JPS6052081B2 - 水素の熱化学的製造方法 - Google Patents
水素の熱化学的製造方法Info
- Publication number
- JPS6052081B2 JPS6052081B2 JP51091428A JP9142876A JPS6052081B2 JP S6052081 B2 JPS6052081 B2 JP S6052081B2 JP 51091428 A JP51091428 A JP 51091428A JP 9142876 A JP9142876 A JP 9142876A JP S6052081 B2 JPS6052081 B2 JP S6052081B2
- Authority
- JP
- Japan
- Prior art keywords
- iodine
- hydrogen
- reaction
- phase
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052739 hydrogen Inorganic materials 0.000 title claims description 35
- 239000001257 hydrogen Substances 0.000 title claims description 35
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims description 31
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 64
- 239000012071 phase Substances 0.000 claims description 51
- 238000006243 chemical reaction Methods 0.000 claims description 50
- 229910001868 water Inorganic materials 0.000 claims description 44
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 claims description 33
- 229910000043 hydrogen iodide Inorganic materials 0.000 claims description 31
- 229910052740 iodine Inorganic materials 0.000 claims description 25
- 239000011630 iodine Substances 0.000 claims description 25
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 20
- 238000000197 pyrolysis Methods 0.000 claims description 11
- 238000000926 separation method Methods 0.000 claims description 11
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 10
- 238000009833 condensation Methods 0.000 claims description 8
- 230000005494 condensation Effects 0.000 claims description 8
- 239000000376 reactant Substances 0.000 claims description 7
- 239000008346 aqueous phase Substances 0.000 claims description 6
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000005979 thermal decomposition reaction Methods 0.000 claims description 4
- 238000011065 in-situ storage Methods 0.000 claims description 3
- 150000001722 carbon compounds Chemical class 0.000 claims description 2
- 230000001737 promoting effect Effects 0.000 claims 1
- 230000000717 retained effect Effects 0.000 claims 1
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 10
- 239000007788 liquid Substances 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- 238000000354 decomposition reaction Methods 0.000 description 8
- 238000004821 distillation Methods 0.000 description 8
- 235000011149 sulphuric acid Nutrition 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 239000007795 chemical reaction product Substances 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 238000009738 saturating Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- XZXYQEHISUMZAT-UHFFFAOYSA-N 2-[(2-hydroxy-5-methylphenyl)methyl]-4-methylphenol Chemical compound CC1=CC=C(O)C(CC=2C(=CC=C(C)C=2)O)=C1 XZXYQEHISUMZAT-UHFFFAOYSA-N 0.000 description 1
- OOEWZEXEJQEFJO-UHFFFAOYSA-N O.[I] Chemical compound O.[I] OOEWZEXEJQEFJO-UHFFFAOYSA-N 0.000 description 1
- PWQNEFAZHKFPOH-UHFFFAOYSA-N O.[I].I Chemical compound O.[I].I PWQNEFAZHKFPOH-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229940107816 ammonium iodide Drugs 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005112 continuous flow technique Methods 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000010574 gas phase reaction Methods 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- -1 hydrogen triiodide Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- FWFGVMYFCODZRD-UHFFFAOYSA-N oxidanium;hydrogen sulfate Chemical compound O.OS(O)(=O)=O FWFGVMYFCODZRD-UHFFFAOYSA-N 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 238000005215 recombination Methods 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/06—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents
- C01B3/068—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents the hydrogen being generated from the water as a result of a cyclus of reactions, not covered by groups C01B3/063 or C01B3/105
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US60191775A | 1975-08-04 | 1975-08-04 | |
| US601917 | 1996-02-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5220394A JPS5220394A (en) | 1977-02-16 |
| JPS6052081B2 true JPS6052081B2 (ja) | 1985-11-18 |
Family
ID=24409270
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP51091428A Expired JPS6052081B2 (ja) | 1975-08-04 | 1976-08-02 | 水素の熱化学的製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4089940A (en, 2012) |
| JP (1) | JPS6052081B2 (en, 2012) |
| DE (1) | DE2634662C2 (en, 2012) |
| FR (1) | FR2320258A1 (en, 2012) |
| GB (1) | GB1550244A (en, 2012) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006199532A (ja) * | 2005-01-20 | 2006-08-03 | Toshiba Corp | 水素生成物質の製造装置及びその方法 |
| JP2007031173A (ja) * | 2005-07-22 | 2007-02-08 | Toshiba Corp | ヨウ化水素製造方法およびヨウ化水素製造装置 |
| JP2008024551A (ja) * | 2006-07-21 | 2008-02-07 | Toshiba Corp | ヨウ化水素製造方法およびヨウ化水素製造装置 |
| JP2009114025A (ja) * | 2007-11-07 | 2009-05-28 | Toshiba Corp | ヨウ化水素製造方法およびその装置 |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4208396A (en) * | 1975-08-04 | 1980-06-17 | General Atomic Company | Oxygen recovery from gas mixtures |
| US4330523A (en) * | 1976-02-25 | 1982-05-18 | Westinghouse Electric Corp. | Decomposition of water |
| GB1577630A (en) * | 1977-04-07 | 1980-10-29 | Euratom | Process for the separation of sulphuric acid and hydriodic acid |
| US4150094A (en) * | 1977-12-30 | 1979-04-17 | General Atomic Company | Method of reacting I2 with a liquid and a gas |
| US4176169A (en) * | 1978-07-03 | 1979-11-27 | General Atomic Company | Method of extracting iodine from liquid mixtures of iodine, water and hydrogen iodide |
| US4258026A (en) * | 1979-03-26 | 1981-03-24 | General Atomic Company | Hydrogen iodide decomposition |
| US4314982A (en) * | 1979-06-21 | 1982-02-09 | General Atomic Company | Catalytic decomposition of H2 SO4 |
| US4244794A (en) * | 1979-07-31 | 1981-01-13 | The United States Of America As Represented By The United States Department Of Energy | Hydrogen production by the decomposition of water |
| US4410505A (en) * | 1982-05-07 | 1983-10-18 | Ga Technologies Inc. | Hydrogen iodide decomposition |
| US4421734A (en) * | 1982-05-11 | 1983-12-20 | Ga Technologies Inc. | Sulfuric acid-sulfur heat storage cycle |
| US4396591A (en) * | 1982-05-18 | 1983-08-02 | Ga Technologies Inc. | Recovery of hydrogen iodide |
| JPS5983903A (ja) * | 1982-11-08 | 1984-05-15 | Toshiba Corp | 水素の製造方法 |
| US5693306A (en) * | 1994-11-28 | 1997-12-02 | Mitsui Toatsu Chemicals, Inc. | Production process for refined hydrogen iodide |
| US20050000825A1 (en) * | 2003-07-04 | 2005-01-06 | Japan Atomic Energy Research Institute | Process for efficient hydrogen production by thermochemical water splitting using iodine and sulfur dioxide |
| JP4239077B2 (ja) * | 2003-08-20 | 2009-03-18 | 独立行政法人 日本原子力研究開発機構 | 高温耐食性セラミックス製コンパクト熱交換器 |
| JP4468092B2 (ja) * | 2004-06-30 | 2010-05-26 | 株式会社東芝 | 水素製造装置 |
| US20060002845A1 (en) * | 2004-06-30 | 2006-01-05 | Lahoda Edward J | Sulfuric acid process |
| JP4535269B2 (ja) * | 2005-02-22 | 2010-09-01 | 千代田化工建設株式会社 | 水素の製造装置及び水素の製造方法 |
| JP4840900B2 (ja) * | 2005-06-02 | 2011-12-21 | 独立行政法人日本原子力研究開発機構 | 熱化学水素製造方法及び熱化学水素製造装置 |
| US20060277917A1 (en) * | 2005-06-09 | 2006-12-14 | Kuai-Teng Hsu | Thermochemical water splitting power generation process and system |
| JP4945109B2 (ja) * | 2005-10-13 | 2012-06-06 | 株式会社東芝 | ヨウ化水素製造方法および水素製造方法並びにそれらのための製造装置 |
| CN100400412C (zh) * | 2005-10-14 | 2008-07-09 | 浙江大学 | 硫碘开路循环制氢的工艺方法 |
| JP4783173B2 (ja) * | 2006-02-15 | 2011-09-28 | 株式会社東芝 | 水素製造方法 |
| JP4925276B2 (ja) * | 2006-09-21 | 2012-04-25 | 独立行政法人日本原子力研究開発機構 | ミキサセトラ型ブンゼン反応器 |
| JP5038680B2 (ja) * | 2006-10-18 | 2012-10-03 | 株式会社東芝 | ヨウ化水素製造方法および水素製造方法ならびにそれらの製造方法のための装置 |
| FI121271B (fi) * | 2007-01-19 | 2010-09-15 | Outotec Oyj | Menetelmä vedyn ja rikkihapon valmistamiseksi |
| KR100831093B1 (ko) * | 2007-04-09 | 2008-05-22 | 한국과학기술연구원 | 이온성 액체를 이용한 ｉｓ 싸이클 공정의 혼합가스로부터순수 이산화황의 분리 회수 방법 |
| US20120034154A1 (en) * | 2007-04-18 | 2012-02-09 | Orchard Material Technology Llc | Production of hydrogen through oxidation of metal sulfides |
| EP2167423A4 (en) * | 2007-07-23 | 2011-11-09 | Exxonmobile Upstream Res Company | PREPARATION OF HYDROGEN GAS FROM SULFUR CONTAINERS |
| ITRM20070446A1 (it) * | 2007-08-20 | 2009-02-21 | Ast Engineering S R L | Impianto modulare per l abbattimento degli inquinanti contenuti nei fumi industriale |
| US20090068090A1 (en) * | 2007-09-06 | 2009-03-12 | Battelle Energy Alliance, Llc | Methods for reacting and separating components of a gas-phase equilibrium reaction and a centrifugal separation device for same |
| KR100981293B1 (ko) * | 2008-08-20 | 2010-09-10 | 한국과학기술원 | 열화학적 효율을 향상시킨 원자력수소생산을 위한 요오드-황 싸이클 공정 |
| DE102012203202A1 (de) * | 2012-03-01 | 2013-09-05 | Lars Nordwig | Vorrichtung zur thermochemischen Spaltung von Wasser |
| JP5821777B2 (ja) * | 2012-05-21 | 2015-11-24 | トヨタ自動車株式会社 | アンモニア合成方法 |
| DE202014006825U1 (de) | 2014-08-18 | 2014-09-17 | Anatoly Borodin | Reaktor für die Durchführung eines zweistufigen thermochemischen Wasserstoffherstellungsverfahrens |
| JP7084378B2 (ja) | 2016-04-28 | 2022-06-14 | インディアン・インスティテゥート・オブ・テクノロジー | 三酸化硫黄の転化方法及び水素生成方法 |
| DE112018007957A5 (de) | 2018-09-05 | 2021-06-02 | Christoph Gregor Wandzik | Wasserstoffreaktor und das regenerative Chemie-Verfahren |
| EP4417593A1 (en) | 2023-02-17 | 2024-08-21 | H2-SPHERE GmbH | Method of converting pyrite into fertilizer |
| CN116621115B (zh) * | 2023-07-23 | 2023-09-26 | 浙江百能科技有限公司 | 一种高压分解碘化氢制取压缩氢气的工艺及装置 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2143222A (en) * | 1936-05-13 | 1939-01-10 | Dow Chemical Co | Process of producing iodine |
| US2339330A (en) * | 1942-04-08 | 1944-01-18 | Colgate Palmolive Peet Co | Preparing anhydrous hydrogen halides |
| US2406930A (en) * | 1942-06-12 | 1946-09-03 | Chemical Construction Corp | Sulphuric acid regeneration |
| US3365276A (en) * | 1964-02-17 | 1968-01-23 | Phillips Petroleum Co | Process for producing hydrogen from dissociation of a hydrogen halide |
| LU68993A1 (en, 2012) * | 1973-12-12 | 1975-03-06 | ||
| US3888750A (en) * | 1974-01-29 | 1975-06-10 | Westinghouse Electric Corp | Electrolytic decomposition of water |
| US3929980A (en) * | 1974-12-26 | 1975-12-30 | Us Energy | Method of producing hydrogen |
-
1976
- 1976-08-02 JP JP51091428A patent/JPS6052081B2/ja not_active Expired
- 1976-08-02 DE DE2634662A patent/DE2634662C2/de not_active Expired
- 1976-08-02 FR FR7623532A patent/FR2320258A1/fr active Granted
- 1976-08-02 GB GB32116/76A patent/GB1550244A/en not_active Expired
-
1977
- 1977-04-08 US US05/786,009 patent/US4089940A/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006199532A (ja) * | 2005-01-20 | 2006-08-03 | Toshiba Corp | 水素生成物質の製造装置及びその方法 |
| JP2007031173A (ja) * | 2005-07-22 | 2007-02-08 | Toshiba Corp | ヨウ化水素製造方法およびヨウ化水素製造装置 |
| JP2008024551A (ja) * | 2006-07-21 | 2008-02-07 | Toshiba Corp | ヨウ化水素製造方法およびヨウ化水素製造装置 |
| JP2009114025A (ja) * | 2007-11-07 | 2009-05-28 | Toshiba Corp | ヨウ化水素製造方法およびその装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2634662C2 (de) | 1987-03-19 |
| FR2320258A1 (fr) | 1977-03-04 |
| DE2634662A1 (de) | 1977-02-17 |
| FR2320258B1 (en, 2012) | 1982-12-03 |
| JPS5220394A (en) | 1977-02-16 |
| US4089940A (en) | 1978-05-16 |
| GB1550244A (en) | 1979-08-08 |
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