JPS60204607A - 立方晶窒化ホウ素の合成法 - Google Patents
立方晶窒化ホウ素の合成法Info
- Publication number
- JPS60204607A JPS60204607A JP6347284A JP6347284A JPS60204607A JP S60204607 A JPS60204607 A JP S60204607A JP 6347284 A JP6347284 A JP 6347284A JP 6347284 A JP6347284 A JP 6347284A JP S60204607 A JPS60204607 A JP S60204607A
- Authority
- JP
- Japan
- Prior art keywords
- boron nitride
- cubic boron
- borazine
- catalyst
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052582 BN Inorganic materials 0.000 title claims abstract description 110
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims abstract description 109
- 239000013078 crystal Substances 0.000 title abstract description 8
- 230000015572 biosynthetic process Effects 0.000 title description 6
- 238000003786 synthesis reaction Methods 0.000 title description 6
- BGECDVWSWDRFSP-UHFFFAOYSA-N borazine Chemical group B1NBNBN1 BGECDVWSWDRFSP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000003054 catalyst Substances 0.000 claims abstract description 23
- 238000006243 chemical reaction Methods 0.000 claims abstract description 15
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 229910052751 metal Inorganic materials 0.000 claims abstract description 7
- 239000002184 metal Substances 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 22
- 230000002194 synthesizing effect Effects 0.000 claims description 9
- 150000002736 metal compounds Chemical class 0.000 claims description 2
- 238000005979 thermal decomposition reaction Methods 0.000 abstract description 4
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- 229910000765 intermetallic Inorganic materials 0.000 abstract 2
- 229910052796 boron Inorganic materials 0.000 description 9
- 238000001308 synthesis method Methods 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 8
- 239000002994 raw material Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 230000003197 catalytic effect Effects 0.000 description 6
- 229910052782 aluminium Inorganic materials 0.000 description 5
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 238000002441 X-ray diffraction Methods 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 150000001639 boron compounds Chemical group 0.000 description 3
- 150000001923 cyclic compounds Chemical class 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- -1 Zr gr rt Chemical class 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910052787 antimony Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910052984 zinc sulfide Inorganic materials 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- 102100040051 Aprataxin and PNK-like factor Human genes 0.000 description 1
- 101000890463 Homo sapiens Aprataxin and PNK-like factor Proteins 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 238000004566 IR spectroscopy Methods 0.000 description 1
- DQKRGOJBRLKONB-UHFFFAOYSA-N NB1NBNB(N1)N Chemical compound NB1NBNB(N1)N DQKRGOJBRLKONB-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 229910052790 beryllium Inorganic materials 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 229910052730 francium Inorganic materials 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000007542 hardness measurement Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- IDBFBDSKYCUNPW-UHFFFAOYSA-N lithium nitride Chemical compound [Li]N([Li])[Li] IDBFBDSKYCUNPW-UHFFFAOYSA-N 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000000634 powder X-ray diffraction Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Landscapes
- Ceramic Products (AREA)
- Catalysts (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6347284A JPS60204607A (ja) | 1984-03-30 | 1984-03-30 | 立方晶窒化ホウ素の合成法 |
| US06/667,802 US4545968A (en) | 1984-03-30 | 1984-11-02 | Methods for preparing cubic boron nitride sintered body and cubic boron nitride, and method for preparing boron nitride for use in the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6347284A JPS60204607A (ja) | 1984-03-30 | 1984-03-30 | 立方晶窒化ホウ素の合成法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60204607A true JPS60204607A (ja) | 1985-10-16 |
| JPS6255896B2 JPS6255896B2 (enrdf_load_stackoverflow) | 1987-11-21 |
Family
ID=13230203
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP6347284A Granted JPS60204607A (ja) | 1984-03-30 | 1984-03-30 | 立方晶窒化ホウ素の合成法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60204607A (enrdf_load_stackoverflow) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62108717A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108716A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108715A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108706A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108714A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108708A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108711A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108713A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108707A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108709A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108712A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108710A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
-
1984
- 1984-03-30 JP JP6347284A patent/JPS60204607A/ja active Granted
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62108717A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108716A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108715A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108706A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108714A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108708A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108711A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108713A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108707A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108709A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108712A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
| JPS62108710A (ja) * | 1985-11-07 | 1987-05-20 | Denki Kagaku Kogyo Kk | 立方晶窒化ほう素の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6255896B2 (enrdf_load_stackoverflow) | 1987-11-21 |
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