JPS6232212B2 - - Google Patents
Info
- Publication number
- JPS6232212B2 JPS6232212B2 JP8609584A JP8609584A JPS6232212B2 JP S6232212 B2 JPS6232212 B2 JP S6232212B2 JP 8609584 A JP8609584 A JP 8609584A JP 8609584 A JP8609584 A JP 8609584A JP S6232212 B2 JPS6232212 B2 JP S6232212B2
- Authority
- JP
- Japan
- Prior art keywords
- titanium oxide
- slurry
- caprolactam
- weight
- diammonium adipate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 74
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 73
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims description 44
- 239000002002 slurry Substances 0.000 claims description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- -1 polyhexamethylene diammonium adipate Polymers 0.000 claims description 12
- UFFRSDWQMJYQNE-UHFFFAOYSA-N 6-azaniumylhexylazanium;hexanedioate Chemical compound [NH3+]CCCCCC[NH3+].[O-]C(=O)CCCCC([O-])=O UFFRSDWQMJYQNE-UHFFFAOYSA-N 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000006116 polymerization reaction Methods 0.000 claims description 5
- 238000007334 copolymerization reaction Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 description 20
- 238000000034 method Methods 0.000 description 13
- 239000004952 Polyamide Substances 0.000 description 11
- 150000001875 compounds Chemical class 0.000 description 11
- 229920002647 polyamide Polymers 0.000 description 11
- 239000007864 aqueous solution Substances 0.000 description 9
- 239000010419 fine particle Substances 0.000 description 9
- 239000002245 particle Substances 0.000 description 9
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 6
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical group NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 6
- 239000012266 salt solution Substances 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 235000011037 adipic acid Nutrition 0.000 description 3
- 239000001361 adipic acid Substances 0.000 description 3
- 229920002302 Nylon 6,6 Polymers 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 2
- 238000006068 polycondensation reaction Methods 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000006059 cover glass Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Polyamides (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP8609584A JPS60231725A (ja) | 1984-05-01 | 1984-05-01 | 酸化チタン含有ポリヘキサメチレンジアンモニウムアジペ−トの製法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP8609584A JPS60231725A (ja) | 1984-05-01 | 1984-05-01 | 酸化チタン含有ポリヘキサメチレンジアンモニウムアジペ−トの製法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS60231725A JPS60231725A (ja) | 1985-11-18 |
JPS6232212B2 true JPS6232212B2 (ko) | 1987-07-13 |
Family
ID=13877147
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP8609584A Granted JPS60231725A (ja) | 1984-05-01 | 1984-05-01 | 酸化チタン含有ポリヘキサメチレンジアンモニウムアジペ−トの製法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS60231725A (ko) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0429124Y2 (ko) * | 1987-10-16 | 1992-07-15 |
-
1984
- 1984-05-01 JP JP8609584A patent/JPS60231725A/ja active Granted
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0429124Y2 (ko) * | 1987-10-16 | 1992-07-15 |
Also Published As
Publication number | Publication date |
---|---|
JPS60231725A (ja) | 1985-11-18 |
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