JPS5956590A - 銅電解廃液からの硫酸ニツケルの回収方法 - Google Patents
銅電解廃液からの硫酸ニツケルの回収方法Info
- Publication number
- JPS5956590A JPS5956590A JP57165852A JP16585282A JPS5956590A JP S5956590 A JPS5956590 A JP S5956590A JP 57165852 A JP57165852 A JP 57165852A JP 16585282 A JP16585282 A JP 16585282A JP S5956590 A JPS5956590 A JP S5956590A
- Authority
- JP
- Japan
- Prior art keywords
- copper
- waste liquid
- sulfuric acid
- solution
- nickel sulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010949 copper Substances 0.000 title claims abstract description 29
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 27
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title claims abstract description 17
- 239000002699 waste material Substances 0.000 title claims abstract description 16
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 title claims abstract description 13
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 title claims abstract description 13
- 239000007788 liquid Substances 0.000 title abstract description 19
- 238000005868 electrolysis reaction Methods 0.000 title description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000003513 alkali Substances 0.000 claims abstract description 10
- 238000000502 dialysis Methods 0.000 claims abstract description 10
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 17
- 239000002244 precipitate Substances 0.000 claims description 15
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 238000002386 leaching Methods 0.000 claims 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract description 19
- 238000011282 treatment Methods 0.000 abstract description 12
- 239000000706 filtrate Substances 0.000 abstract description 6
- 229910052742 iron Inorganic materials 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 3
- 238000007670 refining Methods 0.000 abstract 2
- 229910000366 copper(II) sulfate Inorganic materials 0.000 abstract 1
- JZCCFEFSEZPSOG-UHFFFAOYSA-L copper(II) sulfate pentahydrate Chemical compound O.O.O.O.O.[Cu+2].[O-]S([O-])(=O)=O JZCCFEFSEZPSOG-UHFFFAOYSA-L 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 abstract 1
- QOSATHPSBFQAML-UHFFFAOYSA-N hydrogen peroxide;hydrate Chemical compound O.OO QOSATHPSBFQAML-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000010979 pH adjustment Methods 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 4
- 235000011116 calcium hydroxide Nutrition 0.000 description 4
- 239000000920 calcium hydroxide Substances 0.000 description 4
- 230000003472 neutralizing effect Effects 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 238000006386 neutralization reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000010440 gypsum Substances 0.000 description 2
- 229910052602 gypsum Inorganic materials 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 239000011505 plaster Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 241000237858 Gastropoda Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001879 copper Chemical class 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000000385 dialysis solution Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000004678 hydrides Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000010841 municipal wastewater Substances 0.000 description 1
- 229910000480 nickel oxide Inorganic materials 0.000 description 1
- 239000006259 organic additive Substances 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Manufacture And Refinement Of Metals (AREA)
- Electrolytic Production Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57165852A JPS5956590A (ja) | 1982-09-22 | 1982-09-22 | 銅電解廃液からの硫酸ニツケルの回収方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57165852A JPS5956590A (ja) | 1982-09-22 | 1982-09-22 | 銅電解廃液からの硫酸ニツケルの回収方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5956590A true JPS5956590A (ja) | 1984-04-02 |
| JPH0123556B2 JPH0123556B2 (enrdf_load_stackoverflow) | 1989-05-02 |
Family
ID=15820215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57165852A Granted JPS5956590A (ja) | 1982-09-22 | 1982-09-22 | 銅電解廃液からの硫酸ニツケルの回収方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5956590A (enrdf_load_stackoverflow) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6318091A (ja) * | 1986-07-09 | 1988-01-25 | Dowa Mining Co Ltd | 銅電解液の浄液法 |
| JP2006347815A (ja) * | 2005-06-16 | 2006-12-28 | Astec Irie Co Ltd | 多成分含有ニッケルめっき廃液スラッジの再資源化処理方法 |
| JP2011246795A (ja) * | 2010-05-31 | 2011-12-08 | Sumitomo Metal Mining Co Ltd | 銅電解廃液からの銅の回収方法 |
| CN109280943A (zh) * | 2018-10-30 | 2019-01-29 | 金川集团股份有限公司 | 一种铜电解液电蒸发脱镍槽壁上结晶洗脱方法 |
| CN109338446A (zh) * | 2018-10-30 | 2019-02-15 | 金川集团股份有限公司 | 一种析出铜电解废液中的镍离子结晶的方法 |
-
1982
- 1982-09-22 JP JP57165852A patent/JPS5956590A/ja active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6318091A (ja) * | 1986-07-09 | 1988-01-25 | Dowa Mining Co Ltd | 銅電解液の浄液法 |
| JP2006347815A (ja) * | 2005-06-16 | 2006-12-28 | Astec Irie Co Ltd | 多成分含有ニッケルめっき廃液スラッジの再資源化処理方法 |
| JP2011246795A (ja) * | 2010-05-31 | 2011-12-08 | Sumitomo Metal Mining Co Ltd | 銅電解廃液からの銅の回収方法 |
| CN109280943A (zh) * | 2018-10-30 | 2019-01-29 | 金川集团股份有限公司 | 一种铜电解液电蒸发脱镍槽壁上结晶洗脱方法 |
| CN109338446A (zh) * | 2018-10-30 | 2019-02-15 | 金川集团股份有限公司 | 一种析出铜电解废液中的镍离子结晶的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0123556B2 (enrdf_load_stackoverflow) | 1989-05-02 |
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