JPS57139026A - Preparation of alkylene glycol - Google Patents

Preparation of alkylene glycol

Info

Publication number
JPS57139026A
JPS57139026A JP56024933A JP2493381A JPS57139026A JP S57139026 A JPS57139026 A JP S57139026A JP 56024933 A JP56024933 A JP 56024933A JP 2493381 A JP2493381 A JP 2493381A JP S57139026 A JPS57139026 A JP S57139026A
Authority
JP
Japan
Prior art keywords
compound
halogen
anion exchange
catalyst
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP56024933A
Other languages
Japanese (ja)
Other versions
JPS6056141B2 (en
Inventor
Kazutomo Takahashi
Hiroshi Odanaka
Tsuneyoshi Fujii
Toshihiko Kumazawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Priority to JP56024933A priority Critical patent/JPS6056141B2/en
Publication of JPS57139026A publication Critical patent/JPS57139026A/en
Publication of JPS6056141B2 publication Critical patent/JPS6056141B2/en
Expired legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To prepare the titled compound easily and economically, in high selectivity of especially monoalkylene glycol, by reacting an alkylene oxide with water in the presence of CO2 using a halogen-type anion exchange material as the reaction catalyst.
CONSTITUTION: A mixture composed mainly of the compound of formula II (R1WR4 are H, 1W3C alkyl, 6C aryl, 2W3C alkenyl, or 3W6C cycloalkyl) is prepared by reacting 1mol of the compound of formulaIwith 1W30mol of water in the presence of 0.0001W1mol of CO2 using a halogen-type anion exchange material as the reaction catalyst, at 80W200°C and 2W25kg/cm2G pressure. The above catalyst is suitably a commercially available anion exchange resin substituted with a halogen such as chlorine, bromine, iodine, etc., and the exchange capacity of the catalyst is 0.1W10mol% of the compound of formulaI.
COPYRIGHT: (C)1982,JPO&Japio
JP56024933A 1981-02-24 1981-02-24 Method for producing alkylene glycol Expired JPS6056141B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP56024933A JPS6056141B2 (en) 1981-02-24 1981-02-24 Method for producing alkylene glycol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56024933A JPS6056141B2 (en) 1981-02-24 1981-02-24 Method for producing alkylene glycol

Publications (2)

Publication Number Publication Date
JPS57139026A true JPS57139026A (en) 1982-08-27
JPS6056141B2 JPS6056141B2 (en) 1985-12-09

Family

ID=12151878

Family Applications (1)

Application Number Title Priority Date Filing Date
JP56024933A Expired JPS6056141B2 (en) 1981-02-24 1981-02-24 Method for producing alkylene glycol

Country Status (1)

Country Link
JP (1) JPS6056141B2 (en)

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4579983A (en) * 1984-03-28 1986-04-01 Union Carbide Corporation Process for the hydrolysis of alkylene oxides using organometalates
US4982021A (en) * 1984-03-28 1991-01-01 Union Carbide Chemicals And Plastics Company Inc. Process for the production of alkylene glycols with metalate-containing solid
WO1995020559A1 (en) * 1994-01-31 1995-08-03 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycols
WO1997019043A1 (en) * 1995-11-23 1997-05-29 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycols
JPH1112206A (en) * 1997-04-30 1999-01-19 Mitsubishi Chem Corp Production of alkylene glycols
WO1999031034A1 (en) * 1997-12-18 1999-06-24 The Dow Chemical Company A method for making glycol in an adiabatic reactor system
WO1999031033A1 (en) * 1997-12-18 1999-06-24 The Dow Chemical Company Process for the production of ethylene glycol
US6137014A (en) * 1997-10-30 2000-10-24 Shell Oil Company Catalytic hydrolysis of alkylene oxides
US6147265A (en) * 1997-04-30 2000-11-14 Mitsubishi Chemical Corporation Process for producing alkylene glycol
US6211419B1 (en) * 2000-04-24 2001-04-03 The Dow Chemical Company Process for the preparation of alkylene glycols
US6448456B1 (en) 2001-05-31 2002-09-10 The Dow Chemical Company Process for the preparation of alkylene glycols
JP2002292285A (en) * 2001-03-30 2002-10-08 Nippon Shokubai Co Ltd Preservation method of resin catalyst for addition reaction of alkylene oxide and its use
WO2009051972A1 (en) 2007-10-15 2009-04-23 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Solid catalyst useful for converting an alkylene oxide to an alkylene glycol
US7663005B2 (en) 2007-05-30 2010-02-16 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparing an alkylene glycol
WO2010131839A2 (en) 2009-05-13 2010-11-18 에스케이에너지 주식회사 Polyelectrolyte multilayer thin film catalyst and method for producing same
US8569548B2 (en) 2007-07-20 2013-10-29 Shell Oil Company Process for the preparation of alkylene glycols
CN106478365A (en) * 2015-08-25 2017-03-08 中国石油化工股份有限公司 A kind of synthetic method of vicinal diamines class compound

Cited By (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4579983A (en) * 1984-03-28 1986-04-01 Union Carbide Corporation Process for the hydrolysis of alkylene oxides using organometalates
US4982021A (en) * 1984-03-28 1991-01-01 Union Carbide Chemicals And Plastics Company Inc. Process for the production of alkylene glycols with metalate-containing solid
WO1995020559A1 (en) * 1994-01-31 1995-08-03 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycols
US5488184A (en) * 1994-01-31 1996-01-30 Shell Oil Company Process for the preparation of alkylene glycols
AU681937B2 (en) * 1994-01-31 1997-09-11 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycols
CN1071295C (en) * 1994-01-31 2001-09-19 国际壳牌研究有限公司 Process for the preparation of alkylene glycols
WO1997019043A1 (en) * 1995-11-23 1997-05-29 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycols
CN1074402C (en) * 1995-11-23 2001-11-07 国际壳牌研究有限公司 Process for the preparation of alkylene glycols
US5874653A (en) * 1995-11-23 1999-02-23 Shell Oil Company Process for the preparation of alkylene glycols
JPH1112206A (en) * 1997-04-30 1999-01-19 Mitsubishi Chem Corp Production of alkylene glycols
US6147265A (en) * 1997-04-30 2000-11-14 Mitsubishi Chemical Corporation Process for producing alkylene glycol
US6137014A (en) * 1997-10-30 2000-10-24 Shell Oil Company Catalytic hydrolysis of alkylene oxides
WO1999031033A1 (en) * 1997-12-18 1999-06-24 The Dow Chemical Company Process for the production of ethylene glycol
WO1999031034A1 (en) * 1997-12-18 1999-06-24 The Dow Chemical Company A method for making glycol in an adiabatic reactor system
US6211419B1 (en) * 2000-04-24 2001-04-03 The Dow Chemical Company Process for the preparation of alkylene glycols
WO2001083413A1 (en) * 2000-04-24 2001-11-08 Dow Global Technologies Inc. Improved process for the preparation of alkylene glycols
JP2002292285A (en) * 2001-03-30 2002-10-08 Nippon Shokubai Co Ltd Preservation method of resin catalyst for addition reaction of alkylene oxide and its use
US6448456B1 (en) 2001-05-31 2002-09-10 The Dow Chemical Company Process for the preparation of alkylene glycols
US6479715B1 (en) 2001-05-31 2002-11-12 Dow Global Technologies Inc. Process for the preparation of alkylene glycols
US7663005B2 (en) 2007-05-30 2010-02-16 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparing an alkylene glycol
US8569548B2 (en) 2007-07-20 2013-10-29 Shell Oil Company Process for the preparation of alkylene glycols
WO2009051972A1 (en) 2007-10-15 2009-04-23 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Solid catalyst useful for converting an alkylene oxide to an alkylene glycol
US8053609B2 (en) 2007-10-15 2011-11-08 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Solid catalyst useful for converting an alkylene oxide to an alkylene glycol
WO2010131839A2 (en) 2009-05-13 2010-11-18 에스케이에너지 주식회사 Polyelectrolyte multilayer thin film catalyst and method for producing same
US8784769B2 (en) 2009-05-13 2014-07-22 Sk Innovation Co., Ltd. Polyelectrolyte multilayer thin film catalyst and method for producing same
CN106478365A (en) * 2015-08-25 2017-03-08 中国石油化工股份有限公司 A kind of synthetic method of vicinal diamines class compound

Also Published As

Publication number Publication date
JPS6056141B2 (en) 1985-12-09

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