JPS6377942A - シリコ−ンゴム粒状物の製造方法 - Google Patents
シリコ−ンゴム粒状物の製造方法Info
- Publication number
- JPS6377942A JPS6377942A JP22450086A JP22450086A JPS6377942A JP S6377942 A JPS6377942 A JP S6377942A JP 22450086 A JP22450086 A JP 22450086A JP 22450086 A JP22450086 A JP 22450086A JP S6377942 A JPS6377942 A JP S6377942A
- Authority
- JP
- Japan
- Prior art keywords
- silicone rubber
- liquid
- water
- dispersion
- component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002379 silicone rubber Polymers 0.000 title claims abstract description 54
- 239000004945 silicone rubber Substances 0.000 title claims abstract description 22
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 239000004944 Liquid Silicone Rubber Substances 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000006185 dispersion Substances 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 20
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims abstract description 20
- 125000003342 alkenyl group Chemical group 0.000 claims abstract description 17
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 16
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims abstract description 13
- 229910052697 platinum Inorganic materials 0.000 claims abstract description 9
- 239000003054 catalyst Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 54
- 239000008187 granular material Substances 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- -1 liquid paraffin Substances 0.000 abstract description 23
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 2
- 229940057995 liquid paraffin Drugs 0.000 abstract description 2
- 239000001993 wax Substances 0.000 abstract description 2
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 229920001577 copolymer Polymers 0.000 description 11
- 238000000034 method Methods 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 239000002253 acid Substances 0.000 description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 238000007259 addition reaction Methods 0.000 description 6
- 239000004205 dimethyl polysiloxane Substances 0.000 description 5
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 5
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 5
- 239000004094 surface-active agent Substances 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 150000001451 organic peroxides Chemical class 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000003431 cross linking reagent Substances 0.000 description 3
- 238000010292 electrical insulation Methods 0.000 description 3
- 229910021485 fumed silica Inorganic materials 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000002075 main ingredient Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000007348 radical reaction Methods 0.000 description 2
- 239000012763 reinforcing filler Substances 0.000 description 2
- PLFJWWUZKJKIPZ-UHFFFAOYSA-N 2-[2-[2-(2,6,8-trimethylnonan-4-yloxy)ethoxy]ethoxy]ethanol Chemical compound CC(C)CC(C)CC(CC(C)C)OCCOCCOCCO PLFJWWUZKJKIPZ-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- MWRSABPHNREIIX-UHFFFAOYSA-N 9,9-dimethyldecan-1-ol Chemical compound CC(C)(C)CCCCCCCCO MWRSABPHNREIIX-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 229910020485 SiO4/2 Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 125000005594 diketone group Chemical group 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 229920005645 diorganopolysiloxane polymer Polymers 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 1
- 150000002429 hydrazines Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000011256 inorganic filler Substances 0.000 description 1
- 229910003475 inorganic filler Inorganic materials 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 150000003961 organosilicon compounds Chemical class 0.000 description 1
- 125000005375 organosiloxane group Chemical group 0.000 description 1
- 150000003003 phosphines Chemical class 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical class OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 125000004368 propenyl group Chemical group C(=CC)* 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- 239000005051 trimethylchlorosilane Substances 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Landscapes
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22450086A JPS6377942A (ja) | 1986-09-22 | 1986-09-22 | シリコ−ンゴム粒状物の製造方法 |
| US07/095,794 US4743670A (en) | 1986-09-22 | 1987-09-14 | Method for producing silicone rubber powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22450086A JPS6377942A (ja) | 1986-09-22 | 1986-09-22 | シリコ−ンゴム粒状物の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6377942A true JPS6377942A (ja) | 1988-04-08 |
| JPH0513972B2 JPH0513972B2 (enrdf_load_stackoverflow) | 1993-02-23 |
Family
ID=16814771
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP22450086A Granted JPS6377942A (ja) | 1986-09-22 | 1986-09-22 | シリコ−ンゴム粒状物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6377942A (enrdf_load_stackoverflow) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0812524A (ja) * | 1994-06-30 | 1996-01-16 | Toray Dow Corning Silicone Co Ltd | メーキャップ化粧料 |
| EP0779322A1 (en) | 1995-11-30 | 1997-06-18 | Dow Corning Toray Silicone Company Ltd. | Composite cured silicone powder and method for the preparation thereof |
| EP0822232A3 (en) * | 1996-07-30 | 1998-07-08 | Toshiba Silicone Co., Ltd. | Silicone emulsion composition and process for producing silicone powder therefrom |
| US5973060A (en) * | 1998-02-10 | 1999-10-26 | Dow Corning Toray Silicone Co., Ltd. | Silicone rubber particulate composition and methods for the preparation thereof |
| JP2003101176A (ja) * | 2001-09-26 | 2003-04-04 | Hitachi Chem Co Ltd | 配線板用複合材料とその製造方法 |
| WO2007058386A1 (en) | 2005-11-17 | 2007-05-24 | Dow Corning Toray Co., Ltd. | Method of controlling oil-absorbing properties of a silicone rubber powder |
| JP2008121024A (ja) * | 2008-01-31 | 2008-05-29 | Dow Corning Toray Co Ltd | 粒状シリコーン硬化物、およびその製造方法 |
| US7399803B2 (en) | 2002-12-13 | 2008-07-15 | Dow Corning Toray Company, Ltd. | Composite cured silicone powder, method for production thereof, and aqueous composition |
| EP2075280A1 (en) | 2007-12-26 | 2009-07-01 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition, optoelectric part case, and molding method |
| WO2011052695A1 (ja) | 2009-11-02 | 2011-05-05 | 信越化学工業株式会社 | 球状炭化ケイ素粉末、その製造方法、及びそれを使用する炭化ケイ素セラミックス成形体の製造方法 |
| US8012381B2 (en) | 2008-06-09 | 2011-09-06 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition and optoelectronic part case |
| US8173053B2 (en) | 2008-06-09 | 2012-05-08 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition and optoelectronic part case |
| WO2012121060A1 (ja) | 2011-03-08 | 2012-09-13 | 信越化学工業株式会社 | 易焼結性炭化ケイ素粉末及び炭化ケイ素セラミックス焼結体 |
| WO2014098205A2 (en) | 2012-12-22 | 2014-06-26 | Dow Corning Toray Co., Ltd. | Low platinum content hydrosilylation reaction-crosslinkable silicone rubber powder |
-
1986
- 1986-09-22 JP JP22450086A patent/JPS6377942A/ja active Granted
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0812524A (ja) * | 1994-06-30 | 1996-01-16 | Toray Dow Corning Silicone Co Ltd | メーキャップ化粧料 |
| EP0779322A1 (en) | 1995-11-30 | 1997-06-18 | Dow Corning Toray Silicone Company Ltd. | Composite cured silicone powder and method for the preparation thereof |
| EP0822232A3 (en) * | 1996-07-30 | 1998-07-08 | Toshiba Silicone Co., Ltd. | Silicone emulsion composition and process for producing silicone powder therefrom |
| US5973060A (en) * | 1998-02-10 | 1999-10-26 | Dow Corning Toray Silicone Co., Ltd. | Silicone rubber particulate composition and methods for the preparation thereof |
| US6117933A (en) * | 1998-02-10 | 2000-09-12 | Dow Corning Toray Silicone Co., Ltd. | Silicone rubber particulate composition and methods for the preparation thereof |
| JP2003101176A (ja) * | 2001-09-26 | 2003-04-04 | Hitachi Chem Co Ltd | 配線板用複合材料とその製造方法 |
| US7399803B2 (en) | 2002-12-13 | 2008-07-15 | Dow Corning Toray Company, Ltd. | Composite cured silicone powder, method for production thereof, and aqueous composition |
| US7875699B2 (en) | 2005-11-17 | 2011-01-25 | Dow Corning Toray Company, Ltd. | Method of controlling oil-absorbing properties of a silicone rubber powder |
| WO2007058386A1 (en) | 2005-11-17 | 2007-05-24 | Dow Corning Toray Co., Ltd. | Method of controlling oil-absorbing properties of a silicone rubber powder |
| US8329858B2 (en) | 2005-11-17 | 2012-12-11 | Dow Corning Toray Co., Ltd. | Method of controlling oil-absorbing properties of a silicone rubber powder |
| KR101396163B1 (ko) * | 2005-11-17 | 2014-05-19 | 다우 코닝 도레이 캄파니 리미티드 | 실리콘 고무 분말의 흡유성을 조절하는 방법 |
| EP2075280A1 (en) | 2007-12-26 | 2009-07-01 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition, optoelectric part case, and molding method |
| US8013056B2 (en) | 2007-12-26 | 2011-09-06 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition, optoelectronic part case, and molding method |
| JP2008121024A (ja) * | 2008-01-31 | 2008-05-29 | Dow Corning Toray Co Ltd | 粒状シリコーン硬化物、およびその製造方法 |
| US8012381B2 (en) | 2008-06-09 | 2011-09-06 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition and optoelectronic part case |
| US8173053B2 (en) | 2008-06-09 | 2012-05-08 | Shin-Etsu Chemical Co., Ltd. | White heat-curable silicone resin composition and optoelectronic part case |
| WO2011052695A1 (ja) | 2009-11-02 | 2011-05-05 | 信越化学工業株式会社 | 球状炭化ケイ素粉末、その製造方法、及びそれを使用する炭化ケイ素セラミックス成形体の製造方法 |
| WO2012121060A1 (ja) | 2011-03-08 | 2012-09-13 | 信越化学工業株式会社 | 易焼結性炭化ケイ素粉末及び炭化ケイ素セラミックス焼結体 |
| WO2014098205A2 (en) | 2012-12-22 | 2014-06-26 | Dow Corning Toray Co., Ltd. | Low platinum content hydrosilylation reaction-crosslinkable silicone rubber powder |
| US9561171B2 (en) | 2012-12-22 | 2017-02-07 | Dow Corning Toray Co., Ltd. | Low platinum content hydrosilylation reaction-crosslinked silicone rubber powder |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0513972B2 (enrdf_load_stackoverflow) | 1993-02-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |