JPH0578544B2 - - Google Patents
Info
- Publication number
- JPH0578544B2 JPH0578544B2 JP7385385A JP7385385A JPH0578544B2 JP H0578544 B2 JPH0578544 B2 JP H0578544B2 JP 7385385 A JP7385385 A JP 7385385A JP 7385385 A JP7385385 A JP 7385385A JP H0578544 B2 JPH0578544 B2 JP H0578544B2
- Authority
- JP
- Japan
- Prior art keywords
- structural formula
- represented
- reaction
- nitrophenylhydrazine
- fluoro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- FPHNVJCVEVNNBA-UHFFFAOYSA-N (2-fluoro-5-nitrophenyl)hydrazine Chemical compound NNC1=CC([N+]([O-])=O)=CC=C1F FPHNVJCVEVNNBA-UHFFFAOYSA-N 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 2
- 125000002490 anilino group Chemical class [H]N(*)C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 6
- 150000001448 anilines Chemical class 0.000 description 6
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 4
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000004009 herbicide Substances 0.000 description 3
- 235000010288 sodium nitrite Nutrition 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 229910021626 Tin(II) chloride Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 235000010265 sodium sulphite Nutrition 0.000 description 2
- 239000001119 stannous chloride Substances 0.000 description 2
- 235000011150 stannous chloride Nutrition 0.000 description 2
- KJVBJICWGQIMOZ-UHFFFAOYSA-N 2-fluoro-5-nitroaniline Chemical compound NC1=CC([N+]([O-])=O)=CC=C1F KJVBJICWGQIMOZ-UHFFFAOYSA-N 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000012954 diazonium Substances 0.000 description 1
- 150000001989 diazonium salts Chemical class 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7385385A JPS61233656A (ja) | 1985-04-08 | 1985-04-08 | ２−フルオロ−５−ニトロフエニルヒドラジン及びその製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7385385A JPS61233656A (ja) | 1985-04-08 | 1985-04-08 | ２−フルオロ−５−ニトロフエニルヒドラジン及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61233656A JPS61233656A (ja) | 1986-10-17 |
| JPH0578544B2 true JPH0578544B2 (de) | 1993-10-29 |
Family
ID=13530125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7385385A Granted JPS61233656A (ja) | 1985-04-08 | 1985-04-08 | ２−フルオロ−５−ニトロフエニルヒドラジン及びその製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61233656A (de) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19501948A1 (de) * | 1995-01-24 | 1996-07-25 | Hoechst Ag | Verfahren zur Herstellung von 2-Fluorphenylhydrazin |
-
1985
- 1985-04-08 JP JP7385385A patent/JPS61233656A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61233656A (ja) | 1986-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US6096923A (en) | Process for the preparation of nitrosourea compounds | |
| JP2003533497A (ja) | アニリン化合物の製造方法 | |
| EP0036636B1 (de) | Verfahren und Zwischenprodukte zur Herstellung von 3,3'-Azo-bis(6-hydroxybenzoesäure) | |
| NO116064B (de) | ||
| US5162584A (en) | Fluorobenzene derivatives | |
| JPH0578544B2 (de) | ||
| US4501919A (en) | Process for the production of serine derivatives | |
| SU856382A3 (ru) | Способ получени циннолин-3-ил-карбоновых кислот или их солей | |
| JP3303050B2 (ja) | アゾニアアダマンタン化合物およびこのものからのアザアダマンタン化合物の製造方法並びに該アゾニアアダマンタン化合物の製造方法 | |
| JPH0761993B2 (ja) | アジドスルホニル安息香酸の製造法 | |
| EP2349980B1 (de) | Verfahren zur herstellung von 2-amino-6-nitrobenzoesäure | |
| JPS60136572A (ja) | トリアゾロン誘導体の製造方法 | |
| US6160139A (en) | Process for the oxidation of pseudodiosgenin diacetate to diosone for the production of 16-dehydropregnenolone acetate | |
| JPH04305572A (ja) | カルボキシル基を有する環状アミン化合物 | |
| JPS63216861A (ja) | ４−ハイドロオキシインドリン類の製造法 | |
| JPH06199806A (ja) | ジフルオロメトキシピラゾール誘導体及びその製造方法 | |
| JP2513159B2 (ja) | Ｎ−ホルミル−Ｌ−α−アスパルチル−Ｌ−フェニルアラニンの製法 | |
| US5300688A (en) | Method for making hydrazide or hydrazine compounds | |
| JPH0713042B2 (ja) | ２，６−ジクロロ−３，４−ジニトロエチルベンゼン及びその製法 | |
| CA2225206C (en) | Aminophenyl ketone derivatives and a method for the preparation thereof | |
| JPS6229544A (ja) | フロロフエノ−ル類の製造法 | |
| JPH0761939A (ja) | 芳香族フッ素化合物の製造方法 | |
| JPS5848531B2 (ja) | Ｐ−ヒドロキシベンズアルデヒドの製造法 | |
| JPH0116825B2 (de) | ||
| JPH02169564A (ja) | ２―クロロ―４―メチルスルホニル―ｍ―キシレン及びその製法 |