JPS604933B2 - 所定の化学的パラメ−タについて試料を分析する方法と装置 - Google Patents
所定の化学的パラメ−タについて試料を分析する方法と装置Info
- Publication number
- JPS604933B2 JPS604933B2 JP52051916A JP5191677A JPS604933B2 JP S604933 B2 JPS604933 B2 JP S604933B2 JP 52051916 A JP52051916 A JP 52051916A JP 5191677 A JP5191677 A JP 5191677A JP S604933 B2 JPS604933 B2 JP S604933B2
- Authority
- JP
- Japan
- Prior art keywords
- sample
- laser beam
- tape
- samples
- chemical parameters
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000126 substance Substances 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 13
- 239000002245 particle Substances 0.000 claims description 20
- 230000008016 vaporization Effects 0.000 claims description 19
- 238000004458 analytical method Methods 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 15
- 238000009834 vaporization Methods 0.000 claims description 13
- 239000011261 inert gas Substances 0.000 claims description 3
- 230000001678 irradiating effect Effects 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 230000003287 optical effect Effects 0.000 claims description 2
- 238000000151 deposition Methods 0.000 claims 2
- 239000011364 vaporized material Substances 0.000 claims 1
- 239000000523 sample Substances 0.000 description 32
- 239000000758 substrate Substances 0.000 description 10
- 239000002390 adhesive tape Substances 0.000 description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 4
- 230000001070 adhesive effect Effects 0.000 description 4
- 229910052782 aluminium Inorganic materials 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000000443 aerosol Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- -1 polyethylene Polymers 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 239000011888 foil Substances 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 239000013618 particulate matter Substances 0.000 description 2
- 239000010979 ruby Substances 0.000 description 2
- 229910001750 ruby Inorganic materials 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 238000009614 chemical analysis method Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000004993 emission spectroscopy Methods 0.000 description 1
- 238000000295 emission spectrum Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000009616 inductively coupled plasma Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920006254 polymer film Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000002310 reflectometry Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229910021654 trace metal Inorganic materials 0.000 description 1
- 238000001429 visible spectrum Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/71—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light thermally excited
- G01N21/718—Laser microanalysis, i.e. with formation of sample plasma
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/04—Devices for withdrawing samples in the solid state, e.g. by cutting
- G01N2001/045—Laser ablation; Microwave vaporisation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/2813—Producing thin layers of samples on a substrate, e.g. smearing, spinning-on
- G01N2001/2833—Collecting samples on a sticky, tacky, adhesive surface
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/00009—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor provided with a sample supporting tape, e.g. with absorbent zones
Landscapes
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Optics & Photonics (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Electron Tubes For Measurement (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB18536/76A GB1574812A (en) | 1976-05-06 | 1976-05-06 | Spectrochemical analysis |
| GB18536/76 | 1976-05-06 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS52138991A JPS52138991A (en) | 1977-11-19 |
| JPS604933B2 true JPS604933B2 (ja) | 1985-02-07 |
Family
ID=10114101
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP52051916A Expired JPS604933B2 (ja) | 1976-05-06 | 1977-05-06 | 所定の化学的パラメ−タについて試料を分析する方法と装置 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4220414A (enExample) |
| JP (1) | JPS604933B2 (enExample) |
| AU (1) | AU511779B2 (enExample) |
| CA (1) | CA1103054A (enExample) |
| DD (1) | DD132213A5 (enExample) |
| DE (1) | DE2720486C2 (enExample) |
| FR (1) | FR2350594A1 (enExample) |
| GB (1) | GB1574812A (enExample) |
| IT (1) | IT1079624B (enExample) |
| SE (1) | SE421833B (enExample) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2819711C2 (de) * | 1978-05-05 | 1984-02-16 | Gesellschaft für Strahlen- und Umweltforschung mbH, 8000 München | Verfahren und Vorrichtung zur Analyse einer Probe mit Hilfe gepulster Laserstrahlung |
| DE3125335A1 (de) * | 1981-06-27 | 1983-01-13 | Alfred Prof. Dr. 4400 Münster Benninghoven | Verfahren zur analyse von gasen und fluessigkeiten |
| IL65176A0 (en) * | 1982-03-05 | 1982-05-31 | C I Ltd | Material testing method and apparatus |
| US4504964A (en) * | 1982-09-20 | 1985-03-12 | Eaton Corporation | Laser beam plasma pinch X-ray system |
| US4536884A (en) * | 1982-09-20 | 1985-08-20 | Eaton Corporation | Plasma pinch X-ray apparatus |
| US4618971A (en) * | 1982-09-20 | 1986-10-21 | Eaton Corporation | X-ray lithography system |
| US4633492A (en) * | 1982-09-20 | 1986-12-30 | Eaton Corporation | Plasma pinch X-ray method |
| GB8322709D0 (en) * | 1983-08-24 | 1983-09-28 | British Steel Corp | Analysis of materials |
| FI81453C (fi) * | 1988-06-22 | 1990-10-10 | Outokumpu Oy | Analysatortaetning. |
| EP0458622A3 (en) * | 1990-05-22 | 1992-01-22 | Barringer Technologies Inc. | Method and apparatus for collection and analysis of desquamated skin particulates or other tissue |
| US5210412A (en) * | 1991-01-31 | 1993-05-11 | Wayne State University | Method for analyzing an organic sample |
| FR2714464B1 (fr) * | 1993-12-23 | 1996-02-09 | Cogema | Procédé de contrôle de la contamination surfacique d'un solide et dispositif de mise en Óoeuvre. |
| US5859375A (en) * | 1996-04-03 | 1999-01-12 | Barringer Research Limited | Apparatus for and method of collecting trace samples for analysis |
| FR2752325B1 (fr) * | 1996-08-06 | 1998-10-09 | Cogema | Procede et dispositif de depouissierage de pastilles de combustible nucleaire au moyen d'un faisceau laser |
| US5741984A (en) * | 1996-10-21 | 1998-04-21 | Barringer Technologies Inc. | Method and apparatus for sample collection by a token |
| DE19805569C1 (de) * | 1998-02-12 | 1999-10-07 | Bruker Saxonia Analytik Gmbh | Verfahren zur Detektion von Substanzspuren mit lösungsmittelunterstützter Dosierung und Ionen-Mobilitätsspektrometer zur Durchführung des Verfahrens |
| US6002478A (en) * | 1998-03-20 | 1999-12-14 | Transgenomic Inc. | System and method of determining trace elements in high viscosity liquids, and powders, utilizing laser-ablation |
| US6446514B1 (en) | 2000-01-18 | 2002-09-10 | Barringer Research Limited | Combined particle/vapor sampler |
| US6946300B2 (en) * | 2002-02-01 | 2005-09-20 | Control Screening, Llc | Multi-modal detection of explosives, narcotics, and other chemical substances |
| US6797944B2 (en) | 2002-02-01 | 2004-09-28 | Control Screening, Llc | Laser desorption and detection of explosives, narcotics, and other chemical substances |
| US7687276B2 (en) * | 2002-05-30 | 2010-03-30 | Massachusetts Institute Of Technology | Method of detecting analyte vaporized from sample with low-power UV radiation |
| US6847446B2 (en) * | 2003-03-25 | 2005-01-25 | The United States Of America As Represented By The Secretary Of The Navy | Chemical analysis and detection by selective adsorbent sampling and laser induced breakdown spectroscopy |
| US7113277B2 (en) * | 2003-05-14 | 2006-09-26 | Lockheed Martin Corporation | System and method of aerosolized agent capture and detection |
| WO2007032017A2 (en) * | 2005-09-14 | 2007-03-22 | Hamish Chandru Shahani | Devitalizing viruses in medical laser plumes |
| US7421912B2 (en) * | 2005-12-16 | 2008-09-09 | Smiths Detection, Inc. | Sampling device |
| CZ304648B6 (cs) * | 2007-12-03 | 2014-08-20 | Masarykova Univerzita | Způsob přípravy vzorků pro atomové spektrometrické techniky |
| US8687189B2 (en) * | 2008-03-03 | 2014-04-01 | Ajjer, Llc | Analysis of arrays by laser induced breakdown spectroscopy |
| US20100207038A1 (en) * | 2009-02-13 | 2010-08-19 | Loughborough University | Apparatus and method for laser irradiation |
| EP2239553A1 (en) * | 2009-04-09 | 2010-10-13 | Total S.A. | A carbon compounds collecting system |
| US8506686B2 (en) * | 2010-02-03 | 2013-08-13 | Midwest Research Institute, Inc. | Reel-to-reel bioforensic aerosol collection and storage system |
| CZ2010303A3 (cs) * | 2010-04-19 | 2012-01-11 | Masarykova Univerzita | Zpusob tvorby aerosolu vzorku pro atomové spektrometrické techniky |
| AU2014214888B2 (en) * | 2013-02-09 | 2018-04-05 | Elemental Scientific Lasers, Llc | In-chamber fluid handling system and methods handling fluids using the same |
| US10285255B2 (en) | 2013-02-14 | 2019-05-07 | Elemental Scientific Lasers, Llc | Laser ablation cell and injector system for a compositional analysis system |
| TW201447259A (zh) * | 2013-02-14 | 2014-12-16 | Electro Scient Ind Inc | 用於組成分析系統的雷射剝蝕單元和火炬系統 |
| DE102015114956A1 (de) * | 2015-09-07 | 2017-03-09 | Julius-Maximilians-Universität Würzburg | Vorrichtung und Verfahren zum massenhaften Sammeln von Proben |
| US9958395B2 (en) * | 2016-02-12 | 2018-05-01 | Bwt Property, Inc. | Laser induced breakdown spectroscopy (LIBS) apparatus for the detection of mineral and metal contamination in liquid samples |
| WO2018073443A1 (en) * | 2016-10-21 | 2018-04-26 | Ruprecht-Karls-Universität Heidelberg | Microtome, scanning electron microscope and method for preparing thin slices from a sample and method for analysing thin slices produced from a sample in a scanning electron microscope and use of a magnetic tape for the purpose of depositing and transporting of thin slices of samples in the field of scanning electron microscopy |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3511029A (en) * | 1969-07-08 | 1970-05-12 | Continental Oil Co | Method and apparatus for chromatography sample preparation |
| FR2193200B1 (enExample) * | 1972-07-19 | 1975-03-07 | Ctre Etu Rech Liants H | |
| US3832060A (en) * | 1972-08-10 | 1974-08-27 | Applied Res Lab | Method of preparing analyte material for spectrochemical analysis |
| FR2178555A5 (enExample) * | 1972-12-21 | 1973-11-09 | Petroles Cie Francaise | |
| DE2526679C2 (de) * | 1975-06-14 | 1986-01-09 | Bodenseewerk Perkin-Elmer & Co GmbH, 7770 Überlingen | Verfahren und Vorrichtung zum Untersuchen von Proben in einem Atomabsorptionsspektrometer |
-
1976
- 1976-05-06 GB GB18536/76A patent/GB1574812A/en not_active Expired
-
1977
- 1977-04-28 US US05/791,766 patent/US4220414A/en not_active Expired - Lifetime
- 1977-04-29 CA CA277,443A patent/CA1103054A/en not_active Expired
- 1977-05-04 IT IT49249/77A patent/IT1079624B/it active
- 1977-05-05 SE SE7705228A patent/SE421833B/xx unknown
- 1977-05-05 DE DE2720486A patent/DE2720486C2/de not_active Expired
- 1977-05-06 AU AU24973/77A patent/AU511779B2/en not_active Expired
- 1977-05-06 FR FR7713843A patent/FR2350594A1/fr active Granted
- 1977-05-06 JP JP52051916A patent/JPS604933B2/ja not_active Expired
- 1977-06-06 DD DD7700199323A patent/DD132213A5/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IT1079624B (it) | 1985-05-13 |
| GB1574812A (en) | 1980-09-10 |
| US4220414A (en) | 1980-09-02 |
| FR2350594B1 (enExample) | 1983-07-22 |
| FR2350594A1 (fr) | 1977-12-02 |
| DE2720486A1 (de) | 1977-11-24 |
| SE7705228L (sv) | 1977-11-07 |
| JPS52138991A (en) | 1977-11-19 |
| AU2497377A (en) | 1978-11-09 |
| AU511779B2 (en) | 1980-09-04 |
| SE421833B (sv) | 1982-02-01 |
| DE2720486C2 (de) | 1985-03-07 |
| CA1103054A (en) | 1981-06-16 |
| DD132213A5 (de) | 1978-09-06 |
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