JPS6472978A - Production of calcium phosphate ceramics having porous surface - Google Patents

Production of calcium phosphate ceramics having porous surface

Info

Publication number
JPS6472978A
JPS6472978A JP62230747A JP23074787A JPS6472978A JP S6472978 A JPS6472978 A JP S6472978A JP 62230747 A JP62230747 A JP 62230747A JP 23074787 A JP23074787 A JP 23074787A JP S6472978 A JPS6472978 A JP S6472978A
Authority
JP
Japan
Prior art keywords
calcium phosphate
phosphate ceramics
porous surface
production
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP62230747A
Other languages
English (en)
Other versions
JP2572606B2 (ja
Inventor
Yasuhiko Hirayama
Tetsuro Ogawa
Satoshi Kojima
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pentax Corp
Original Assignee
Asahi Kogaku Kogyo Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Kogaku Kogyo Co Ltd filed Critical Asahi Kogaku Kogyo Co Ltd
Priority to JP62230747A priority Critical patent/JP2572606B2/ja
Priority to GB8821501A priority patent/GB2209746B/en
Priority to DE3831260A priority patent/DE3831260A1/de
Publication of JPS6472978A publication Critical patent/JPS6472978A/ja
Priority to US07/511,814 priority patent/US5017518A/en
Application granted granted Critical
Publication of JP2572606B2 publication Critical patent/JP2572606B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/447—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/50—Preparations specially adapted for dental root treatment
    • A61K6/58—Preparations specially adapted for dental root treatment specially adapted for dental implants
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/70—Preparations for dentistry comprising inorganic additives
    • A61K6/71—Fillers
    • A61K6/74—Fillers comprising phosphorus-containing compounds
    • A61K6/75—Apatite
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/80—Preparations for artificial teeth, for filling teeth or for capping teeth
    • A61K6/849—Preparations for artificial teeth, for filling teeth or for capping teeth comprising inorganic cements
    • A61K6/864—Phosphate cements
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/02—Inorganic materials
    • A61L27/12—Phosphorus-containing materials, e.g. apatite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/048—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing phosphorus, e.g. phosphates, apatites, hydroxyapatites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/04—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by dissolving-out added substances
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/53—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone involving the removal of at least part of the materials of the treated article, e.g. etching, drying of hardened concrete
    • C04B41/5338—Etching
    • C04B41/5353—Wet etching, e.g. with etchants dissolved in organic solvents
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/91—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics involving the removal of part of the materials of the treated articles, e.g. etching
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F2310/00—Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
    • A61F2310/00005—The prosthesis being constructed from a particular material
    • A61F2310/00179—Ceramics or ceramic-like structures
    • A61F2310/00293—Ceramics or ceramic-like structures containing a phosphorus-containing compound, e.g. apatite
JP62230747A 1987-09-14 1987-09-14 表面多孔質なリン酸カルシウム系セラミックスの製造法 Expired - Fee Related JP2572606B2 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP62230747A JP2572606B2 (ja) 1987-09-14 1987-09-14 表面多孔質なリン酸カルシウム系セラミックスの製造法
GB8821501A GB2209746B (en) 1987-09-14 1988-09-14 Process for producing calcium phosphate ceramics having porous surface
DE3831260A DE3831260A1 (de) 1987-09-14 1988-09-14 Verfahren zur herstellung von calciumphosphat-keramik mit poroeser oberflaeche
US07/511,814 US5017518A (en) 1987-09-14 1990-04-18 Process for producing calcium phosphate ceramics having porous surface

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62230747A JP2572606B2 (ja) 1987-09-14 1987-09-14 表面多孔質なリン酸カルシウム系セラミックスの製造法

Publications (2)

Publication Number Publication Date
JPS6472978A true JPS6472978A (en) 1989-03-17
JP2572606B2 JP2572606B2 (ja) 1997-01-16

Family

ID=16912656

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62230747A Expired - Fee Related JP2572606B2 (ja) 1987-09-14 1987-09-14 表面多孔質なリン酸カルシウム系セラミックスの製造法

Country Status (4)

Country Link
US (1) US5017518A (ja)
JP (1) JP2572606B2 (ja)
DE (1) DE3831260A1 (ja)
GB (1) GB2209746B (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5215941A (en) * 1989-11-10 1993-06-01 Asahi Kogaku Kogyo K.K. Process for producing a sintered apatite article having a porous surface using an acidic buffer solution
JP2010523232A (ja) * 2007-04-13 2010-07-15 ドクトル．ハー．ツェー．ロベルト マシーズ スティフツング パイロジェンフリーのリン酸カルシウムの生産方法

Families Citing this family (47)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6002065A (en) * 1988-04-20 1999-12-14 Norian Corporation Kits for preparing calcium phosphate minerals
DE3935060C2 (de) * 1989-10-20 1996-05-30 Herbst Bremer Goldschlaegerei Verfahren zur Herstellung eines keramischen Materials für den Dentalbereich und eine Verwendung desselben
JP2978203B2 (ja) * 1990-04-20 1999-11-15 日本特殊陶業株式会社 生体活性な表面層を有するセラミックス体の製造方法
DE4113021C2 (de) * 1991-04-20 1995-01-26 Carus Carl Gustav Resorbierbare Phosphatgläser und resorbierbare Phosphatglaskeramiken, Verfahren zu ihrer Herstellung und Verwendung
US5338356A (en) * 1991-10-29 1994-08-16 Mitsubishi Materials Corporation Calcium phosphate granular cement and method for producing same
JPH05124919A (ja) * 1991-11-05 1993-05-21 Sangi Co Ltd 抗菌性セラミツクス
US5534031A (en) * 1992-01-28 1996-07-09 Asahi Kogaku Kogyo Kabushiki Kaisha Prosthesis for spanning a space formed upon removal of an intervertebral disk
US5776233A (en) * 1992-04-24 1998-07-07 Bego Bremer Goldschlagerei Wilh. Herbst Gmbh & Co. Process for preparing a ceramic material for use in dental fillings and dental crowns
FR2697243A1 (fr) * 1992-10-26 1994-04-29 Commissariat Energie Atomique Procédé de préparation de pièces microporeuses en phosphate de calcium comprenant de l'hydroxylapatite, à microporosité contrôlée, et pièces obtenues par ce procédé.
DE4302072A1 (de) * 1993-01-26 1994-07-28 Herbst Bremer Goldschlaegerei Keramisches Material für Zahnfüllungen und/oder Zahnersatz und Verfahren zur Herstellung desselben
DE4423826B4 (de) * 1993-07-07 2007-01-04 Pentax Corp. Keramische Wirbelprothese
US5531794A (en) * 1993-09-13 1996-07-02 Asahi Kogaku Kogyo Kabushiki Kaisha Ceramic device providing an environment for the promotion and formation of new bone
DE4416127C2 (de) * 1994-05-06 2000-11-30 Heidelberger Druckmasch Ag Reinigungsvorrichtung für Zylinder einer Druckmaschine
JP3689146B2 (ja) * 1995-05-30 2005-08-31 ペンタックス株式会社 骨へのスクリュー固定用素子
DE19627924C2 (de) * 1996-06-21 2003-02-20 Michael Kuehn Verfahren und Mischung zur Herstellung eines selbsttragenden Werkstoffs sowie Werkstoff
DE19630034A1 (de) * 1996-07-25 1998-04-23 Huels Chemische Werke Ag Biohybrides Zahnimplantat
US5858318A (en) * 1996-11-27 1999-01-12 Luo; Ping Methods of synthesizing hydroxyapatite powders and bulk materials
JP3679570B2 (ja) 1997-03-14 2005-08-03 ペンタックス株式会社 骨補填材及びその製造方法
AU766735B2 (en) 1998-09-15 2003-10-23 Isotis N.V. Osteoinduction
DE19852783B4 (de) * 1998-11-16 2006-04-13 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Kristalline poröse Festkörper
US6840995B2 (en) * 1999-07-14 2005-01-11 Calcitec, Inc. Process for producing fast-setting, bioresorbable calcium phosphate cements
US6960249B2 (en) * 1999-07-14 2005-11-01 Calcitec, Inc. Tetracalcium phosphate (TTCP) having calcium phosphate whisker on surface
US7270705B2 (en) 1999-07-14 2007-09-18 Jiin-Huey Chern Lin Method of increasing working time of tetracalcium phosphate cement paste
US7094282B2 (en) * 2000-07-13 2006-08-22 Calcitec, Inc. Calcium phosphate cement, use and preparation thereof
US7169373B2 (en) * 1999-07-14 2007-01-30 Calcitec, Inc. Tetracalcium phosphate (TTCP) having calcium phosphate whisker on surface and process for preparing the same
US6338752B1 (en) * 2000-04-20 2002-01-15 Purzer Pharmaceutical Co., Ltd. α-TCP/HAP biphasic cement and its preparing process
US7156915B2 (en) * 2000-07-13 2007-01-02 Calcitec, Inc. Tetracalcium phosphate (TTCP) with surface whiskers and method of making same
US7204876B2 (en) * 2000-07-13 2007-04-17 Calcitec, Inc. Calcium phosphate cements made from (TTCP) with surface whiskers and process for preparing same
US6713420B2 (en) * 2000-10-13 2004-03-30 Toshiba Ceramics Co., Ltd. Porous ceramics body for in vivo or in vitro use
JP4070951B2 (ja) * 2000-12-07 2008-04-02 ペンタックス株式会社 多孔質リン酸カルシウム系セラミックス焼結体の製造方法
US6949251B2 (en) * 2001-03-02 2005-09-27 Stryker Corporation Porous β-tricalcium phosphate granules for regeneration of bone tissue
US20030216777A1 (en) * 2002-05-16 2003-11-20 Yin-Chun Tien Method of enhancing healing of interfacial gap between bone and tendon or ligament
JP4680771B2 (ja) * 2003-05-26 2011-05-11 Ｈｏｙａ株式会社 リン酸カルシウム含有複合多孔体及びその製造方法
MXPA05014103A (es) * 2003-06-24 2006-05-25 Kyushu Tlo Co Ltd Material sustituido de hueso para uso medico y metodo para producir el mismo.
US7163651B2 (en) * 2004-02-19 2007-01-16 Calcitec, Inc. Method for making a porous calcium phosphate article
US6994726B2 (en) * 2004-05-25 2006-02-07 Calcitec, Inc. Dual function prosthetic bone implant and method for preparing the same
US7118705B2 (en) 2003-08-05 2006-10-10 Calcitec, Inc. Method for making a molded calcium phosphate article
EP1686934B1 (en) * 2003-11-07 2020-03-18 Vivex Biologics Group, Inc. Injectable bone substitute
JP4643166B2 (ja) * 2004-03-30 2011-03-02 独立行政法人物質・材料研究機構 アパタイト／コラーゲン複合体繊維を含む多孔体の平均気孔径制御方法
CA2564605A1 (en) * 2004-05-12 2005-12-01 Massachusetts Institute Of Technology Manufacturing process, such as three-dimensional printing, including solvent vapor filming and the like
US8025903B2 (en) 2005-09-09 2011-09-27 Wright Medical Technology, Inc. Composite bone graft substitute cement and articles produced therefrom
WO2007030616A2 (en) * 2005-09-09 2007-03-15 Wright Medical Technology, Inc. Composite bone graft substitute cement and articles produced therefrom
CA2642830A1 (en) * 2006-02-17 2007-08-23 Progentix Orthobiology B.V. Osteoinductive calcium phosphates
CN102046238A (zh) * 2008-05-30 2011-05-04 皇家飞利浦电子股份有限公司 可植入连接装置
WO2011143226A1 (en) 2010-05-11 2011-11-17 Howmedica Osteonics Corp. Organophosphorous, multivalent metal compounds, & polymer adhesive interpenetrating network compositions & methods
US8765189B2 (en) 2011-05-13 2014-07-01 Howmedica Osteonic Corp. Organophosphorous and multivalent metal compound compositions and methods
TWI651103B (zh) 2013-12-13 2019-02-21 萊特醫技股份有限公司 多相骨移植替代材料

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US3929971A (en) * 1973-03-30 1975-12-30 Research Corp Porous biomaterials and method of making same
US4207306A (en) * 1974-08-02 1980-06-10 Sterling Drug Inc. Process for producing polycrystalline ceramic oxides
US4308064A (en) * 1978-10-19 1981-12-29 Ngk Spark Plugs Co., Ltd. Phosphate of calcium ceramics
JPS577856A (en) * 1980-06-13 1982-01-16 Mitsubishi Mining & Cement Co Manufacture of calcium phosphate porous body
JPS5883605A (ja) * 1981-11-13 1983-05-19 Takuro Ishibashi 歯科用セメント組成物とその製法
JPS59182263A (ja) * 1983-03-31 1984-10-17 科学技術庁無機材質研究所長 リン酸カルシウム質セメント硬化物の生成法
US4626392A (en) * 1984-03-28 1986-12-02 Ngk Spark Plug Co., Ltd. Process for producing ceramic body for surgical implantation
US4693986A (en) * 1985-06-25 1987-09-15 Orthomatrix, Inc. Ceramic process and products
JPS62153204A (ja) * 1985-12-27 1987-07-08 Advance Res & Dev Co Ltd 歯科用根管充填材
DD258713A3 (de) * 1986-03-14 1988-08-03 Akad Wissenschaften Ddr Calciumphosphathaltiger, biokompatibler schichtkoerper und verfahren zu seiner herstellung

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5215941A (en) * 1989-11-10 1993-06-01 Asahi Kogaku Kogyo K.K. Process for producing a sintered apatite article having a porous surface using an acidic buffer solution
JP2010523232A (ja) * 2007-04-13 2010-07-15 ドクトル．ハー．ツェー．ロベルト マシーズ スティフツング パイロジェンフリーのリン酸カルシウムの生産方法

Also Published As

Publication number Publication date
GB2209746B (en) 1991-04-17
JP2572606B2 (ja) 1997-01-16
DE3831260C2 (ja) 1993-05-19
DE3831260A1 (de) 1989-03-23
US5017518A (en) 1991-05-21
GB8821501D0 (en) 1988-10-12
GB2209746A (en) 1989-05-24

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Legal Events

Date Code Title Description
LAPS Cancellation because of no payment of annual fees