JPS5455537A - Preparation of dinitrobiphenyl ethers - Google Patents

Preparation of dinitrobiphenyl ethers

Info

Publication number
JPS5455537A
JPS5455537A JP11860377A JP11860377A JPS5455537A JP S5455537 A JPS5455537 A JP S5455537A JP 11860377 A JP11860377 A JP 11860377A JP 11860377 A JP11860377 A JP 11860377A JP S5455537 A JPS5455537 A JP S5455537A
Authority
JP
Japan
Prior art keywords
dinitrobiphenyl
ethers
halonitrobenzenes
hydrogencarbonates
alkali metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11860377A
Other languages
Japanese (ja)
Other versions
JPS5748058B2 (en
Inventor
Tadatoshi Honda
Yoichi Hosono
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP11860377A priority Critical patent/JPS5455537A/en
Publication of JPS5455537A publication Critical patent/JPS5455537A/en
Publication of JPS5748058B2 publication Critical patent/JPS5748058B2/ja
Granted legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To obtain the title compounds useful as raw materials for medicines, pesticides, synthetic resins, etc., by reacting halonitrobenzenes only with alkali metal carbonates or hydrogencarbonates in the presence of nitrous ions in a polar aprotic solvent.
CONSTITUTION: Halonitrobenzenes, e.g. p-chloronitrobenzene, etc. of formula I: (X is halogen; Y1 and Y2 are H, alkyl, alkoxy, or carboxyl groups; n is 1 or 2, at least one of the nitro groups is at the o- or p-position to X) are reacted with alkali metal carbonates, e.g. sodium carbonate, etc., or hydrogencarbonates in the presence of nitrous ions, e.g. sodium nitrite, etc., in an amount of 0.005W0.5 mole per mole of the starting materials in a polar aprotic solvent, e.g. dimethyl sulfoxide, etc. to give dinitrobiphenyl ethers, e.g. bis(4-nitrophenyl)ether, etc. of formula II.
EFFECT: Expensive K salts are unnecessary
COPYRIGHT: (C)1979,JPO&Japio
JP11860377A 1977-10-04 1977-10-04 Preparation of dinitrobiphenyl ethers Granted JPS5455537A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11860377A JPS5455537A (en) 1977-10-04 1977-10-04 Preparation of dinitrobiphenyl ethers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11860377A JPS5455537A (en) 1977-10-04 1977-10-04 Preparation of dinitrobiphenyl ethers

Publications (2)

Publication Number Publication Date
JPS5455537A true JPS5455537A (en) 1979-05-02
JPS5748058B2 JPS5748058B2 (en) 1982-10-14

Family

ID=14740647

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11860377A Granted JPS5455537A (en) 1977-10-04 1977-10-04 Preparation of dinitrobiphenyl ethers

Country Status (1)

Country Link
JP (1) JPS5455537A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007324894A (en) * 2006-05-31 2007-12-13 Japan Radio Co Ltd Tone signal detection circuit for radio equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007324894A (en) * 2006-05-31 2007-12-13 Japan Radio Co Ltd Tone signal detection circuit for radio equipment

Also Published As

Publication number Publication date
JPS5748058B2 (en) 1982-10-14

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