JPS58157941A - Permanent magnet alloy - Google Patents

Permanent magnet alloy

Info

Publication number
JPS58157941A
JPS58157941A JP57039812A JP3981282A JPS58157941A JP S58157941 A JPS58157941 A JP S58157941A JP 57039812 A JP57039812 A JP 57039812A JP 3981282 A JP3981282 A JP 3981282A JP S58157941 A JPS58157941 A JP S58157941A
Authority
JP
Japan
Prior art keywords
permanent magnet
magnet alloy
composition
heat treatment
alloy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP57039812A
Other languages
Japanese (ja)
Inventor
Takeshi Yoshino
剛 吉野
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Panasonic Holdings Corp
Original Assignee
Matsushita Electric Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Matsushita Electric Industrial Co Ltd filed Critical Matsushita Electric Industrial Co Ltd
Priority to JP57039812A priority Critical patent/JPS58157941A/en
Publication of JPS58157941A publication Critical patent/JPS58157941A/en
Pending legal-status Critical Current

Links

Landscapes

  • Hard Magnetic Materials (AREA)

Abstract

PURPOSE:To obtain a permanent magnet alloy without requiring a complex heat treatment after sintering by providing a composition consisting of specified amounts of 1 or >=2 kinds of rare earth metals such as Sm and Ce, Co, Cu, Mn and >=1 kind of element selected from Zr, Zn, Ti, Hf and Mo. CONSTITUTION:The composition of this permanent magnet alloy consists of, by weight, 22-28% of 1 or >=2 kinds of rare earh metals such as Sm and Ce, 43-61% Co, 8-12% Cu, 8-12% Mn and 1-6% of >=1 kind of element selected from Zr, Zn, Ti, Hf and Mo. A material having said composition is pulverized, and the fine powder is press-molded in a metallic mold in a magnetic field, sintered at about 1,180 deg.C in vacuum for about 60min, and cooled to obtain the permanent magnet alloy. The performance of the magnet alloy is not considerably improved even when the alloy is subjected to a complex heat treatment after the sintering.

Description

【発明の詳細な説明】 本発明はR2’017系金属間化合物(ただしRは希土
類金属)を主体とする永久磁石合金に関するものである
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a permanent magnet alloy mainly composed of an R2'017 intermetallic compound (where R is a rare earth metal).

従来のR2C01?系金属間化合物を主体とした永久磁
石合金としては、その配合組成にSs 、 co。
Conventional R2C01? Permanent magnetic alloys mainly composed of intermetallic compounds include Ss and co.

we、cuの基本4元素あるいはそれに添加物を加えた
もので構成されており、高性能な永久磁石合金が得られ
るとされていた。
It is composed of the four basic elements of we and cu, or additives added to them, and was said to produce a high-performance permanent magnet alloy.

しかしながら、従来のこの種の永久磁石合金に共通して
いえることは高い飽和磁束密度(Br)を得るために多
量のyeを含んでいた。このため、保磁力(He)がか
なり犠牲になっていた。
However, a common feature of conventional permanent magnet alloys of this type is that they contain a large amount of ye in order to obtain a high saturation magnetic flux density (Br). For this reason, the coercive force (He) was considerably sacrificed.

このようなことから最近ではこの保磁力(He)を高め
るために添加物を加えたり、温度9時間を段階的に変化
させるなどの複雑な熱処理工程が開発されているがいま
だ、十分満足できるものが得られるにいたっていない。
For this reason, complex heat treatment processes such as adding additives and changing the temperature stepwise over 9 hours have recently been developed to increase the coercive force (He), but these are still not fully satisfactory. has not yet been achieved.

本発明は以上のような従来の欠点を除去するものであり
、焼結後複雑な熱処理をしなくても安定した保磁力の得
られる永久磁石合金を提供することを目的とするもので
ある。
The present invention eliminates the above-mentioned conventional drawbacks, and aims to provide a permanent magnet alloy that can obtain stable coercive force without complicated heat treatment after sintering.

以下、本発明の一実施例について説明する。An embodiment of the present invention will be described below.

重量%で27%のSB、51.1%のco  、1oa
%のOu、8%のMn、3%のM(Mとして2.2%の
Zrと0.8%のZn )からなる材料を真空溶解しs
N2  ガスを用いたジェットミル粉砕機により微粉砕
粉を作り、この微粉砕粉を12KO6の磁界中でato
n/cJの圧力で金型を用いて成形する。
Weight% 27% SB, 51.1% co, 1 oa
A material consisting of % Ou, 8% Mn, and 3% M (2.2% Zr and 0.8% Zn as M) was melted in vacuum.
Finely pulverized powder is made using a jet mill using N2 gas, and this finely pulverized powder is atomized in a magnetic field of 12KO6.
Molding is performed using a mold at a pressure of n/cJ.

この成形体を真空中で118 o’cの温度で60分間
焼結し、800°Cまでを3〜6°O15+で急冷し、
その後は2oO0Cまで10°C/分にて徐冷して永久
磁石合金を得た。
This compact was sintered in vacuum at a temperature of 118 o'c for 60 minutes, quenched to 800°C at 3-6° O15+,
Thereafter, it was slowly cooled to 2oOOC at a rate of 10°C/min to obtain a permanent magnet alloy.

この永久磁石合金の磁気特性は下記の第1表に示す通り
である。さらにこの永久磁石合金を従来と同様に真空中
で800°Cにて60分間加熱しその後2008Cまで
6°C15+で徐冷する熱処理を行ったものの磁気特性
を比較のため第1表に並記した。
The magnetic properties of this permanent magnet alloy are shown in Table 1 below. Furthermore, this permanent magnet alloy was heat treated in a vacuum at 800°C for 60 minutes and then slowly cooled to 2008°C at 6°C 15+, and the magnetic properties are listed in Table 1 for comparison. .

第   1   表 この結果、本発明の永久磁石合金は熱処理をしてもしな
くてもその性能に大差のないことが明らかである。
Table 1 As a result, it is clear that there is no significant difference in performance of the permanent magnet alloy of the present invention whether it is heat treated or not.

また、添加物Mを変えた場合の磁気特性を第2表に示す
が、これは全て前述の製造法と同じ方法で製造され、熱
処理を施さないもののデータである。
Further, Table 2 shows the magnetic properties when the additive M is changed, but all of these data are for products manufactured by the same method as described above and without heat treatment.

以上のよ、うに本発明の永久磁石合金は構成されるため
、熱処理を施さずに安定した磁気特性が得られ、生産性
の向上が計れコスト面でも有利になるなどの効果をもち
、工業的価値の大なるものである。
As described above, since the permanent magnet alloy of the present invention is constructed, stable magnetic properties can be obtained without heat treatment, productivity can be improved, and it is advantageous in terms of cost. It is of great value.

Claims (1)

【特許請求の範囲】 重量%で22〜28%のR(ただしRFib、。 aSを中心とする希土類金属の1種または2種以上の組
合せ)、43〜61%のCO,S〜12%のCu、s 
〜12%のMn、1〜5%のM(ただしMはZr 、Z
n 、 Ti 、HfおよびMOのうち少なくとも1種
以上)の組成からなることを特徴とする永久磁石合金。
[Claims] 22 to 28% R (RFib, a combination of one or more rare earth metals, mainly aS), 43 to 61% CO, and S to 12% by weight. Cu,s
~12% Mn, 1~5% M (where M is Zr, Z
A permanent magnet alloy characterized by having a composition of at least one of n, Ti, Hf, and MO.
JP57039812A 1982-03-12 1982-03-12 Permanent magnet alloy Pending JPS58157941A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP57039812A JPS58157941A (en) 1982-03-12 1982-03-12 Permanent magnet alloy

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP57039812A JPS58157941A (en) 1982-03-12 1982-03-12 Permanent magnet alloy

Publications (1)

Publication Number Publication Date
JPS58157941A true JPS58157941A (en) 1983-09-20

Family

ID=12563375

Family Applications (1)

Application Number Title Priority Date Filing Date
JP57039812A Pending JPS58157941A (en) 1982-03-12 1982-03-12 Permanent magnet alloy

Country Status (1)

Country Link
JP (1) JPS58157941A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111489888A (en) * 2019-01-28 2020-08-04 日立金属株式会社 Method for producing R-T-B sintered magnet

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111489888A (en) * 2019-01-28 2020-08-04 日立金属株式会社 Method for producing R-T-B sintered magnet
CN111489888B (en) * 2019-01-28 2024-01-02 株式会社博迈立铖 Method for producing R-T-B sintered magnet

Similar Documents

Publication Publication Date Title
JPH06340902A (en) Production of sintered rare earth base permanent magnet
JP2002038245A (en) Rare earth alloy powder for rermanent magnet and method for manufacturing rare earth permanent magnet
JPS6043900B2 (en) permanent magnet material
US4601876A (en) Sintered Fe-Cr-Co type magnetic alloy and method for producing article made thereof
JPS58157941A (en) Permanent magnet alloy
JPH0146575B2 (en)
JPS5952822A (en) Manufacture of permanent magnet
JPS62173704A (en) Manufacture of permanent magnet
JPS6091601A (en) Method for pulverization for rare earth-boron-iron permanent magnet alloy powder
JPH0146574B2 (en)
JPH01155603A (en) Manufacture of oxidation-resistant rare-earth permanent magnet
JPH01105502A (en) Rare earth permanent magnet exhibiting high resistance to oxidation and manufacture thereof
JPS6386502A (en) Rare earth magnet and manufacture thereof
JPS59154004A (en) Manufacture of permanent magnet
JPS5835251B2 (en) Permanent magnetic alloy containing rare earth metals
JPH0362775B2 (en)
JPS62158852A (en) Permanent magnet material
JPS594107A (en) Manufacture of rare earth and cobalt group magnetic material
JPH0252413B2 (en)
JPS6053107B2 (en) Rare earth magnet manufacturing method
JPH01289101A (en) Manufacture of rare earth transition metallic magnet alloy powder
JPH056831A (en) Manufacture of rare-earth cobalt magnet with excellent heat-resistant property
JPS6014407A (en) Permanent magnet material
JPH0732200A (en) Production of sn-containing ndfeb sintered magnet having excellent corrosion resistance
JPS63502B2 (en)