JPS5748969A - Preparation of 1-alkyl-3-methylpyrazole type compound - Google Patents
Preparation of 1-alkyl-3-methylpyrazole type compoundInfo
- Publication number
- JPS5748969A JPS5748969A JP12519280A JP12519280A JPS5748969A JP S5748969 A JPS5748969 A JP S5748969A JP 12519280 A JP12519280 A JP 12519280A JP 12519280 A JP12519280 A JP 12519280A JP S5748969 A JPS5748969 A JP S5748969A
- Authority
- JP
- Japan
- Prior art keywords
- methylpyrazole
- type compound
- alkyl
- formula
- halogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
PURPOSE: To obtain a 1-alkyl-3-methylpyrazole type compound under mild conditions in high yield, by reacting a 3-methylpyrazole type compound with an alkanol in the presence of a halogen as well as an acid.
CONSTITUTION: A 3-methylpyrazole type compound shown by the formula I [X is H, a group shown by the formula II (Y1 and Y2 are H, halogen, nitro, or trifluoromethyl)] is reacted with an alkanol, e.g., methyl alcohol, etc., to give a 1-alkyl- 3-methylpyrazole type compound shown by the formula III (R is alkyl). In the reaction, a halogen (e.g., iodine, bromine, etc.) is present besides a mineral acid or an organic sulfonic acid. In case of the compound shown by the formula I wherein X=H, the yield is ≥85%. Particularly complicate reaction operations, reaction devices, etc. are not required.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12519280A JPS5748969A (en) | 1980-09-09 | 1980-09-09 | Preparation of 1-alkyl-3-methylpyrazole type compound |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12519280A JPS5748969A (en) | 1980-09-09 | 1980-09-09 | Preparation of 1-alkyl-3-methylpyrazole type compound |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5748969A true JPS5748969A (en) | 1982-03-20 |
Family
ID=14904188
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP12519280A Pending JPS5748969A (en) | 1980-09-09 | 1980-09-09 | Preparation of 1-alkyl-3-methylpyrazole type compound |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5748969A (en) |
-
1980
- 1980-09-09 JP JP12519280A patent/JPS5748969A/en active Pending
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