 4ℓ가 될 때까지(1시간) 가열한후 증류탱크에 남은 물 4ℓ를 5기압의 고압산소와 함께 정제탱크에 분사 시킨 다음 정제탱크에서 얻을 물을 여과기를 통해 여과 시킴으로써 불순물이 제거된 옻물 4ℓ를 얻었다.Cut the raw lacquer cultivated in Gangwon-do area into 5 ~ 50mm size, and put 1kg of the cut lacquer into 8 distillation tank with 8 liters of water and supply 1.5 atmospheres of high pressure oxygen at the temperature of 200 ~ 230 ℃ while stirring. After heating the distilled urushiol extract to 4ℓ (1 hour), 4 liters of water remaining in the distillation tank is injected into the refinery tank with 5 atm of high pressure oxygen, and the water from the refinery tank is filtered through a filter to remove impurities. 4 liters of removed lacquer was obtained.

[실시예 2] 우루시올 제거 확인 시험Example 2 Urushiol Removal Confirmation Test

우루시올이 제거 되었는지를 확인하기 위하여 실시예 1에서 얻어진 옻물 100㎖를 시료로 채취하여 에테르로 3회 반복하여 추출한다. 추출한 에테르층은 황산소오다로 건조한 다음 농축하여 플레이트 상에서 헥산:에틸아세테이트(8:2 v/v)로 전개하여 우루시올의 존재를 확인한 결과 우루시올이 완전히 제거되었음을 확인할 수 있었다.In order to confirm that urushiol was removed, 100 ml of lacquer obtained in Example 1 was taken as a sample, and extracted three times with ether. The extracted ether layer was dried over sodium sulfate and concentrated to develop hexane: ethyl acetate (8: 2 v / v) on the plate to confirm the presence of urushiol. As a result, it was confirmed that urushiol was completely removed.

[실시예 3] 우루시올 제거 확인 시험Example 3 Urushiol Removal Confirmation Test

증류 공정에서 우루시올이 제거되었는지를 확인하기 위하여 냉각기를 거친 우루시올 추출액 100㎖를 시료로 채취하여 에테르로 추출한다. 에테르층은 황산소오다로 건조한 다음 농축하여 TLC 플레이트 상에서 헥산:에틸아세테이트(8:2 v/v)로 전개하여 우루시올 성분(Rf=4.0)이 다른 성분과 분리됨을 확인하였으며, 그 성분을 확인하기 위하여 컬럼크로마토그래피로 분리하여 HP-Inowax 25m capillary column과 5973 MSD가 장착된 HP-6890 GC를 이용하여 분석한 결과 용출시간이 20~40분 사이에 분자량 314~320을 갖는 여러 종류의 우루시올을 확인할 수 있었다.In order to confirm that urushiol was removed in the distillation process, 100 ml of urushiol extract, which passed through a cooler, was taken as a sample and extracted with ether. The ether layer was dried over sodium sulfate and concentrated to develop hexane: ethyl acetate (8: 2 v / v) on a TLC plate to confirm that the urushiol component (Rf = 4.0) was separated from the other components. After separation by column chromatography and analysis using HP-Inowax 25m capillary column and HP-6890 GC equipped with 5973 MSD, the elution time was identified between 20 and 40 minutes. Could.

[실시예 4] 옻물의 피부에 대한 반응 시험Example 4 Reaction Test on Skin of Lacquer Water

실시예 1에서 얻어진 옻물을 피부에 발라 알러지 반응이 일어나는지 여부를 확인한 결과 전체 53명 모두에서 아무런 이상 증후를 발견할 수 없었다.As a result of applying the lacquer obtained in Example 1 to the skin and checking whether an allergic reaction occurred, no abnormal symptoms were found in all 53 patients.

이와같은 옻물 제조 방법과 그 장치를 이용하여 얻어진 옻물은 다양한 용도로 사용될 수 있으며 본 발명에서는 함침기(41)에서 상기 옻물에 함침된 지류 및 직물재질의 원지(40)를 드라이기(42)로 이송하여 건조시키고 이를 옻물이 공급되는 인쇄 로울러(43)에 통과시켜 무늬가 인쇄되도록 한 인쇄물를 일실시예로 제시한다.The lacquer obtained by using the method and the apparatus for manufacturing such a lacquer can be used for various purposes. In the present invention, the paper 40 of the paper and fabric material impregnated in the lacquer in the impregnator 41 is transferred to the dryer 42. The printed matter is dried and then passed through a printing roller 43 to which a lacquer is supplied so that a pattern is printed.

상기 인쇄물은 지류 및 직물 재질로 벽지,의류 등에 사용된다.The printed matter is used for wallpaper, clothing, etc. as a paper and textile material.

상기와 같이 인쇄 로울러에 의해 인쇄된 옻물은 덧치워지는 부분이 짙게 표현됨으로써 농담으로 질감을 나타내는 수묵화와 같은 시각적 효과를 갖는 벽지를 얻을 수 있었다.As described above, the lacquered water printed by the printing roller was expressed in a darkened portion, thereby obtaining a wallpaper having a visual effect such as ink painting, which expresses the texture in light and shade.

이와같이 본 발명은 건조시키지 않은 생옻나무 조각을 증류탱크 내에서 물과 함께 고압산소로 가압하면서 증류시켜 우루시올을 제거한 다음 고압산소와 함께 정제탱크 내에 분사하여 정제후 여과시킨 옻물을 제공함으로써 알러지 염려없이 다양한 용도로 옻물을 사용할 수 있게 한 효과가 있는 발명이다. Thus, the present invention is to remove the dried lacquer wood by pressing with high pressure oxygen with water in the distillation tank to remove urushiol, and then sprayed in a purification tank with high pressure oxygen to provide filtered lacquer without worrying about allergies It is an invention that has the effect of allowing the use of lacquer for use.

도 1은 본 발명의 옻물 제조장치를 보인 도면1 is a view showing a lacquer manufacturing apparatus of the present invention

도 2는 본 발명의 옻물 인쇄장치를 보인 도면2 is a view showing a lacquer printing apparatus of the present invention

삭제delete

[도면의 주요 부분에 대한 부호의 설명][Description of Symbols for Main Parts of Drawing]

10 : 증류 탱크 11 : 모터10: distillation tank 11: motor

12 : 교반익 13 : 가열수단12: stirring blade 13: heating means

14 : 증기 배출라인 15 : 냉각기14 steam discharge line 15 cooler

16, 21, 32 : 고압산소 공급라인16, 21, 32: high pressure oxygen supply line

22 : 물공급 라인 23 : 노즐공22: water supply line 23: nozzle hole

30 : 여과기 31 : 여과 라인30: filter 31: filtration line

41 : 함침기 42 : 드라이기41: impregnator 42: hair dryer

43 : 인쇄 로울러43: printing roller

Claims (5)

5~50㎜ 크기로 절단된 생옻나무 1㎏에 대하여 물 6~10ℓ를 증류탱크에 넣어 교반익으로 섞어주는 상태에서 150~300℃로 가열하는 증류공정; 상기 증류공정에서 얻은 물을 여과기로 공급하여 불순물을 제거하는 여과공정;으로 이루어진 것에 있어서, 1.5~2.5기압의 고압산소가 증류탱크에 공급되어 생옻나무가 가압되는 상태에서 상기 증류공정이 이루어지고, 상기 증류공정에서 발생된 증기는 냉각기를 통해 3~5ℓ추출해내며, 상기 증류탱크에 남은 물만을 4.5~5기압의 산소와 함께 정제탱크 내에 고압으로 분사하는 정제공정을 더 거친후 여과공정이 이루어지도록 한 것을 특징으로 하는 알러지 유발성분이 제거된 옻물 제조방법.Distillation step of heating to 150 ~ 300 ℃ in the state of mixing 6 ~ 10L of water into a distillation tank for mixing 1 kg of lacquer wood cut into 5 ~ 50㎜ size with a stirring blade; A filtration step of removing impurities by supplying water obtained in the distillation step with a filter; wherein the distillation step is performed while a high pressure oxygen of 1.5 to 2.5 atm is supplied to the distillation tank to pressurize the live lacquer. The steam generated in the distillation process is extracted 3 to 5 L through a cooler, and after the purification process is performed through a refining process in which only water remaining in the distillation tank is sprayed with high pressure into the refining tank with oxygen of 4.5 to 5 atm. Lacquer production method is characterized in that allergens are removed. 모터(11)에 의해 구동되는 교반익(12)이 내부에 설치되고, 외부에는 가열수단(13)이 설치되어 물과 생옻나무가 넣어지는 증류탱크(10); 한쪽이 상기 증류탱크(10)와 연결 설치된 물공급라인(22); 상기 물공급라인(22)의 다른 쪽에 연결 설치된 정제탱크(20); 상기 정제탱크(20)와 여과라인(31)에 의해 연결 설치된 여과기(30);로 이루어진 것에 있어서, 상기 증류탱크(10)에 1.5~2.5기압의 고압산소를 공급하여 생옻나무를 가압하는 고압산소 공급라인(16)과 냉각기(15)가 중간에 설치된 증기 배출라인(14)을 각각 연결 설치하고, 상기 물공급라인(22)의 다른 쪽에는 상기 정제탱크(20) 내부에 위치하는 다수의 노즐공(23)을 형성하며, 상기 물공급라인(22)의 중간에 4.5~5기압의 고압산소를 공급하는 고압산소 공급라인(21)을 연결설치 하여서 된 것을 특징으로 하는 알러지 유발성분이 제거된 옻물 제조장치.A distillation tank 10 in which a stirring vane 12 driven by a motor 11 is installed inside, and a heating means 13 is installed outside so that water and live lacquer are put therein; A water supply line 22 having one side connected to the distillation tank 10; A purification tank 20 connected to the other side of the water supply line 22; High pressure oxygen for pressurizing the raw lacquer tree by supplying high pressure oxygen of 1.5 to 2.5 atm to the distillation tank 10; A plurality of nozzles connected to each of the steam discharge line 14 having a supply line 16 and a cooler 15 interposed therebetween, and located at the other side of the water supply line 22, are located in the purification tank 20. The ball 23 is formed, and the allergen causing component is removed by connecting the high pressure oxygen supply line 21 for supplying the high pressure oxygen of 4.5 to 5 atm in the middle of the water supply line 22. Lacquer manufacturing apparatus. 삭제delete 청구항 2에 있어서, 상기 여과기(30)가 설치된 여과라인(31)에 고압산소 공급라인(32)을 설치하여서 된 것을 특징으로 하는 알러지 성분이 제거된 옻물 제조장치.The method of claim 2, wherein the high pressure oxygen supply line (32) is installed in the filtration line (31) in which the filter (30) is installed, the allergen component is removed lacquer production apparatus. 5~50㎜ 크기로 절단된 생옻나무 1㎏에 대하여 물 6~10ℓ를 증류탱크에 넣고 1.5~2.5기압의 고압산소를 공급하면서 교반익으로 섞어주는 상태에서 150~300℃로 가열하여 발생된 증기를 냉각기를 통해 3~5ℓ추출하는 증류공정; 상기 증류탱크에 남은 물만을 4.5~5기압의 산소와 함께 정제탱크 내에 분사하는 정제공정; 상기 정제탱크의 물을 여과기로 공급하여 불순물을 제거하는 여과공정;을 거쳐 제조된 옻물을 함침기(41)에 공급하여 원지(40)를 옻물에 함침시키고, 함침된 원지(40)를 드라이기(42)에서 건조시킨후 옻물이 공급되는 인쇄 로울러(43)에 통과시켜 무늬가 인쇄되도록 한 알러지 성분이 제거된 옻물을 이용한 인쇄물.Steam generated by heating to 150-300 ℃ while mixing 6-10 liters of water into a distillation tank and supplying 1.5-2.5 atmospheres of high-pressure oxygen and mixing it with stirring blades for 1kg of cut lacquer trees cut to a size of 5-50 mm. Distillation step of extracting 3 to 5 L through a cooler; A purifying step of spraying only the water remaining in the distillation tank together with the oxygen of 4.5 to 5 atm in the refining tank; A filtration step of removing impurities by supplying the water of the purification tank to a filter; supplying the prepared lacquer to the impregnator 41 to impregnate the base paper 40 in the lacquer, and the impregnated base paper 40 to dry. 42) The printed matter using the lacquer from which the allergic component which removed the allergy component which passed through the printing roller 43 which supplies a lacquer is supplied after it was dried in a pattern is printed.
KR1020070111380A 2007-11-02 2007-11-02 Method of manufacturing lacquer with allergen-free components and its manufacturing apparatus and printed matter using this lacquer KR100840212B1 (en)

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KR101185675B1 (en) 2010-07-29 2012-09-24 농업회사법인주식회사자연과미래 Process for the preparation of fabric containing anthocyanin and rhus verniciflua ingredients
KR101635934B1 (en) 2015-04-28 2016-07-04 김려원 Manufacturing method of lacquer water
KR101802258B1 (en) * 2015-11-04 2017-11-29 임태용 extract producing device and producing method for extract
KR102056836B1 (en) * 2018-09-19 2020-01-22 주식회사 비플럭스파머 A method of detoxifying lacquer and a device for detoxifying Lacquer tree

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