JPH0571593B2 - - Google Patents
Info
- Publication number
- JPH0571593B2 JPH0571593B2 JP30157488A JP30157488A JPH0571593B2 JP H0571593 B2 JPH0571593 B2 JP H0571593B2 JP 30157488 A JP30157488 A JP 30157488A JP 30157488 A JP30157488 A JP 30157488A JP H0571593 B2 JPH0571593 B2 JP H0571593B2
- Authority
- JP
- Japan
- Prior art keywords
- naphthalene
- formula
- cycloocta
- tetrahydro
- dithia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- -1 8,10-dithia-8,9,10,11-tetrahydro-7H-cycloocta[de]naphthalene compound Chemical class 0.000 claims description 13
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 18
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 12
- 150000001875 compounds Chemical class 0.000 description 8
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene-acid Natural products C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 8
- 229910015900 BF3 Inorganic materials 0.000 description 6
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- JKNPWHHGFOPCTJ-UHFFFAOYSA-N [8-(sulfanylmethyl)naphthalen-1-yl]methanethiol Chemical compound C1=CC(CS)=C2C(CS)=CC=CC2=C1 JKNPWHHGFOPCTJ-UHFFFAOYSA-N 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 150000001728 carbonyl compounds Chemical class 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000005160 1H NMR spectroscopy Methods 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000000921 elemental analysis Methods 0.000 description 2
- 238000004949 mass spectrometry Methods 0.000 description 2
- 239000012044 organic layer Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 125000004434 sulfur atom Chemical group 0.000 description 2
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 239000013081 microcrystal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920001021 polysulfide Polymers 0.000 description 1
- 239000005077 polysulfide Substances 0.000 description 1
- 150000008117 polysulfides Polymers 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000007363 ring formation reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP30157488A JPH02145582A (ja) | 1988-11-29 | 1988-11-29 | ８，１０―ジチア―８，９，１０，１１―テトラヒドロ―７Ｈ―シクロオクタ〔ｄｅ〕ナフタレン化合物 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP30157488A JPH02145582A (ja) | 1988-11-29 | 1988-11-29 | ８，１０―ジチア―８，９，１０，１１―テトラヒドロ―７Ｈ―シクロオクタ〔ｄｅ〕ナフタレン化合物 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02145582A JPH02145582A (ja) | 1990-06-05 |
| JPH0571593B2 true JPH0571593B2 (enrdf_load_html_response) | 1993-10-07 |
Family
ID=17898583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP30157488A Granted JPH02145582A (ja) | 1988-11-29 | 1988-11-29 | ８，１０―ジチア―８，９，１０，１１―テトラヒドロ―７Ｈ―シクロオクタ〔ｄｅ〕ナフタレン化合物 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH02145582A (enrdf_load_html_response) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0538474B1 (en) * | 1991-03-11 | 1997-07-23 | CHLORINE ENGINEERS CORP., Ltd. | Electrolytic vessel for producing hypochlorite |
-
1988
- 1988-11-29 JP JP30157488A patent/JPH02145582A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0538474B1 (en) * | 1991-03-11 | 1997-07-23 | CHLORINE ENGINEERS CORP., Ltd. | Electrolytic vessel for producing hypochlorite |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02145582A (ja) | 1990-06-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4172074A (en) | Preparation of an antidepressant | |
| SU660592A3 (ru) | Способ получени -циклоалкилметил-2-фениламино-имидазолинов-(2) или их солей | |
| Gasco et al. | Unsymmetrically substituted furoxans. IIII. Methylnitrofuroxan: Its structure and behavior toward nucleophilie substitution | |
| JP2731853B2 (ja) | トリ低級アルカノイルオキシホウ素の製造法 | |
| SU1055333A3 (ru) | Способ получени алкалоидов типа лейрозина или их кислых аддитивных солей | |
| JPH0571593B2 (enrdf_load_html_response) | ||
| GB2036744A (en) | Eburnane derivatives | |
| US5654429A (en) | Method for the preparation of 3-amino-2-chloro-4-alkylpyridines | |
| JP2578797B2 (ja) | Ｎ−（スルホニルメチル）ホルムアミド類の製造法 | |
| SU383373A1 (ru) | Способ получени динатриевой соли дисульфида 3,3-дипропандисульфокислоты | |
| JPS595595B2 (ja) | １５−ヒドロキシイミノ−ｅ−ホモエブルナン誘導体の製造方法 | |
| US3928334A (en) | Process for the production of cefamandole | |
| JP2659587B2 (ja) | ４―アジリジニルピリミジン誘導体及びその製造法 | |
| SU681058A1 (ru) | Способ получени 3-арил-или 3,4-арилзамещенных 6,7-диметоксиизокумаринов | |
| SU687075A1 (ru) | Способ получени 2,3-дизамещенных 6-азаиндола | |
| SU465786A3 (ru) | Способ получени соли 4-хлор-м-толуол или 3,4-дихлорбензолсульфокислоты и -форм пропоксифена | |
| KR910003636B1 (ko) | 벤조페논 옥심화합물의 제조방법 | |
| KR890002251B1 (ko) | 옥사졸 화합물의 제조방법 | |
| KR940006531B1 (ko) | 피리딘 유도체의 제조방법 | |
| KR0179320B1 (ko) | (±)-2-(톨릴술피닐)-시클로펜타데칸-1-온 및 그의 제법 | |
| KR800001450B1 (ko) | 1, 3, 5-트리치환 벤젠 유도체의 제조방법 | |
| SU472966A1 (ru) | Способ получени 2,2 диметил-5 ,5 диизопропил-п-квинквифенила | |
| KR930005625B1 (ko) | 아미노케톤의 제조방법 | |
| RU1810343C (ru) | 4,4-Динитро-2,3-диокситетрагидрофуран и способ его получени | |
| US3865854A (en) | Process of preparation of alkyl tridecatrienoates and intermediates |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |