KR100480681B1 - Manufacturing method of feed additive - Google Patents
Manufacturing method of feed additive Download PDFInfo
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- KR100480681B1 KR100480681B1 KR10-2001-0050512A KR20010050512A KR100480681B1 KR 100480681 B1 KR100480681 B1 KR 100480681B1 KR 20010050512 A KR20010050512 A KR 20010050512A KR 100480681 B1 KR100480681 B1 KR 100480681B1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
Abstract
본 발명은 부식물질 중에서 풀브산(Fulvic acid) 및 금속착체(金屬錯體)가 유리(遊離)의 상태로 유도되어 있으면서 산화효소가 함유되어있어 자체산화기능, 산화탈취의 촉매의 기능, 유기물질을 부식화기능, 동·식물에 미네랄(Minerals) 공급기능 등을 가지고 있는 활성부식물질(活性腐植物質)을 이용하여 급여가축의 성장속도의 향상, 질병에 대한 내성의 강화, 육질의 향상, 축사환경의 개선 등의 효과를 가져올 수 있는 사료첨가제를 만드는 것을 목적으로 한다.In the present invention, the fluoric acid and the metal complex in the corrosive substance are induced in the free state while containing the oxidase, so that the self-oxidation function, the function of the catalyst of oxidative deodorization, organic substance By using active corrosive substance which has corrosive function and supplying minerals to animals and plants, it improves the growth rate of feedstocks, strengthens resistance to diseases, improves meat quality, and raises The objective is to make feed additives that can bring about environmental benefits.
이를 위하여 풀브산 함량이 높은 해양성 동 ·식물이 퇴적되어 형성된 이탄(토탄)을 산처리를 하여 풀브산을 유리시키고 난 다음 과산화수소(H2O2)와 염화제일철을 가해 산화환원전위(ORP) 값을 +350∼+400mV 범위로 산화하여 활성화시킨 다음 활성화된 미네랄성분이 많은 광물의 분말을 반응시켜 풀브산과산화물의 킬레이트(Chelate)성 미네랄(Minerals)착염 형태의 활성화된 부식물질인 사료첨가제를 만든다.To this end, the peat (peat) formed by the deposition of marine animals and plants with high fulvic acid content was liberated to liberate fulvic acid, and then hydrogen peroxide (H 2 O 2 ) and ferrous chloride were added to the redox potential (ORP). Is activated by oxidizing in the range of +350 to + 400mV, and then reacted with a powder of minerals with a large amount of activated minerals to form a feed additive, an activated corrosive in the form of a chelate mineral complex of fulvic acid peroxide. .
활성화된 부식물질인 사료첨가제는 가축과 같은 동물은 물론이고 식물의 성장에도 여러 가지의 유용한 작용을 하기 때문에 사료첨가제 및 기타 여러 분야에도 다양하게 응용될 것으로 기대한다.It is expected that the feed additive, which is an active corrosive, has various useful effects on the growth of plants as well as animals such as livestock, and thus, it is expected to be applied to a variety of feed additives and other fields.
Description
본 발명은 부식물질이 풀브산(Fulvic acid) 및 금속착체(金屬錯體)가 유리(遊離)의 상태로 유도(誘導)되어 있으면서 산화효소가 함유되어 있어 자체산화기능, 산화탈취의 촉매의 기능, 유기물질을 거대 고분자물질인 부식물질을 생성반응에서 촉매기능, 동·식물에 미네랄(Minerals) 공급기능 등을 가진 활성부식물질을 가축사료에 첨가하여 가축에 급여함으로서 가축의 성장속도 향상, 육질의 개선, 축사환경의 개선, 가축의 질병에 대한 내성의 증진 등의 효과를 가져올 수 있는 사료첨가제를 제조하는 방법에 관한 것이다.In the present invention, the oxidizing agent is contained while the corrosive substance is induced in the free state of the fulvic acid and the metal complex. In addition, it is possible to increase the growth rate of livestock by feeding active corrosive materials with catalysis function and supplying minerals to animals and plants in livestock feed by producing organic materials as corrosive substances that are macromolecules. The present invention relates to a method for preparing a feed additive that can bring about effects such as improving the quality of livestock, improving the livestock environment, and improving resistance to livestock diseases.
일본 공개특허공보 평(平) 1-240152호에서는 식물성 이탄을 공기와 충분히 접촉하여 활성화한 것을 사료 첨가제로 이용하였으나 일반 이탄의 경우 공기접촉만으로는 활성화가 되지 않으면서 킬레이트(Chelate)성 미네랄(Minerals)착염 성분의 형성이 적기 때문에 효과가 떨어져 상업적인 가치가 없었다.In Japanese Unexamined Patent Application Publication No. 1-240152, vegetable peat has been activated in sufficient contact with air as a feed additive. However, in general peat, chelate minerals are not activated by air contact alone. Due to the low formation of complexing components, the effect was not commercially viable.
또한, 일본 공개특허공보 평(平) 3-58753, 262444호와 평(平) 4-40858호 역시 활성부식물질 생성메커니즘(Mechanism)을 정확하게 파악되지 않은 상태에서 일반 부식물질을 처리한 것으로 일본 나가사키현(長崎縣)의 가라고(唐比) 습지에서 출토되는 천연산 활성부식물질보다 성능이 월등히 떨어져 상업화가 되지 못하고 있다.In addition, Japanese Laid-Open Patent Publications Hei 3-58753, 262444 and Hei 4-40858 have also dealt with general corrosive substances without knowing the mechanism of formation of active corrosive substances. It is not commercialized because its performance is much lower than that of the natural active corrosive material excavated from the Karago wetland in the prefecture.
본 발명에서는 이탄 중에서 풀브산(Fulvic acid) 함량이 높은 해양성 규조류, 플랑크톤(Plankton), 해초와 같은 해양성 동·식물이 퇴적되어 생성된 부식물질을 pH 2이하로 산(황산, 염산)처리를 하여 풀브산을 유리(遊離)시킨 다음, 과산화수소(H2O2)와 황산제일철(FeSO4)을 주입하여 산화환원전위(ORP ; Oxidation Reduction Potential) 값이 +350∼+400mV범위로 조정한 것에 활성화 미네랄성분이 많은 유문암질(流紋巖質)이나 대사이드(Dacite)질의 화산회토나 부석(경석)을 분쇄한 분말 또는 석탄회(Fly-ash)를 산성수용액에서 고온(90∼100℃)처리를 하여 알로페인(Allophane)질광물인 비정질함수알루미늄규산염(Hydrate non-crystalline Alumino-silicate)으로 전환한 것을 혼합하여 킬레이트성과산화풀브산미네랄착화합물인 활성부식물질을 만들어 사료에 0.006∼0.1% 정도 혼합하여 급여하면, 성장속도의 향상, 장내 유용미생물로 정균작용이 일어나므로 질병에 대한 내성이 강화되면서 배설분에서 악취가 저감되므로 축사환경개선효과를 가져오면서 육질이 개선될 수 있다.In the present invention, by treating acid (sulfuric acid, hydrochloric acid) with a pH of 2 or less, the corrosives formed by depositing marine animals and plants such as marine diatoms, plankton, and seaweeds with high Fulvic acid content in peat are deposited. It is activated by releasing fulvic acid and adjusting Oxidation Reduction Potential (ORP) in the range of +350 to +400 mV by injecting hydrogen peroxide (H 2 O 2 ) and ferrous sulfate (FeSO 4 ). Powder or fly ash obtained by pulverizing rhodolite or Dacite-rich volcanic ash or pumice which is rich in minerals is treated with high temperature (90-100 ℃) in acidic aqueous solution. It is mixed with the conversion of allophane quaternary mineral, amorphous non-crystalline alumino-silicate, to make active corrosive substance which is chelate and mineral oxide complex of fulbrate oxide. if, The growth rate, bacteriostatic action occurs as a useful microorganism in the intestine, so that resistance to disease is enhanced and odor is reduced in excreta. Therefore, meat quality can be improved while bringing an improvement effect on the livestock environment.
본 발명의 목적은 가축의 성장속도가 향상, 질병에 의한 사고율의 저하, 육질의 개선, 축사환경의 개선 등의 효과를 가져올 수 있는 사료첨가제를 만들고자 한다.An object of the present invention is to create a feed additive that can bring about the effect of improving the growth rate of livestock, lowering the accident rate due to disease, improving the meat quality, improving the livestock environment.
본 발명에서 사료첨가제로 이용하는 활성부식물질의 의미와 사료적인 특성을 보면 다음과 같다.Looking at the meaning and feed characteristics of the active corrosive material used as feed additive in the present invention.
그리고, 다음 제조방법 및 실시 예에서 "부"는 무게단위의 "부"를 의미한다.In the following manufacturing method and examples, "part" means "part" of the weight unit.
천연에서 출토되고 있는 전형적인 활성부식토는 일본 나가사키현(長崎縣)의 가라고(唐比)의 함몰(陷沒)습지에서 출토되고 있는데, 이 가라고 습지의 이탄(泥炭)은 해양성규조류, 플랑크톤, 해초와 같은 해양성 동 ·식물과 갈대, 연꽃과 같은 수생식물이 인근 운젠(雲仙) 활화산군의 화산활동에서 분출된 대사이드(Dacite)질 화산회와 혼합 퇴적되어 활성화된 규소와 알루미늄(Aluminium)이 물과 가수분해반응에 의해 방출된 수소이온(H+)에 의해 pH가 2.3정도의 산성의 부식토로 되어 풀브산(Fulvic acid)이 유리(遊離)상태로 유도(誘導)되면서 대사이드(Dacite)질 화산회 중 활성화된 미네랄과 반응하여 킬레이트성풀브산미네랄착염의 상태로 되었으며, 또한 외부와 폐쇄된 함몰습지로 유기물질이 부식화과정에서 생성된 과산화수소(H2O2)와 제일철의 촉매작용에 의해서 킬레이트성과산화풀브산미네랄착염 형태인 활성화된 부식물질의 형태로 존재한다.Typical active corrosive soils excavated from nature are excavated from the sinking wetlands of Kagora in Nagasaki Prefecture, Japan. Aquatic plants, such as marine animals, plants, reeds, and lotus flowers are mixed and deposited with the Dacite-like volcanic ash from the volcanic activity of the nearby Unzen active volcanoes. Hydrogen ions (H + ) released by decomposition result in acidic caustic soils with an pH of about 2.3, leading to the liberation of fulvic acid into the free state. the reaction was activated minerals and to the state of the chelating seongpul beusan mineral complex salts, and the catalytic action to the recessed marsh closed and the outside of the organic material is generated by the corrosion development process hydrogen peroxide (H 2 O 2) and ferrous It is present in the form of the active substance chelate corrosion and oxidation pool beusan mineral complex form.
이와 같은 활성화된 부식물질의 사료적인 측면에서 특성은 다음과 같다.The feed characteristics of such activated corrosives are as follows.
①킬레이트성과산화풀브산미네랄착염은 동 ·식물의 성장에 필요한 미네랄 공급이 용이하므로써 성장속도를 향상시킨다.① Chelate and oxidized fulbrate mineral complex improve the growth rate by easily supplying minerals necessary for the growth of animals and plants.
②풀브산과산화물은 산화환원전위값이 낮을 때 활발한 대사활동을 하는 부패 및 변패성미생물이나 유해병원성미생물의 생육을 억제시키면서 유기물을 부식물질로 전환하는 부식화미생물과 이들 미생물과 상호공생관계에 있는 유용미생물의 생육에 적합한 환경분위기를 조성하므로서 급여가축의 장내 정균작용이 일어나 질병에 대한 내성이 강화된다.② Fulvic acid peroxide is a corrosive microorganism that correlates with these microorganisms and corrosive microorganisms that convert organic matter into corrosive substances while suppressing the growth of decaying and degrading microorganisms or harmful pathogenic microorganisms that actively perform metabolic activity when the redox potential is low. By creating an environment suitable for the growth of useful microorganisms, the intestinal bacteriostatic action of feed livestock occurs, resulting in increased resistance to disease.
③동·식물의 생육에 도움을 주는 생리활성물질인 비타민(Vitamin)류, 성장촉진물질인 호르몬(Hormone), 유해병원성미생물의 생육을 억제하는 항생물질 등이 함유되어 있어 성장이 향상되면서 질병에 대한 예방효과가 있다.③ Vitamins (Vitamin), a bioactive substance that helps the growth of animals and plants, hormones (Hormone), which are growth promoting substances, and antibiotics that inhibit the growth of harmful pathogenic microorganisms. It has a preventive effect.
④악취발생물질인 암모니아(Ammonia), 유화수소, 휘발성아민, 휘발성유기산, 메르캅탄(Mercaptan)과 같은 물질을 활성부식물질은 물에 불용성이면서 비휘발성물질인 부식전구물질(腐植前驅物質)에 부동화(不動化)됨으로서 배설분에서 악취발생이 저감되므로 축사환경의 개선효과가 있다.④ Passivates substances such as ammonia, hydrogen sulfide, volatile amines, volatile organic acids, and mercaptan, which are odor generating substances, to corrosive precursors, which are insoluble in water and nonvolatile. As a result, the odor is reduced in the excreta powder, which improves the barn environment.
⑤상온에서 액상인 오레인산(Oleic acid), 리노린산(Linoleic acid)과 같은 불포화지방산을 상온에서 고체인 포화지방산이나 공역지방산으로 전환하므로서 돼지의 경우 상강육(霜降肉)형성이 형성되면서 등지방두께가 적어져 육질이 개선된다.⑤ By converting unsaturated fatty acids such as oleic acid and linoleic acid, which are liquid at room temperature, into saturated fatty acid or conjugated fatty acid, which are solid at room temperature, pigs are formed as upper limbs are formed. Less thickness will improve meat quality.
또한, 소화흡수효율이 향상되므로 사료이용효율이 향상된다.In addition, since the digestive absorption efficiency is improved, the feed utilization efficiency is improved.
본 발명에서는 상기의 목적을 달성하기 위하여 전술한 활성부식물질의 특성을 감안하여 풀브산 함량이 많은 해양성 규조류, 플랑크톤, 해초 등의 해양성 동 ·식물이 퇴적되어 생성된 자연산 이탄 100부에 산을 처리하여 pH를 2이하로 하여 풀브산을 유리(遊離)의 상태로 유도(誘導)한다.In the present invention, in order to achieve the above object, the acid is treated to 100 parts of natural peat produced by depositing marine animals and plants such as marine diatoms, plankton, and seaweed with high fulvic acid content in view of the characteristics of the active corrosive materials described above. The pH is set to 2 or less to induce the fulvic acid to a free state.
여기에 과산화수소(H2O2)와 황산제일철(FeSO4)을 당량 대 당량으로 혼합한 용액을 주입하여 산화환원전위(ORP)값이 +350∼+400mV 범위가 되게 혼합교반을 하여 유리상태의 풀브산과산화물(Peroxyfulvic acid)을 만든다.Into this solution, a mixture of hydrogen peroxide (H 2 O 2 ) and ferrous sulfate (FeSO 4 ) was added in an equivalent weight equivalent to the mixture. The mixture was stirred so that the redox potential (ORP) was in the range of +350 to +400 mV. Produces peroxyfulvic acid.
그리고, 활성화미네랄(Activated minerals)성분의 함량이 높은 유문암질(流紋巖質)이나 대사이드(Dacite)질의 화산회토나 이들 광물의 부석을 분쇄한 분말 또는 석탄회(Fly-ash)를 pH 2이하의 산성 수용액에서 고온(90∼100℃)으로 처리하여 비정질함수(非晶質含水)의 규산알루미늄염(Aluminosilicate)인 활성화미네랄성분이 많은 알로페인(Allophane)질 광물질로 전환한 것을 건량기준으로 50~55부를 혼합한 후에 2주에 1∼2회정도 뒤집기를 하면서 3∼4개월 이상 방치하여 풀브산과산화물의 킬레이트성풀브산미네랄착염상태의 활성부식물질인 사료첨가제를 제조한다.Also, powder or fly ash obtained by pulverizing rhyolite or Daecite volcanic ash, which have high content of activated minerals, or pumice of these minerals, can be used at pH 2 or below. 50 ~ on a dry basis, which was converted to an allophane mineral with a large amount of activated mineral, an aluminum silicate of amorphous function, treated at high temperature (90 ~ 100 ℃) in an acidic aqueous solution. After mixing 55 parts, the mixture is inverted once or twice in two weeks and left for 3 to 4 months to prepare a feed additive which is an active corrosive substance in the chelated fulic acid mineral complex salt of fulvic acid peroxide.
또는, 일본 나가사키(長崎縣)의 가라고(唐比) 습지에서와 같은 천연의 활성부식물질의 경우에도 산화환원전위(ORP) 값이 +250mV 이하인 경우에는 과산화수소(H2O2)와 황산제일철(FeSO4)을 가해서 산화환원전위(ORP) 값이 +350∼+400mV로 조정하여 활성도를 높인다.Alternatively, even in the case of natural active corrosive substances, such as in the Kago Wetlands of Nagasaki, Japan, hydrogen peroxide (H 2 O 2 ) and ferrous sulfate (ORP) when the ORP value is less than +250 mV. FeSO 4 ) is added to adjust the redox potential (ORP) to +350 to +400 mV to increase the activity.
이상과 같은 사료첨가제(활성부식물질)를 소, 돼지, 닭, 오리와 같은 가축이나 물고기의 사료에 0.006∼0.1% 정도 혼합하여 급여한다.Feed additives (active corrosive substances) as described above are fed to feed of livestock or fish such as cattle, pigs, chickens, ducks, etc. 0.006 ~ 0.1%.
[실시 예1]Example 1
비육돈을 30㎏에서 110㎏까지 사육하는 기간에 배합사료에 전술한 활성부식물질을 표1에서와 같이 각각 혼합한 사료와 활성부식물질을 첨가하지 않은(무첨가)사료를 급여하여 사육한 결과 사육일수 및 도축결과 A, B등급의 비율은 표 1의 내용과 같다.In the period of raising 30 kg to 110 kg of pigs, the number of days of breeding was obtained by feeding the above-mentioned active corrosive to the blended feed and feed without the active corrosive (additive-free), respectively, as shown in Table 1. The ratios of A and B grades are shown in Table 1.
[실시 예2]Example 2
젖소에 표2에서와 같이 활성부식물질을 사료에 첨가하여 젖소에 급여한 결과 우유생산 증가율은 표 2의 내용과 같다.As shown in Table 2, the increase in milk production as a result of feeding the active corrosive to the feed and feeding the cows is shown in Table 2.
실시 예에서와 같이 활성부식물질의 첨가량이 0.0006% 이하에서는 효과가 거의 없었으며, 0.1%이상에서도 효과가 감소하였다.As in Example, the amount of active corrosive added was less than 0.0006%, and the effect was decreased even at 0.1% or more.
그리고, 활성부식토를 급여한 가축의 분에서는 악취발생이 저감하였다.Odor generation was reduced in the livestock fed the active corrosive soil.
비육돈의 경우 무첨가 돈사에서는 암모니아(NH3) 농도가 12ppm 이상으로 심한 악취를 발생하였으나 활성부식물질을 0.05%정도를 사료첨가제로 혼합하여 급여한 돈사에서는 암모니아 농도가 2∼3ppm으로 감소되었다.In the case of finishing pigs, ammonia (NH 3 ) concentration was more than 12ppm in non-added pigs, but ammonia concentration was reduced to 2-3ppm in pigs fed 0.05% of active corrosive with feed additives.
전술한 기술내용으로부터 자명하듯이, 활성부식물질을 가축의 사료첨가제로 사료와 혼합하여 급여하면 성장속도의 향상, 육질의 개선, 악취발생이 저감되므로서 축사환경의 개선 등의 효과가 있기 때문에 사료첨가제로 널리 보급될 것으로 기대된다.As is apparent from the foregoing description, when the active corrosive material is mixed with the feed as a feed additive for livestock, the feed is improved because the growth rate, the quality of the meat, and the odor are reduced, thereby improving the livestock environment. It is expected to be widely used as an additive.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100554214B1 (en) | 2005-07-20 | 2006-02-24 | 노영빈 | Composition of feed supplements containing herbaceous peat and animal products using it |
| WO2011078891A1 (en) * | 2009-12-22 | 2011-06-30 | Ralco Nutrition, Inc. | Organically chelated mineral compositions and methods thereof |
| US10570066B2 (en) | 2014-04-17 | 2020-02-25 | Ralco Nutrition, Inc. | Agricultural compositions and applications utilizing mineral compounds |
| RU2817566C1 (en) * | 2023-10-10 | 2024-04-16 | Общество с ограниченной ответственностью "Сибурметахим" | Method of producing a therapeutic fodder additive from peat |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100473516B1 (en) * | 2001-08-22 | 2005-03-10 | 서희동 | Manufacturing method for soil conditioner by using activated humic substances and clay minerals |
| KR100464865B1 (en) * | 2002-04-20 | 2005-01-06 | 서희동 | Using method of purifying agent for sewage, wastewater, night-soil, red tide, green algal ... etc from fly ash or cinder |
| US20080044548A1 (en) * | 2003-09-04 | 2008-02-21 | Hale Edward C Iii | Animal feed and methods for reducing ammonia and phosphorus levels in manure |
| US7713562B2 (en) | 2003-09-04 | 2010-05-11 | Rose Acre Farms, Inc. | Animal feed and methods for reducing ammonia and phosphorus levels in manure |
| CN107362174A (en) * | 2016-05-12 | 2017-11-21 | 吴政宏 | Fulvic acid is preparing treatment or prevention by the shrimp of bacterium infection or the purposes of the feed of fish and/or preparation |
| RU2741090C1 (en) * | 2020-09-14 | 2021-01-22 | Общество с ограниченной ответственностью «РОСТОДАР» | Method of producing an organomineral additive |
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|---|---|---|---|---|
| WO1981002888A1 (en) * | 1980-04-03 | 1981-10-15 | Oxfam | Treatment of activated or humus sludge |
| JPS56134966A (en) * | 1980-03-21 | 1981-10-22 | Keikichi Oohira | Feed made from peat |
| JPS63123347A (en) * | 1986-11-12 | 1988-05-27 | Risaku Shimoda | Preparation of feed for larva of beetle |
| JPH10327771A (en) * | 1997-06-03 | 1998-12-15 | Green Karuchiyaa:Kk | Feed additive for fish and its use |
| JPH11157970A (en) * | 1997-09-18 | 1999-06-15 | Tadashi Miyamoto | Production of fertilizer using organic waste as stock |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56134966A (en) * | 1980-03-21 | 1981-10-22 | Keikichi Oohira | Feed made from peat |
| WO1981002888A1 (en) * | 1980-04-03 | 1981-10-15 | Oxfam | Treatment of activated or humus sludge |
| JPS63123347A (en) * | 1986-11-12 | 1988-05-27 | Risaku Shimoda | Preparation of feed for larva of beetle |
| JPH10327771A (en) * | 1997-06-03 | 1998-12-15 | Green Karuchiyaa:Kk | Feed additive for fish and its use |
| JPH11157970A (en) * | 1997-09-18 | 1999-06-15 | Tadashi Miyamoto | Production of fertilizer using organic waste as stock |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100554214B1 (en) | 2005-07-20 | 2006-02-24 | 노영빈 | Composition of feed supplements containing herbaceous peat and animal products using it |
| WO2011078891A1 (en) * | 2009-12-22 | 2011-06-30 | Ralco Nutrition, Inc. | Organically chelated mineral compositions and methods thereof |
| US10696602B2 (en) | 2009-12-22 | 2020-06-30 | Ralco Nutrition, Inc. | Organically chelated mineral compositions and methods thereof |
| US11078127B2 (en) | 2009-12-22 | 2021-08-03 | Ralco Nutrition, Inc. | Organically chelated mineral compositions and methods thereof |
| US10570066B2 (en) | 2014-04-17 | 2020-02-25 | Ralco Nutrition, Inc. | Agricultural compositions and applications utilizing mineral compounds |
| RU2817566C1 (en) * | 2023-10-10 | 2024-04-16 | Общество с ограниченной ответственностью "Сибурметахим" | Method of producing a therapeutic fodder additive from peat |
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