JPS5852986B2 - ベタイン複塩の製造法 - Google Patents
ベタイン複塩の製造法Info
- Publication number
- JPS5852986B2 JPS5852986B2 JP50029438A JP2943875A JPS5852986B2 JP S5852986 B2 JPS5852986 B2 JP S5852986B2 JP 50029438 A JP50029438 A JP 50029438A JP 2943875 A JP2943875 A JP 2943875A JP S5852986 B2 JPS5852986 B2 JP S5852986B2
- Authority
- JP
- Japan
- Prior art keywords
- betaine
- water
- double salt
- solution
- moles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 title claims description 117
- 229960003237 betaine Drugs 0.000 title claims description 59
- 150000003839 salts Chemical class 0.000 title claims description 37
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 43
- 239000000243 solution Substances 0.000 claims description 39
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 27
- 239000000203 mixture Substances 0.000 claims description 23
- 229960003403 betaine hydrochloride Drugs 0.000 claims description 9
- HOPSCVCBEOCPJZ-UHFFFAOYSA-N carboxymethyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CC(O)=O HOPSCVCBEOCPJZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000011734 sodium Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 150000002500 ions Chemical class 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 27
- 238000002425 crystallisation Methods 0.000 description 14
- 230000008025 crystallization Effects 0.000 description 13
- 239000011780 sodium chloride Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 12
- 235000013372 meat Nutrition 0.000 description 9
- 239000013078 crystal Substances 0.000 description 8
- 239000000796 flavoring agent Substances 0.000 description 8
- 235000019634 flavors Nutrition 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 235000021536 Sugar beet Nutrition 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- -1 chlorine ions Chemical class 0.000 description 2
- 238000000280 densification Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 235000019264 food flavour enhancer Nutrition 0.000 description 2
- 235000011194 food seasoning agent Nutrition 0.000 description 2
- 229960002449 glycine Drugs 0.000 description 2
- 235000019643 salty taste Nutrition 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- QCQCHGYLTSGIGX-GHXANHINSA-N 4-[[(3ar,5ar,5br,7ar,9s,11ar,11br,13as)-5a,5b,8,8,11a-pentamethyl-3a-[(5-methylpyridine-3-carbonyl)amino]-2-oxo-1-propan-2-yl-4,5,6,7,7a,9,10,11,11b,12,13,13a-dodecahydro-3h-cyclopenta[a]chrysen-9-yl]oxy]-2,2-dimethyl-4-oxobutanoic acid Chemical compound N([C@@]12CC[C@@]3(C)[C@]4(C)CC[C@H]5C(C)(C)[C@@H](OC(=O)CC(C)(C)C(O)=O)CC[C@]5(C)[C@H]4CC[C@@H]3C1=C(C(C2)=O)C(C)C)C(=O)C1=CN=CC(C)=C1 QCQCHGYLTSGIGX-GHXANHINSA-N 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- 241001669680 Dormitator maculatus Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
- 229940106681 chloroacetic acid Drugs 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001035 methylating effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/21—Synthetic spices, flavouring agents or condiments containing amino acids
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Seasonings (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH341274A CH586653A5 (OSRAM) | 1974-03-12 | 1974-03-12 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS50123623A JPS50123623A (OSRAM) | 1975-09-29 |
| JPS5852986B2 true JPS5852986B2 (ja) | 1983-11-26 |
Family
ID=4255422
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP50029438A Expired JPS5852986B2 (ja) | 1974-03-12 | 1975-03-11 | ベタイン複塩の製造法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4652711A (OSRAM) |
| JP (1) | JPS5852986B2 (OSRAM) |
| CH (1) | CH586653A5 (OSRAM) |
| DE (1) | DE2506151C3 (OSRAM) |
| FR (1) | FR2264004B1 (OSRAM) |
| GB (1) | GB1467535A (OSRAM) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4530799A (en) * | 1974-03-12 | 1985-07-23 | Nestec S. A. | Betaine derivative |
| JPS5285115A (en) * | 1976-01-09 | 1977-07-15 | Nestle Sa | Betaine double salt |
| US5156845A (en) * | 1990-05-04 | 1992-10-20 | Colgate-Palmolive Company | Dry mouth lozenge |
| FI99260C (fi) * | 1996-03-01 | 1998-01-26 | Neste Oy | Lämmönsiirtoneste |
| ES2255489T3 (es) | 1999-02-24 | 2006-07-01 | Danisco Usa, Inc. | Betaina y productos de panaderia. |
| US20100197809A1 (en) * | 2009-02-04 | 2010-08-05 | Ortiz Alvaro Ernesto | Skin solution and preparation method thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1219226A (en) * | 1914-03-04 | 1917-03-13 | Agfa Ag | Process for the manufacture of betain from vinasses. |
| US2549763A (en) * | 1950-01-17 | 1951-04-24 | Jr Thomas F Banigan | Process of isolating betaine from guayule extract |
| FR1437540A (fr) * | 1965-03-22 | 1966-05-06 | Kuhlmann Ets | Procédé de préparation d'hydrate de bétaïne |
| US4359430A (en) * | 1980-02-29 | 1982-11-16 | Suomen Sokeri Osakeyhtio | Betaine recovery process |
-
1974
- 1974-03-12 CH CH341274A patent/CH586653A5/xx not_active IP Right Cessation
-
1975
- 1975-01-27 GB GB340075A patent/GB1467535A/en not_active Expired
- 1975-01-31 FR FR7503161A patent/FR2264004B1/fr not_active Expired
- 1975-02-14 DE DE2506151A patent/DE2506151C3/de not_active Expired
- 1975-03-11 JP JP50029438A patent/JPS5852986B2/ja not_active Expired
-
1985
- 1985-02-04 US US06/697,881 patent/US4652711A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CH586653A5 (OSRAM) | 1977-04-15 |
| FR2264004B1 (OSRAM) | 1979-09-28 |
| DE2506151B2 (de) | 1977-07-21 |
| GB1467535A (en) | 1977-03-16 |
| DE2506151A1 (de) | 1975-09-18 |
| FR2264004A1 (OSRAM) | 1975-10-10 |
| DE2506151C3 (de) | 1978-03-02 |
| US4652711A (en) | 1987-03-24 |
| JPS50123623A (OSRAM) | 1975-09-29 |
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