JPS6212231B2 - - Google Patents
Info
- Publication number
- JPS6212231B2 JPS6212231B2 JP53018629A JP1862978A JPS6212231B2 JP S6212231 B2 JPS6212231 B2 JP S6212231B2 JP 53018629 A JP53018629 A JP 53018629A JP 1862978 A JP1862978 A JP 1862978A JP S6212231 B2 JPS6212231 B2 JP S6212231B2
- Authority
- JP
- Japan
- Prior art keywords
- silane
- adsorption bed
- biphenyl
- bed
- adsorption
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 claims description 295
- 238000001179 sorption measurement Methods 0.000 claims description 198
- 235000010290 biphenyl Nutrition 0.000 claims description 148
- 239000004305 biphenyl Substances 0.000 claims description 146
- 239000002904 solvent Substances 0.000 claims description 124
- 238000000034 method Methods 0.000 claims description 109
- 229910000077 silane Inorganic materials 0.000 claims description 107
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 106
- 150000002430 hydrocarbons Chemical class 0.000 claims description 104
- 239000004215 Carbon black (E152) Substances 0.000 claims description 102
- 229930195733 hydrocarbon Natural products 0.000 claims description 102
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims description 68
- 150000004756 silanes Chemical class 0.000 claims description 60
- 238000003795 desorption Methods 0.000 claims description 56
- 239000003463 adsorbent Substances 0.000 claims description 53
- 238000001125 extrusion Methods 0.000 claims description 42
- 239000012535 impurity Substances 0.000 claims description 42
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 35
- 238000000746 purification Methods 0.000 claims description 30
- NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 claims description 19
- JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 claims description 19
- 239000003610 charcoal Substances 0.000 claims description 16
- OSXYHAQZDCICNX-UHFFFAOYSA-N dichloro(diphenyl)silane Chemical group C=1C=CC=CC=1[Si](Cl)(Cl)C1=CC=CC=C1 OSXYHAQZDCICNX-UHFFFAOYSA-N 0.000 claims description 14
- 239000002808 molecular sieve Substances 0.000 claims description 14
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 14
- 239000011261 inert gas Substances 0.000 claims description 9
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000012264 purified product Substances 0.000 claims description 6
- GTPDFCLBTFKHNH-UHFFFAOYSA-N chloro(phenyl)silicon Chemical compound Cl[Si]C1=CC=CC=C1 GTPDFCLBTFKHNH-UHFFFAOYSA-N 0.000 claims description 5
- 239000003849 aromatic solvent Substances 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 238000011282 treatment Methods 0.000 claims description 3
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- 125000001309 chloro group Chemical group Cl* 0.000 claims 5
- 150000001282 organosilanes Chemical class 0.000 claims 5
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 76
- -1 siloxanes Chemical class 0.000 description 71
- 230000008569 process Effects 0.000 description 36
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical class Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 35
- 239000005046 Chlorosilane Substances 0.000 description 33
- 238000004821 distillation Methods 0.000 description 25
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 15
- 239000000047 product Substances 0.000 description 14
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
- 229920001296 polysiloxane Polymers 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 8
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 7
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 230000008929 regeneration Effects 0.000 description 4
- 238000011069 regeneration method Methods 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 229920005573 silicon-containing polymer Polymers 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 230000000274 adsorptive effect Effects 0.000 description 3
- NBWIIOQJUKRLKW-UHFFFAOYSA-N chloro(phenyl)silane Chemical class Cl[SiH2]C1=CC=CC=C1 NBWIIOQJUKRLKW-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 150000008282 halocarbons Chemical group 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- TVJPBVNWVPUZBM-UHFFFAOYSA-N [diacetyloxy(methyl)silyl] acetate Chemical compound CC(=O)O[Si](C)(OC(C)=O)OC(C)=O TVJPBVNWVPUZBM-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 2
- 150000004074 biphenyls Chemical class 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 150000003071 polychlorinated biphenyls Chemical group 0.000 description 2
- 230000001172 regenerating effect Effects 0.000 description 2
- 238000012958 reprocessing Methods 0.000 description 2
- 229940024463 silicone emollient and protective product Drugs 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- 239000008096 xylene Substances 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 229920006368 Hylar Polymers 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 125000003668 acetyloxy group Chemical group [H]C([H])([H])C(=O)O[*] 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000003545 alkoxy group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- FYBYQXQHBHTWLP-UHFFFAOYSA-N bis(silyloxysilyloxy)silane Chemical class [SiH3]O[SiH2]O[SiH2]O[SiH2]O[SiH3] FYBYQXQHBHTWLP-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 125000000753 cycloalkyl group Chemical group 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000005055 methyl trichlorosilane Substances 0.000 description 1
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 1
- BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000005054 phenyltrichlorosilane Substances 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000005049 silicon tetrachloride Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000002594 sorbent Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- ORVMIVQULIKXCP-UHFFFAOYSA-N trichloro(phenyl)silane Chemical compound Cl[Si](Cl)(Cl)C1=CC=CC=C1 ORVMIVQULIKXCP-UHFFFAOYSA-N 0.000 description 1
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/20—Purification, separation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77032977A | 1977-02-22 | 1977-02-22 | |
| US05/828,367 US4127598A (en) | 1977-02-22 | 1977-08-29 | Process for removing biphenyls from chlorosilanes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS53111043A JPS53111043A (en) | 1978-09-28 |
| JPS6212231B2 true JPS6212231B2 (US20110009641A1-20110113-C00256.png) | 1987-03-17 |
Family
ID=27118300
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1862978A Granted JPS53111043A (en) | 1977-02-22 | 1978-02-22 | Method for purification of silane and siloxane |
Country Status (9)
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01122233U (US20110009641A1-20110113-C00256.png) * | 1988-02-12 | 1989-08-18 | ||
| JPH0267535U (US20110009641A1-20110113-C00256.png) * | 1988-11-11 | 1990-05-22 | ||
| JPH0310448U (US20110009641A1-20110113-C00256.png) * | 1989-06-16 | 1991-01-31 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH045293A (ja) * | 1990-04-19 | 1992-01-09 | Tosoh Akzo Corp | 有機シリコーン化合物の精製法 |
| US5445742A (en) * | 1994-05-23 | 1995-08-29 | Dow Corning Corporation | Process for purifying halosilanes |
| JP4024469B2 (ja) * | 2000-11-06 | 2007-12-19 | 信越化学工業株式会社 | オルガノポリシロキサンの精製方法及びその精製方法により得られるオルガノポリシロキサン |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US831216A (en) * | 1906-05-21 | 1906-09-18 | George W Davis | Car-step. |
| US2971607A (en) * | 1958-07-14 | 1961-02-14 | Union Carbide Corp | Method for purifying silance |
| US3029135A (en) * | 1958-05-16 | 1962-04-10 | Int Standard Electric Corp | Purification of gases used in the production of silicon |
| US3151045A (en) * | 1960-03-31 | 1964-09-29 | Bayer Ag | Process for the removal of aromatic impurities from phenyl methyl polysiloxanes |
| US3755152A (en) * | 1970-09-14 | 1973-08-28 | Ouvoe Chem Ind Inc | Removing contaminants from organic materials |
| US3803195A (en) * | 1971-09-29 | 1974-04-09 | Wacker Chemie Gmbh | Process for the production of organosiloxanes |
| JPS509598A (US20110009641A1-20110113-C00256.png) * | 1973-05-30 | 1975-01-31 | ||
| JPS5133540A (en) * | 1974-09-17 | 1976-03-22 | Tokyo Shibaura Electric Co | Fet zofukuki no ratsushudenryuboshikairo |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1488994A (fr) * | 1965-09-10 | 1967-07-21 | Rhone Poulenc Sa | Procédé de purification de chlorosilanes |
| GB1526065A (en) * | 1974-10-16 | 1978-09-27 | Asahi Chemical Ind | Process for separation of hydrocarbon mixture |
-
1978
- 1978-02-10 GB GB546078A patent/GB1567096A/en not_active Expired
- 1978-02-20 FR FR7804722A patent/FR2408616A1/fr active Granted
- 1978-02-22 AR AR27118978A patent/AR226149A1/es active
- 1978-02-22 AU AU33522/78A patent/AU519804B2/en not_active Expired
- 1978-02-22 BR BR7801089A patent/BR7801089A/pt unknown
- 1978-02-22 MX MX17251878A patent/MX147873A/es unknown
- 1978-02-22 DE DE19782807589 patent/DE2807589A1/de active Granted
- 1978-02-22 NL NL7801982A patent/NL7801982A/xx not_active Application Discontinuation
- 1978-02-22 JP JP1862978A patent/JPS53111043A/ja active Granted
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US831216A (en) * | 1906-05-21 | 1906-09-18 | George W Davis | Car-step. |
| US3029135A (en) * | 1958-05-16 | 1962-04-10 | Int Standard Electric Corp | Purification of gases used in the production of silicon |
| US2971607A (en) * | 1958-07-14 | 1961-02-14 | Union Carbide Corp | Method for purifying silance |
| US3151045A (en) * | 1960-03-31 | 1964-09-29 | Bayer Ag | Process for the removal of aromatic impurities from phenyl methyl polysiloxanes |
| US3755152A (en) * | 1970-09-14 | 1973-08-28 | Ouvoe Chem Ind Inc | Removing contaminants from organic materials |
| US3803195A (en) * | 1971-09-29 | 1974-04-09 | Wacker Chemie Gmbh | Process for the production of organosiloxanes |
| JPS509598A (US20110009641A1-20110113-C00256.png) * | 1973-05-30 | 1975-01-31 | ||
| JPS5133540A (en) * | 1974-09-17 | 1976-03-22 | Tokyo Shibaura Electric Co | Fet zofukuki no ratsushudenryuboshikairo |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01122233U (US20110009641A1-20110113-C00256.png) * | 1988-02-12 | 1989-08-18 | ||
| JPH0267535U (US20110009641A1-20110113-C00256.png) * | 1988-11-11 | 1990-05-22 | ||
| JPH0310448U (US20110009641A1-20110113-C00256.png) * | 1989-06-16 | 1991-01-31 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2807589A1 (de) | 1978-09-07 |
| DE2807589C2 (US20110009641A1-20110113-C00256.png) | 1991-12-19 |
| AU519804B2 (en) | 1981-12-24 |
| BR7801089A (pt) | 1979-01-02 |
| AR226149A1 (es) | 1982-06-15 |
| FR2408616A1 (fr) | 1979-06-08 |
| AU3352278A (en) | 1979-08-30 |
| MX147873A (es) | 1983-01-26 |
| JPS53111043A (en) | 1978-09-28 |
| FR2408616B1 (US20110009641A1-20110113-C00256.png) | 1984-01-27 |
| NL7801982A (nl) | 1978-08-24 |
| GB1567096A (en) | 1980-05-08 |
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