JPS5566545A - Catalytic hydrogenation of nitrobenzene - Google Patents

Catalytic hydrogenation of nitrobenzene

Info

Publication number
JPS5566545A
JPS5566545A JP10613379A JP10613379A JPS5566545A JP S5566545 A JPS5566545 A JP S5566545A JP 10613379 A JP10613379 A JP 10613379A JP 10613379 A JP10613379 A JP 10613379A JP S5566545 A JPS5566545 A JP S5566545A
Authority
JP
Japan
Prior art keywords
support
nitrobenzene
per liter
catalyst
grams
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP10613379A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0234938B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html
Inventor
Birugenshiyutotsuku Udo
Ratsuhaman Burukuharuto
Metsuten Yozefu
Shiyumitsuto Heruberuto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of JPS5566545A publication Critical patent/JPS5566545A/ja
Publication of JPH0234938B2 publication Critical patent/JPH0234938B2/ja
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/36Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56Platinum group metals
    • B01J23/64Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56Platinum group metals
    • B01J23/64Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/648Vanadium, niobium or tantalum or polonium
    • B01J23/6482Vanadium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02Impregnation, coating or precipitation
    • B01J37/0201Impregnation
    • B01J37/0205Impregnation in several steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00Constitutive chemical elements of heterogeneous catalysts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16Reducing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16Reducing
    • B01J37/18Reducing with gases containing free hydrogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP10613379A 1978-11-11 1979-08-22 Catalytic hydrogenation of nitrobenzene Granted JPS5566545A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19782849002 DE2849002A1 (de) 1978-11-11 1978-11-11 Verfahren zur katalytischen hydrierung von nitrobenzol

Publications (2)

Publication Number Publication Date
JPS5566545A true JPS5566545A (en) 1980-05-20
JPH0234938B2 JPH0234938B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1990-08-07

Family

ID=6054430

Family Applications (1)

Application Number Title Priority Date Filing Date
JP10613379A Granted JPS5566545A (en) 1978-11-11 1979-08-22 Catalytic hydrogenation of nitrobenzene

Country Status (10)

Country Link
US (1) US4265834A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP0011090B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS5566545A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
AT (1) ATE612T1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BR7905432A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CA (1) CA1136651A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (2) DE2849002A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ES (1) ES483534A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
MX (1) MX151217A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ZA (1) ZA794454B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009529549A (ja) * 2006-03-14 2009-08-20 バイエル・テクノロジー・サービシーズ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング 不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置
JP2010526791A (ja) * 2007-05-10 2010-08-05 ビーエーエスエフ ソシエタス・ヨーロピア アミンの製造方法
JP2015516970A (ja) * 2012-04-16 2015-06-18 バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG 芳香族ニトロ化合物から芳香族アミンを製造する間に反応を停止するための改良方法
JP2022546362A (ja) * 2019-08-30 2022-11-04 コベストロ、ドイチュラント、アクチエンゲゼルシャフト 芳香族ニトロ化合物を水素化する方法

Families Citing this family (37)

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US4469816A (en) * 1982-12-14 1984-09-04 Allied Corporation Palladium on alumina aerogel catalyst composition and process for making same
US4929737A (en) * 1988-02-03 1990-05-29 Eastman Kodak Company Hydrogenation of halonitroaromatic compounds
DE4039026A1 (de) * 1990-12-07 1992-06-11 Bayer Ag Verfahren zur herstellung von anilin
FR2671347B1 (fr) * 1991-01-07 1994-09-09 Inst Francais Du Petrole Reduction catalytique de composes nitroaromatiques substitues ou non en composes aminoaromatiques correspondants.
FR2682106B1 (fr) * 1991-10-04 1993-11-26 Rhone Poulenc Chimie Procede d'hydrogenation en phase vapeur utilisables pour des derives aromatiques nitres.
EP0676391B1 (de) * 1994-04-07 1998-10-14 Bayer Ag Verfahren zur Herstellung von Isocyanaten oder Isocyanatgemischen
DE4428018A1 (de) * 1994-08-08 1996-02-15 Bayer Ag Verfahren zur Herstellung von aromatischen Aminen
DE4428017A1 (de) * 1994-08-08 1996-02-15 Bayer Ag Verfahren zur Herstellung von aromatischen Aminen
DK0825979T3 (da) * 1995-05-19 2001-05-07 Novartis Ag Fremgangsmåde til fremstilling af aromatiske nitroforbindelser
DE19521587A1 (de) * 1995-06-14 1996-12-19 Bayer Ag Verfahren und Katalysator zur Herstellung von aromatischen Aminen durch Gasphasenhydrierung
DE59705933D1 (de) * 1996-06-05 2002-02-07 Basf Ag Reduktive Kopplung von Nitrobenzol oder kernsubstituierten Nitrobenzolen zu den entsprechenden Azobenzolen und Azoxybenzolen mit Redoxkatalysatoren
WO1998013331A1 (en) 1996-09-23 1998-04-02 Novartis Ag Process for the preparation of substituted aromatic amino compounds
US5962741A (en) * 1996-11-19 1999-10-05 Novartis Ag Process for the production of aromatic halogen-amino compounds
DE19651688A1 (de) * 1996-12-12 1998-06-18 Bayer Ag Verfahren zur Herstellung von aromatischen Aminen durch Gasphasenhydrierung
DE19715746A1 (de) * 1997-04-16 1998-10-22 Bayer Ag Herstellung von aromatischen Aminen mittels neuer Hydrierkatalysatoren
US6179996B1 (en) 1998-05-22 2001-01-30 Membrane Technology And Research, Inc. Selective purge for hydrogenation reactor recycle loop
DE10047435A1 (de) * 2000-09-26 2002-04-11 Degussa Verfahren zur Herstellung von Oximen
DE10208254A1 (de) * 2002-02-26 2003-09-04 Bayer Ag Katalysator
CN1301154C (zh) * 2002-11-29 2007-02-21 东北师范大学 可再生的加氢催化剂及其制备方法
DE10347439A1 (de) * 2003-10-13 2005-05-04 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen durch heterogen katalysierte Hydrierung
DE10347438A1 (de) * 2003-10-13 2005-05-04 Bayer Materialscience Ag Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe
DE102005006692A1 (de) * 2005-02-15 2006-08-24 Bayer Materialscience Ag Verfahren zur Herstellung von Di-und Polyaminen der Diphenylmethanreihe
DE102006007619A1 (de) * 2006-02-18 2007-08-23 Bayer Materialscience Ag Verfahren zur Herstellung von Anilin
DE102006035203A1 (de) * 2006-07-29 2008-01-31 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen
ATE472522T1 (de) 2006-09-19 2010-07-15 Basf Se Verfahren zur herstellung von aromatischen aminen in einem wirbelschichtreaktor
DE102009019436A1 (de) 2009-04-29 2010-11-04 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen
PT2598241E (pt) 2010-07-30 2014-07-09 Bayer Ip Gmbh Processo para restaurar a actividade de um catalisador
MX2013005523A (es) 2010-11-18 2013-07-05 Bayer Ip Gmbh Reactor quimico con material textil de malla metalica de punto como dispositivo de contencion para particulas.
CN103313963B (zh) * 2011-01-11 2015-11-25 拜耳知识产权有限责任公司 制备芳族胺的方法
DE102011081897A1 (de) * 2011-08-31 2013-02-28 Bayer Materialscience Aktiengesellschaft Katalysator und Verfahren zur Herstellung von aromatischen Aminen in der Gasphase
DE102011081898A1 (de) 2011-08-31 2013-02-28 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
EP2653462A1 (de) 2012-04-16 2013-10-23 Bayer MaterialScience AG Verfahren zum verbesserten Anfahren der Reaktion bei der Herstellung von aromatischen Aminen aus Nitroaromaten
RU2017102015A (ru) 2014-06-24 2018-07-24 Ковестро Дойчланд Аг Способ получения химических продуктов с производственными простоями
EP3500553B1 (de) 2016-08-17 2021-05-12 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung eines isocyanats und mindestens eines weiteren chemischen produkts in einem produktionsverbund
JP2019531873A (ja) 2016-08-18 2019-11-07 ザ ユニバーシティ オブ シカゴThe University Of Chicago 高度に効率的な有機変換のための金属酸化物に支持された地球に豊富な金属の触媒
JP2024508014A (ja) 2021-03-01 2024-02-21 コベストロ、ドイチュラント、アクチエンゲゼルシャフト 芳香族ニトロ化合物を水素化する方法
EP4549619A1 (en) 2023-10-31 2025-05-07 Basf Se Preparation of amines by hydrogenation of nitro compounds using hydrogen with low deuterium content

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5229731A (en) * 1975-08-28 1977-03-05 Polaroid Corp Photographic camera exposure controller

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US2823235A (en) * 1955-05-10 1958-02-11 Du Pont Hydrogenation of nitro compounds to amines and catalyst therefor
US3265636A (en) * 1963-03-26 1966-08-09 Du Pont Catalyst for the hydrogenation of nitro compounds
US3830847A (en) * 1966-11-04 1974-08-20 Grace W R & Co Selective oxidation of olefins
US3472897A (en) * 1966-12-22 1969-10-14 Grace W R & Co Reduction of nitrobenzene
US3666813A (en) * 1969-08-27 1972-05-30 Engelhard Min & Chem Process for preparing aromatic haloamines from aromatic nitroamines
DE2100373C3 (de) * 1971-01-15 1979-04-12 Institut Chimitscheskich Nauk Akademii Nauk Kasachskoj Ssr Katalysator zum Hydrieren von Nitroverbindungen
BE790275A (fr) * 1971-11-19 1973-04-19 Inst Francais Du Petrole Catalyseur utilisable en particulier pour la deshydrogenation des hydrocarbures satures
US3804779A (en) * 1972-10-02 1974-04-16 Dart Ind Inc Carbon supported palladium catalyst
US4137254A (en) * 1977-07-27 1979-01-30 Texaco, Inc. Preparation of aromatic nitriles

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5229731A (en) * 1975-08-28 1977-03-05 Polaroid Corp Photographic camera exposure controller

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009529549A (ja) * 2006-03-14 2009-08-20 バイエル・テクノロジー・サービシーズ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング 不均一系触媒による水素化を利用する芳香族アミンの製造方法及び装置
JP2010526791A (ja) * 2007-05-10 2010-08-05 ビーエーエスエフ ソシエタス・ヨーロピア アミンの製造方法
JP2015516970A (ja) * 2012-04-16 2015-06-18 バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG 芳香族ニトロ化合物から芳香族アミンを製造する間に反応を停止するための改良方法
JP2022546362A (ja) * 2019-08-30 2022-11-04 コベストロ、ドイチュラント、アクチエンゲゼルシャフト 芳香族ニトロ化合物を水素化する方法

Also Published As

Publication number Publication date
JPH0234938B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1990-08-07
MX151217A (es) 1984-10-11
BR7905432A (pt) 1980-05-20
ES483534A1 (es) 1980-05-16
DE2849002A1 (de) 1980-05-22
ATE612T1 (de) 1982-02-15
EP0011090B1 (de) 1982-01-27
CA1136651A (en) 1982-11-30
DE2961976D1 (en) 1982-03-11
EP0011090A1 (de) 1980-05-28
ZA794454B (en) 1980-09-24
US4265834A (en) 1981-05-05

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