JPS59133228A - ポリカ−ボネ−ト樹脂粒状体の製造法 - Google Patents
ポリカ−ボネ−ト樹脂粒状体の製造法Info
- Publication number
- JPS59133228A JPS59133228A JP797183A JP797183A JPS59133228A JP S59133228 A JPS59133228 A JP S59133228A JP 797183 A JP797183 A JP 797183A JP 797183 A JP797183 A JP 797183A JP S59133228 A JPS59133228 A JP S59133228A
- Authority
- JP
- Japan
- Prior art keywords
- polycarbonate resin
- tank
- methylene chloride
- water
- granules
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920005668 polycarbonate resin Polymers 0.000 title claims abstract description 75
- 239000004431 polycarbonate resin Substances 0.000 title claims abstract description 75
- 239000008187 granular material Substances 0.000 title claims description 55
- 238000004519 manufacturing process Methods 0.000 title claims description 12
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims abstract description 153
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 85
- 239000002002 slurry Substances 0.000 claims abstract description 64
- 238000005469 granulation Methods 0.000 claims abstract description 52
- 230000003179 granulation Effects 0.000 claims abstract description 52
- 150000001875 compounds Chemical class 0.000 claims abstract description 9
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 229920005989 resin Polymers 0.000 claims abstract description 7
- 239000011347 resin Substances 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 3
- 239000000725 suspension Substances 0.000 claims abstract description 3
- 229920000515 polycarbonate Polymers 0.000 claims description 33
- 239000004417 polycarbonate Substances 0.000 claims description 33
- 238000000034 method Methods 0.000 claims description 12
- 238000001704 evaporation Methods 0.000 claims description 9
- 230000008020 evaporation Effects 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 5
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 239000002245 particle Substances 0.000 abstract description 30
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 abstract 2
- 238000000227 grinding Methods 0.000 abstract 1
- 230000003134 recirculating effect Effects 0.000 abstract 1
- 238000001238 wet grinding Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 28
- 239000000047 product Substances 0.000 description 17
- 229920000642 polymer Polymers 0.000 description 16
- 238000003756 stirring Methods 0.000 description 15
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 14
- 238000000605 extraction Methods 0.000 description 8
- 238000010298 pulverizing process Methods 0.000 description 8
- 239000001294 propane Substances 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 4
- 235000013339 cereals Nutrition 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 150000002430 hydrocarbons Chemical group 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000008400 supply water Substances 0.000 description 3
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- -1 diaryl compound Chemical class 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 125000005843 halogen group Chemical group 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- CXKWCBBOMKCUKX-UHFFFAOYSA-M methylene blue Chemical compound [Cl-].C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 CXKWCBBOMKCUKX-UHFFFAOYSA-M 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- JKTORXLUQLQJCM-UHFFFAOYSA-N 4-phosphonobutylphosphonic acid Chemical compound OP(O)(=O)CCCCP(O)(O)=O JKTORXLUQLQJCM-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 101150110550 Bo17 gene Proteins 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 241000282994 Cervidae Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000218691 Cupressaceae Species 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 235000011511 Diospyros Nutrition 0.000 description 1
- 244000236655 Diospyros kaki Species 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 238000012695 Interfacial polymerization Methods 0.000 description 1
- 241000283986 Lepus Species 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 206010000269 abscess Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- ZPUCINDJVBIVPJ-LJISPDSOSA-N cocaine Chemical compound O([C@H]1C[C@@H]2CC[C@@H](N2C)[C@H]1C(=O)OC)C(=O)C1=CC=CC=C1 ZPUCINDJVBIVPJ-LJISPDSOSA-N 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 150000001924 cycloalkanes Chemical class 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000002550 fecal effect Effects 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 125000005027 hydroxyaryl group Chemical group 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229960000907 methylthioninium chloride Drugs 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 150000003462 sulfoxides Chemical class 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000020985 whole grains Nutrition 0.000 description 1
Landscapes
- Processes Of Treating Macromolecular Substances (AREA)
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP797183A JPS59133228A (ja) | 1983-01-20 | 1983-01-20 | ポリカ−ボネ−ト樹脂粒状体の製造法 |
US06/568,422 US4546172A (en) | 1983-01-20 | 1984-01-05 | Process for producing polycarbonate resin particles |
DE8484100242T DE3468225D1 (en) | 1983-01-20 | 1984-01-11 | Process for producing polycarbonate resin particles |
EP84100242A EP0116836B1 (en) | 1983-01-20 | 1984-01-11 | Process for producing polycarbonate resin particles |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP797183A JPS59133228A (ja) | 1983-01-20 | 1983-01-20 | ポリカ−ボネ−ト樹脂粒状体の製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS59133228A true JPS59133228A (ja) | 1984-07-31 |
JPS6354011B2 JPS6354011B2 (enrdf_load_stackoverflow) | 1988-10-26 |
Family
ID=11680345
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP797183A Granted JPS59133228A (ja) | 1983-01-20 | 1983-01-20 | ポリカ−ボネ−ト樹脂粒状体の製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS59133228A (enrdf_load_stackoverflow) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60202126A (ja) * | 1984-03-28 | 1985-10-12 | Teijin Chem Ltd | ポリカ−ボネ−ト粒状体の製造方法 |
JPS6172055A (ja) * | 1984-09-18 | 1986-04-14 | Mitsubishi Chem Ind Ltd | ポリカ−ボネ−ト樹脂粒状体組成物 |
JPS6176530A (ja) * | 1984-09-21 | 1986-04-19 | Mitsubishi Chem Ind Ltd | ポリカ−ボネ−ト樹脂成形品の製造法 |
JPS61250026A (ja) * | 1985-04-27 | 1986-11-07 | Mitsubishi Gas Chem Co Inc | ビ−ズ状ポリカ−ボネ−ト固形粒子の水スラリ−液の製造法 |
JPS63286436A (ja) * | 1987-05-19 | 1988-11-24 | Teijin Chem Ltd | ポリカ−ボネ−ト粒状体の製造方法 |
US5196507A (en) * | 1991-01-24 | 1993-03-23 | Mitsui Toatsu Chemicals, Inc. | Process for producing granules of polycarbonate and composition thereof |
JP2010053169A (ja) * | 2008-08-26 | 2010-03-11 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
JP2010106182A (ja) * | 2008-10-31 | 2010-05-13 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5446083B2 (ja) * | 2007-10-19 | 2014-03-19 | 三菱化学株式会社 | ポリカーボネート樹脂粒状体の製造方法 |
JP2011026471A (ja) * | 2009-07-27 | 2011-02-10 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
JP2012025860A (ja) * | 2010-07-23 | 2012-02-09 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3267074A (en) * | 1962-11-02 | 1966-08-16 | Mobay Chemical Corp | Process for producing polycarbonates |
US3294741A (en) * | 1959-04-25 | 1966-12-27 | Bayer Ag | Method of making polycarbonate particles |
JPS5544098A (en) * | 1978-09-22 | 1980-03-28 | Siemens Ag | Arc suppression device for trolley line sorter |
-
1983
- 1983-01-20 JP JP797183A patent/JPS59133228A/ja active Granted
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3294741A (en) * | 1959-04-25 | 1966-12-27 | Bayer Ag | Method of making polycarbonate particles |
US3267074A (en) * | 1962-11-02 | 1966-08-16 | Mobay Chemical Corp | Process for producing polycarbonates |
JPS5544098A (en) * | 1978-09-22 | 1980-03-28 | Siemens Ag | Arc suppression device for trolley line sorter |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60202126A (ja) * | 1984-03-28 | 1985-10-12 | Teijin Chem Ltd | ポリカ−ボネ−ト粒状体の製造方法 |
JPS6172055A (ja) * | 1984-09-18 | 1986-04-14 | Mitsubishi Chem Ind Ltd | ポリカ−ボネ−ト樹脂粒状体組成物 |
JPS6176530A (ja) * | 1984-09-21 | 1986-04-19 | Mitsubishi Chem Ind Ltd | ポリカ−ボネ−ト樹脂成形品の製造法 |
JPS61250026A (ja) * | 1985-04-27 | 1986-11-07 | Mitsubishi Gas Chem Co Inc | ビ−ズ状ポリカ−ボネ−ト固形粒子の水スラリ−液の製造法 |
JPS63286436A (ja) * | 1987-05-19 | 1988-11-24 | Teijin Chem Ltd | ポリカ−ボネ−ト粒状体の製造方法 |
US5196507A (en) * | 1991-01-24 | 1993-03-23 | Mitsui Toatsu Chemicals, Inc. | Process for producing granules of polycarbonate and composition thereof |
JP2010053169A (ja) * | 2008-08-26 | 2010-03-11 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
JP2010106182A (ja) * | 2008-10-31 | 2010-05-13 | Teijin Chem Ltd | ポリカーボネート粒状体の連続製造方法 |
Also Published As
Publication number | Publication date |
---|---|
JPS6354011B2 (enrdf_load_stackoverflow) | 1988-10-26 |
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