JPS6315297B2 - - Google Patents
Info
- Publication number
- JPS6315297B2 JPS6315297B2 JP53076590A JP7659078A JPS6315297B2 JP S6315297 B2 JPS6315297 B2 JP S6315297B2 JP 53076590 A JP53076590 A JP 53076590A JP 7659078 A JP7659078 A JP 7659078A JP S6315297 B2 JPS6315297 B2 JP S6315297B2
- Authority
- JP
- Japan
- Prior art keywords
- aqueous solution
- salt
- diamine
- weight
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003839 salts Chemical class 0.000 claims description 24
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 claims description 22
- 239000007864 aqueous solution Substances 0.000 claims description 21
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000004952 Polyamide Substances 0.000 claims description 12
- 229920002647 polyamide Polymers 0.000 claims description 12
- 235000011037 adipic acid Nutrition 0.000 claims description 7
- 239000001361 adipic acid Substances 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000007858 starting material Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 230000003472 neutralizing effect Effects 0.000 claims 1
- 150000004985 diamines Chemical class 0.000 description 17
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 12
- 238000009833 condensation Methods 0.000 description 11
- 230000005494 condensation Effects 0.000 description 11
- 238000006386 neutralization reaction Methods 0.000 description 9
- 239000012266 salt solution Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- UFFRSDWQMJYQNE-UHFFFAOYSA-N 6-azaniumylhexylazanium;hexanedioate Chemical compound [NH3+]CCCCCC[NH3+].[O-]C(=O)CCCCC([O-])=O UFFRSDWQMJYQNE-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000000155 melt Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 150000001991 dicarboxylic acids Chemical class 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- WMRCTEPOPAZMMN-UHFFFAOYSA-N 2-undecylpropanedioic acid Chemical compound CCCCCCCCCCCC(C(O)=O)C(O)=O WMRCTEPOPAZMMN-UHFFFAOYSA-N 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 229920001778 nylon Polymers 0.000 description 2
- 238000006068 polycondensation reaction Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- TYFQFVWCELRYAO-UHFFFAOYSA-N suberic acid Chemical compound OC(=O)CCCCCCC(O)=O TYFQFVWCELRYAO-UHFFFAOYSA-N 0.000 description 2
- PWGJDPKCLMLPJW-UHFFFAOYSA-N 1,8-diaminooctane Chemical compound NCCCCCCCCN PWGJDPKCLMLPJW-UHFFFAOYSA-N 0.000 description 1
- JPSKCQCQZUGWNM-UHFFFAOYSA-N 2,7-Oxepanedione Chemical compound O=C1CCCCC(=O)O1 JPSKCQCQZUGWNM-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000002216 antistatic agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- YQLZOAVZWJBZSY-UHFFFAOYSA-N decane-1,10-diamine Chemical compound NCCCCCCCCCCN YQLZOAVZWJBZSY-UHFFFAOYSA-N 0.000 description 1
- YWJUZWOHLHBWQY-UHFFFAOYSA-N decanedioic acid;hexane-1,6-diamine Chemical compound NCCCCCCN.OC(=O)CCCCCCCCC(O)=O YWJUZWOHLHBWQY-UHFFFAOYSA-N 0.000 description 1
- 238000006114 decarboxylation reaction Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- QFTYSVGGYOXFRQ-UHFFFAOYSA-N dodecane-1,12-diamine Chemical compound NCCCCCCCCCCCCN QFTYSVGGYOXFRQ-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- -1 filaments Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 238000010137 moulding (plastic) Methods 0.000 description 1
- 238000001139 pH measurement Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
- C08G69/28—Preparatory processes
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19772728931 DE2728931A1 (de) | 1977-06-27 | 1977-06-27 | Verfahren zur herstellung von polyamiden |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5411999A JPS5411999A (en) | 1979-01-29 |
| JPS6315297B2 true JPS6315297B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-04-04 |
Family
ID=6012472
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7659078A Granted JPS5411999A (en) | 1977-06-27 | 1978-06-26 | Preparation of polyamide |
Country Status (5)
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58205492A (ja) * | 1982-05-27 | 1983-11-30 | Q P Corp | 酒類用顆粒の製法 |
| US4442260A (en) * | 1983-03-14 | 1984-04-10 | E. I. Du Pont De Nemours & Company | Preparation of salt solution useful for making nylon |
| US4617373A (en) | 1985-02-15 | 1986-10-14 | Eastman Kodak Company | Condensation polymers and products therefrom |
| JPH02503521A (ja) * | 1987-12-03 | 1990-10-25 | ユニヴァーシティ オブ フロリダ | 定位法放射線治療に用いられる装置 |
| DE4403452A1 (de) * | 1993-04-26 | 1994-10-27 | Zimmer Ag | Diskontinuierliches katalytisches Verfahren zur Herstellung von Polyamid-6.6 |
| US20070287822A1 (en) * | 2006-06-13 | 2007-12-13 | Eastman Chemical Company | Light absorbing compositions |
| CN103974997B (zh) | 2011-12-05 | 2017-06-23 | 因温斯特技术公司 | 用于制备聚酰胺的方法 |
| TW201444792A (zh) * | 2013-05-01 | 2014-12-01 | Invista Tech Sarl | 用於計量供製造尼龍鹽溶液之二羧酸粉末之方法 |
| TWI787251B (zh) | 2017-04-13 | 2022-12-21 | 英商英威達紡織（英國）有限公司 | 製備用於聚醯胺化製程之前體之單體平衡控制 |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE487516A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1948-05-01 | |||
| NL102671C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1955-07-23 | |||
| BE591399A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1959-06-06 | |||
| BE640369A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1963-08-12 | 1964-03-16 | ||
| NL298696A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1962-10-04 | |||
| GB1159151A (en) | 1966-04-22 | 1969-07-23 | Ici Ltd | Improvements in or relating to Continuous Polymerisation of Polyamides |
| US3952051A (en) * | 1971-05-08 | 1976-04-20 | Asahi Kasei Kogyo Kabushiki Kaisha | Method for crystallization of diamine dicarboxylate |
| CA1012729A (en) * | 1973-01-17 | 1977-06-28 | E.I. Du Pont De Nemours And Company | Controlling evaporator temperature according to pressure drop between finisher and spinning manifold |
| US4131712A (en) * | 1977-08-10 | 1978-12-26 | E. I. Du Pont De Nemours And Company | Process for preparing polyamide from diacid-rich component and diamine-rich component |
-
1977
- 1977-06-27 DE DE19772728931 patent/DE2728931A1/de not_active Withdrawn
-
1978
- 1978-06-08 US US05/913,748 patent/US4251653A/en not_active Expired - Lifetime
- 1978-06-14 EP EP78100150A patent/EP0000142B1/de not_active Expired
- 1978-06-14 DE DE7878100150T patent/DE2860225D1/de not_active Expired
- 1978-06-20 IT IT24768/78A patent/IT1096578B/it active
- 1978-06-26 JP JP7659078A patent/JPS5411999A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| IT1096578B (it) | 1985-08-26 |
| IT7824768A0 (it) | 1978-06-20 |
| US4251653A (en) | 1981-02-17 |
| DE2860225D1 (en) | 1980-12-04 |
| EP0000142B1 (de) | 1980-08-20 |
| JPS5411999A (en) | 1979-01-29 |
| EP0000142A1 (de) | 1979-01-10 |
| DE2728931A1 (de) | 1979-01-04 |
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