JPS62185066A - ３，５，６−トリフルオロ−４−メルカプトフタル酸 - Google Patents
３，５，６−トリフルオロ−４−メルカプトフタル酸Info
- Publication number
- JPS62185066A JPS62185066A JP2688586A JP2688586A JPS62185066A JP S62185066 A JPS62185066 A JP S62185066A JP 2688586 A JP2688586 A JP 2688586A JP 2688586 A JP2688586 A JP 2688586A JP S62185066 A JPS62185066 A JP S62185066A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- trifluoro
- mercaptophthalic
- formula
- alkali metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JXVICXPMIXTSIU-UHFFFAOYSA-N 3,4,6-trifluoro-5-sulfanylphthalic acid Chemical compound OC(=O)C1=C(F)C(F)=C(S)C(F)=C1C(O)=O JXVICXPMIXTSIU-UHFFFAOYSA-N 0.000 title claims 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- YJLVXRPNNDKMMO-UHFFFAOYSA-N 3,4,5,6-tetrafluorophthalic acid Chemical compound OC(=O)C1=C(F)C(F)=C(F)C(F)=C1C(O)=O YJLVXRPNNDKMMO-UHFFFAOYSA-N 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 3
- HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 abstract description 3
- 239000004593 Epoxy Substances 0.000 abstract description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract description 2
- 239000012736 aqueous medium Substances 0.000 abstract description 2
- 229910000037 hydrogen sulfide Inorganic materials 0.000 abstract description 2
- 239000011368 organic material Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract 2
- 239000003905 agrochemical Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- -1 alkali metal hydrogen sulfide Chemical class 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 239000004848 polyfunctional curative Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 238000000862 absorption spectrum Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- FZUUAPPKEJXGEN-UHFFFAOYSA-N 4-sulfanylphthalic acid Chemical compound OC(=O)C1=CC=C(S)C=C1C(O)=O FZUUAPPKEJXGEN-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- MTJGVAJYTOXFJH-UHFFFAOYSA-N 3-aminonaphthalene-1,5-disulfonic acid Chemical compound C1=CC=C(S(O)(=O)=O)C2=CC(N)=CC(S(O)(=O)=O)=C21 MTJGVAJYTOXFJH-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229920001002 functional polymer Polymers 0.000 description 1
- 125000004356 hydroxy functional group Chemical group O* 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- PXQLVRUNWNTZOS-UHFFFAOYSA-N sulfanyl Chemical class [SH] PXQLVRUNWNTZOS-UHFFFAOYSA-N 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2688586A JPS62185066A (ja) | 1986-02-12 | 1986-02-12 | ３，５，６−トリフルオロ−４−メルカプトフタル酸 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2688586A JPS62185066A (ja) | 1986-02-12 | 1986-02-12 | ３，５，６−トリフルオロ−４−メルカプトフタル酸 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62185066A true JPS62185066A (ja) | 1987-08-13 |
| JPH0519546B2 JPH0519546B2 (enrdf_load_stackoverflow) | 1993-03-17 |
Family
ID=12205721
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2688586A Granted JPS62185066A (ja) | 1986-02-12 | 1986-02-12 | ３，５，６−トリフルオロ−４−メルカプトフタル酸 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62185066A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009503012A (ja) * | 2005-08-04 | 2009-01-29 | エボニック デグサ ゲーエムベーハー | ２，４，６−トリメルカプト−１，３，５−トリアジンの製造方法 |
-
1986
- 1986-02-12 JP JP2688586A patent/JPS62185066A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009503012A (ja) * | 2005-08-04 | 2009-01-29 | エボニック デグサ ゲーエムベーハー | ２，４，６−トリメルカプト−１，３，５−トリアジンの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0519546B2 (enrdf_load_stackoverflow) | 1993-03-17 |
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